• Journal of the Korean Ceramic Society
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• v.41 no.2
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• pp.143-150
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• 2004

Biaxial flexure strength (ball-on-3-ball) and fracture toughness (indentation microfracture) of heat-pressable glass-ceramics for dental use were investigated in this study. Crystal phase and microstructure of glass-ceramics were analyzed by XRD. SEM, and TEM. Crack propagation in specimens was not effectively arrested by dispersed crystalline particles. However, higher degree of crystallization probably contributes to strengthening of glass-ceramics. Better clinical reliability can be expected from lithium disilicate glass-ceramic because of its significantly higher biaxial flexure strength and fracture toughness.

• Journal of Biomedical Engineering Research
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• v.17 no.3
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• pp.327-336
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• 1996

This study was performed to investigate the effec% of immersion in water and thermal cycling on the mechanical peoperties of light cured restorative composite resins. Five commerically available light-cured composite resins(Photo Clearfil A : CA, Lite-Fil A . LF, Clearril Photo Posterior CP, Prisms AP.H.. PA, 2100 : ZH) were unto The specimens of 12 m in diameter and 0.7 m in thickness were made, and an immersion in $37^{\circ}C$ water for 7 days and a thermal cycling of 1000 cycles at 15 second dwell time each in $5^{\circ}C$ and $55^{\circ}C$ baths were performed. Biaxial flexure test was conducted using the ball-on-three-ball method at the crosshead speed of 0.5mm/min. In order to investigate the deterioration of composite resins during the thermal cycling test, Weibull analysis for the biaxial flexure strengths was done. Fracture surfaces and the surfaces before and after the thermal cycling test were examined by SEM. The highest Weibull modulus value of 10.09 after thermal cycling tests which means the lowest strength variation, was observed in the CP group, and the lowest value of 4.47 was obsered in the LF Group. Biaxial flexure strengths and Knoop hardness numbers significantly decreased due to the thermal cycling ($\textit{p}$< 0.01), however, they recovered when specimens were drie4 The highest biaxial flexure strength of 125.65MPa was observed in the ZH group after the thermal cycling test, and the lowest value of 64.86MPa was observed in the CA group. Biaxial flexure strengths of ZH and CP groups were higher than those of PA, CF, and CA groups after thermal cycling test($\textit{p}$< 0.05). Knoop hardness numbers of CP group after the thermal cycling test was the highest(95.47 $\pm$ 7.35kg/$mm^2$) among the samples, while that of CA group was the lowest(30.73 $\pm$ 2.58kg/$mm^2$). Knoop hardness numbers showed the significant differences between the CP group and others after the thermal cycling test(($\textit{p}$< 0.05). Fracture surfaces showed that the composite resin failure developed along the matrix resin and the filler/resin interface region, and the cracks propagated in the conical shape from the maximum tensile stress zone.

• Journal of the Korea Concrete Institute
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• v.23 no.4
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• pp.479-486
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• 2011

In this study, we conducted experiment and finite element analysis on the flexural behavior of the round concrete panels according to the evaluation method of biaxial flexural tensile strengths. The Round Panel Test (RPT) and the Biaxial Flexure Test (BFT) were used to determine the biaxial flexural strength of round plain concrete panels. In order to understand the stress distribution on the panels, we measured load-strain relationship at the center of the panels' bottom surface. Test results show that fracture pattern in RPT and BFT panels are similar, and the tensile stress distribution is uniform in all directions at the center of the bottom surface of the panels for both RPT and BFT. The distribution of stresses in two test specimens coincided with the analysis result. The average biaxial flexural strength of RPT is about 29% greater than those of the BFT. The coefficient of variations (COV) of the RPT and BFT for the biaxial flexure strength is 8%, 6%, respectively, which indicates that BFT method is useful and reliable for determining biaxial flexural strengths of the concrete.

• Journal of Dental Rehabilitation and Applied Science
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• v.17 no.3
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• pp.199-204
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• 2001

This study was to investigate the reused possibility of zirconia reinforced glass-ceramic(IPS Empress Cosmo ceramic) with sprue button in the flexure strength and fracture toughness. 40 disk-shaped ceramic specimens (20 specimens: as-pressed material; 20 specimens: reused material) with approximately 1.7 mm thickness and 15 mm diameter were prepared by "lost wax" technique. The remnants(sprue buttons) were used for repressing. The surface treatments for the discs were gradually abraded with 320, 800, 1200, and 2000 grit SiC sandpaper. The specimens were evaluated their flexure strength with the biaxial flexure jig(ball-on-three balls) and their fracture toughness with Vickers Indentation-microfracture test. The Weibull moduli were calculated for biaxial flexural strength. The mean flexure strength and fracture toughness of each group were $122.2{\pm}18.3MPa$, $1.00{\pm}0.09MPa{\cdot}m^{0.5}$ (as-pressed ceramics), and $122.2{\pm}20.3MPa$, $1.01{\pm}0.10MPa{\cdot}m^{0.5}$ (reused ceramics). There were no significant differences in the strength and the fracture toughness between the as-pressed and the reused IPS Empress Cosmo ceramic (P>0.05). This implied zirconia reinforced glass-ceramic(IPS Empress Cosmo ceramic) could be used one more time by reusing of sprue button in the flexure strength and fracture toughness.

• Proceedings of the KACD Conference
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• 2003.11a
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• pp.575-575
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• 2003

The majority of studies comparing the mechanical properties of brittle dental restorative materials now include use of the Weibull Modulus (m). This modulus is determined from analysis of the statistical distribution of strength measurements, which can be determined using a variety of methods, including biaxial flexure, 3pt bend and 4pt bend. In comparing materials it is usually implicitly assumed that the modulus (m) is independent of test method although it is recognised to be highly dependent on flaw distributions. However, in some cases flaw distributions can be modified by sample preparation and test method may modify stressing patterns. This study investigated the pattern of strength and m in two light setting materials.

• The Journal of Korean Academy of Prosthodontics
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• v.38 no.5
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• pp.595-605
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• 2000

Dental ceramics have good aesthetics, biocompatibility, low thermal conductivity, abrasion resistance, and color stability. However poor resistance to fracture and shrinkage during firing process have been limiting factors in their use, particularly in multiunit ceramic restorations. A new method for making all-ceramic crowns that have high strength and low processing shrinkage has been developed and is referred to as the Vita In-Ceram method. This study was performed to investigate the effect of $CeO_2$ addition in borosilicate glasses on the strength of alumina-glass composites. Porous alumina compacts were prepared by slip casting and sintered at $1,100^{\circ}C$ for 2 hours. Dense composites were made by infiltration of molten glass into partially sintered alumina at $1,140^{\circ}C$ for 4 hours. Specimens were polished sequentially from #800 to #2000 diamond disk. and the final surface finishing on the tensile side was received an additional polishing sequence through $1{\mu}m$ diamond paste. Biaxial flexure test was conducted by using ball-on-three-ball method at a crosshead speed of 0.5mm/min. To examine the microstructural aspect of crack propagation in the alumina-glass composites, Vickers-produced indentation crack was made on the tensile surface at a load of 98.0 N and dwell time of 15 sec, and the radial crack patterns were examined by an optical microscope and a scanning electron microscope. The results obtained were summarized as follows; 1. The porosity rates of partially sintered alumina decreased with the rising of firing temperature. 2. The maximum biaxial flexure strength of 423.5MPa in alumina-glass composites was obtained with an addition of 3 mol% $CeO_2$ in glass composition and strength values showed the aspect of decrease with the increase of $CeO_2$ content. 3 The biaxial flexure strength values of alumina-glass composites were decreased with rising the firing temperature. 4. Observation of the fracture surfaces of alumina-glass composites indicated that the enhancement of strength in alumina-glass composites was due to the frictional or geometrical inter-locking of rough fracture surfaces and ligamentary bridging by intact islands of materials left behind the fracture front.

• Restorative Dentistry and Endodontics
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• v.31 no.1
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• pp.58-65
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• 2006

The possibility of applying a hi-axial flexure strength test on composite resin was examined using three point and hi-axial flexure strength tests to measure the strength of the light-cured resin and to compare the relative reliability using the Weibull modulus. The materials used in this study were light-curing restorative materials, $MICRONEW^{TM},\;RENEW^{(R)}$ (Bisco, Schaumburg, USA). The hi-axial flexure strength measurements used the piston-on-3-ball test according to the regulations of the International Organization for Standardization (ISO) 6872 and were divided into 6 groups, where the radius of the specimens were 12mm (radius connecting the 3-balls: 3.75mm), 16 mm(radius connecting the 3-balls: 5mm), and the thickness were 0.5mm, 1mm, 2mn for each radius. The hi-axial flexure strength of the $MICRONEW^{TM}\;and\;RENEW^{(R)}$ were higher than the three point flexure strength and the Weibull modulus value were also higher in all of the bi-axial flexure strength groups, indicating that the hi-axial strength test is relatively less affected by experimental error. In addition, the 2 mm thick specimens had the highest Weibull modulus values in the hi-axial flexure strength test, and the $MICRONEW^{TM}$ group showed no significant statistical difference (p>0.05). Besides the 2mm $MICRONEW^{TM}$ group, each group showed significant statistical differences (p<0.05) according to the thickness of the specimen and the radius connecting the 3-balls. The results indicate that for the 2mm group, the hi-axial flexure strength test is a more reliable testing method than the three point flexure strength test.

• Computers and Concrete
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• v.4 no.5
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• pp.363-376
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• 2007

The paper presents the development of an adaptable strut-and-tie model that can be applied to the design or analysis of four-pile caps that support axial compression and biaxial flexure from a supported rectangular column. Due to an absence of relevant test data, the model is validated using nonlinear finite element analyses (NLFEA). The results indicate that the use of the proposed model would lead to safe and economical designs. The proposed model can be easily extended to any number of piles, providing a rational procedure for the design of wide range of pile caps.

• Structural Engineering and Mechanics
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• v.10 no.2
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• pp.165-180
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• 2000

An analytical model with tension softening for the prediction of the capacity of prestressed concrete beams under pure torsion and under torsion combined with shear and flexure is introduced. The proposed approach employs bilinear stress-strain relationship with post cracking tension softening branch for the concrete in tension and special failure criteria for biaxial stress states. Further, for the solution of the governing equations a special numerical scheme is adopted which can be applied to elements with practically any cross-section since it utilizes a numerical mapping. The proposed method is mainly applied to plain prestressed concrete elements, but is also applicable to prestressed concrete beams with light transverse reinforcement. The aim of the present work is twofold; first, the validation of the approach by comparison between experimental results and analytical predictions and second, a parametrical study of the influence of concentric and eccentric prestressing on the torsional capacity of concrete elements and the interaction between torsion and shear for various levels of prestressing. The results of this investigation presented in the form of interaction curves, are compared to experimental results and code provisions.

• Journal of Dental Rehabilitation and Applied Science
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• v.30 no.2
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• pp.102-111
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• 2014

Purpose: Surface damage and bonding strength difference after micromechanical treatment of zirconia surface are to be studied yet. The aim of this study was to evaluate the difference of fracture resistance and bonding strength between more surface-damaged group from higher air-blasting particle size and pressure, and less damaged group. Materials and Methods: Disk shape zirconia ($LAVA^{TM}$) was sintered and air-blasted with $30{\mu}m$ particle size (Cojet), under 2.8 bar for 15 seconds, $110{\mu}m$ particle size (Rocatec), under 2.8 bar for 15 seconds, and $110{\mu}m$ particle size (Rocatec), under 3.8 bar for 30 seconds respectively. Biaxial flexure test and bonding failure load test were performed serially (n = 10 per group). For bonding test, specimens were bonded on the base material having similar modulus of elasticity of dentin with $200{\mu}m$-thick resin cement for tension of surface damage. Failure load of bonding was detected with acoustic emission (AE) sensor. Results: There were no significant differences both in the biaxial flexure test and bonding failure load test between groups (P > 0.05). Sub-surface cracks were all radial cracks except for two specimens. Conclusion: Within the limitations of no aging under monotonic load test, surface damage from higher air-blasting particle size and pressure was not significant. Evaluations of failure load with bonded zirconia disks was clinically relevant modality for surface damage and bonding strength, simultaneously.