• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2008년도 추계학술대회A
• /
• pp.1-6
• /
• 2008

Due to the self-similarity of Berkovich and conical indenters, different materials may show the same loaddepth curve for single indentation. In this study, we first compare the load-depth characteristics of conical and Berkovich indenters via finite element method. We also analyze the variation of load-depth curves with angle of Berkovich indenter, indentation parameters, and material properties. With numerical regressions of obtained data, we then propose dual-Berkovich indentation formulae for material property evaluation. The proposed approach provides the values of elastic modulus, yield strength and strain-hardening exponent and corresponding stress-strain curve with an average error of less than 3%. The method is valid for any elastic indenters made of tungsten carbide and diamond for instance.

• 한국정밀공학회지
• /
• 제22권10호
• /
• pp.167-173
• /
• 2005

The Berkovich nano-indentation is an indentation test method analyzing mechanical properties of materials such as hardness and elastic modulus. The length scale of the penetration is measured in nanometers. Therefore, this method becomes widely useful for analyzing the mechanical property of thin film which can not be measured before. In this paper, comparing two results of the load-displacement curve obtained by the Berkovich nano-indentation and the 3-D finite element analysis, it was confirmed that the 3-D finite element analysis is useful. The phenomenon of pile-up and sink-in due to material properties was discussed by the finite element analysis.

• 대한기계학회논문집A
• /
• 제38권9호
• /
• pp.943-951
• /
• 2014

마이크로/나노 압입시험에 사용되는 각뿔 혹은 원뿔형 압입자의 선단 형상은 제작한계 및 사용 중 마모 등으로 인해 필수적으로 곡면 형태를 띄게 된다. 많은 압입시험 관련 연구에서 각뿔형 압입자의 선단 형상은 편의상 구형으로 가정한 후, 얕은 압입에 대한 구형압입 이론식을 적용하고 있다. 이러한 가정에는 근본적으로 두 가지 문제점이 있는데, 첫 번째로 이론해의 정확성은 재료 물성치 및 압입자 형상에 따라 변화한다는 점이며, 두 번째로 각뿔형 압입자의 실제 선단 형상은 이상적인 구형이 아니라는 점이다. 본 연구에서는 유한요소해석에 기반하여 압입시험에 미치는 이 두 요소의 영향을 분석한다. 먼저 탄성 구형 압입시험에 대해 푸아송비와 하중-변위 곡선의 상관관계를 살펴보고, 이를 기반으로 수정된 구형 탄성 압입 관계식을 제시한다. 이어 가정된 Berkovich 선단 형상의 3차원 유한요소해석으로부터 압입깊이에 따른 하중-변위 곡선의 특성을 분석한다.

• 한국정밀공학회:학술대회논문집
• /
• 한국정밀공학회 2004년도 추계학술대회 논문집
• /
• pp.343-346
• /
• 2004

In recent years, various forms of indentation testing have been increasingly used to determine the material properties of specimens. This technique, particularly the nano-indentation method , has been extended to the testing of coating systems in order to calculate the individual properties of the thin coatings and the substrates. However, the interpretation of the test data to achieve this is complex and continues to be a widely studied subject. Based on the finite element method of coated surfaces indented by a Berkovich diamond tip, this paper describes methods for combining FEM and experimental indentation testing to determine coating modulus and hardness independent of substrate effects. Using this proposed methodology, testing and FEM to measure coefficients of friction of sheet steel for outer panel were studied.

• 한국재료학회지
• /
• 제13권1호
• /
• pp.53-58
• /
• 2003

For the rib materials in PDP(plasma display panel), an effective method to improve the mechanical properties is to form a composite material by reinforcing a glass matrix with rigid fillers, such as alumina and titania powders. In this study, two types of ribs with different volume percent of fillers and with different glass matrix were tested for hardness, Young's modulus with the Berkovich indentation. As a result, cracks appeared around at the load of 1345 mN for the dense type of rib, while porous one endured until 2427 mN without any crack formation. Young's modulus and hardness decreased at the range: 90∼65 GPa, 9∼4 GPa, respectively as a function of indent load. Thus, a new method with nanoindenter represents a possible evaluation method for mechanical properties of barrier ribs.

• 대한기계학회논문집A
• /
• 제37권12호
• /
• pp.1453-1463
• /
• 2013

본 연구에서는 유한요소해석과 압입시험으로 압입자 형상이 압입균열특성에 미치는 영향을 조사했다. 본 논문에서는 Lee 등(2012)이 제시한 cohesive zone 모델특성 및 균열생성, 진전을 위한 해석조건에 기초해 다양한 균열해석을 수행했다. 우선, 사각뿔 및 삼각뿔 압입균열 시험과 해석을 비교해 해석모델의 유효성을 검증했다. 아울러 비대칭 압입자에 의한 압입시, 압입하부에서 비대칭 균열의 발생여부를 해석적으로 관찰했다. 최종적으로 압입발생 균열수와 균열길이 관계를 조사했다. 균열수와 균열길이 관계 및 동일 압입자형상(압입자 모서리수)에서 압입자각에 따른 균열길이 변화를 이용하면, 특정 압입자 형태의 압입시험에서 얻은 균열길이 만으로 다양한 압입자 형태의 균열길이를 예측할 수 있다.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2004년도 춘계학술대회 논문집
• /
• pp.148-151
• /
• 2004

Mechanical properties such as Young's modulus and hardness of thin film in coated steel are difficult to determine by nano-indentation from the conventional analysis using the load-displacement curve. Therefore, an analysis of the nano-indentation loading curve was used to determine the Young's modulus, hardness and strain hardening exponent. A new method is recently being developed for plasticity properties of materials from nano-indentation. Elastic modulus of the thin films shows relatively small influence whereas yield strength and strain hardening are found to have significant effect on measured data. The load-displacement behavior of material tested with a Berkovich indenter and nano-indentation continuous stiffness method is used to measure the modulus and hardness through thin films.

• 소성∙가공
• /
• 제13권8호
• /
• pp.731-737
• /
• 2004

Mechanical properties such as Young's modulus and hardness of thin film in coated steel are difficult to determine by nano-indentation from the conventional analysis using the load-displacement curve. Therefore, an analysis of the nano-indentation loading-unloading curve was used to determine the Young's modulus, hardness. A new method is recently being developed for elastic-plastic properties of materials from nano-indentation. Elastic modulus of the thin films shows relatively small influence whereas yield strength is found to have significant effect on measured data. The load-displacement curves of material tested with a Berkovich indenter and nano-indentation continuous stiffness method is used to measure the modulus and hardness through thin films, and then these are computed using the analysis procedure. The developed neural networks apply also to obtain reliable mechanical properties.

• Tribology and Lubricants
• /
• 제25권3호
• /
• pp.163-170
• /
• 2009

We developed a compact micro indentation testing device (designated SNUT) which is capable to measure Young's modulus of a sample using depth and applied load data during indentation. Performance of this device was evaluated using pure Ti, pure Ni, and die steel (SKD11). As a result of analysing the indentation test data, the frame compliance $C_f$ was found to influence mainly the modulus by 80% among several factors affecting accuracy of Young's modulus. Project area, which was determined by indirect indentation method, was modified using direct SEM observation. Finally, Young's modulus error was reduced to 5% after taking into consideration the frame compliance and modified projected area from 80% error without any these two correction factors. The performance of SNUT and MTS instruments was compared using same specimen (pure Ti).

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2005년도 춘계학술대회 논문집
• /
• pp.225-228
• /
• 2005

The purpose of this study is to investigate effects of the plastic/elastic deformation energy on wet etching characterization on the surface of material by using the nanoindentation and HF wet etching technique. Indents were made on the surface of Pyrex 7740 glass by the hyperfine indentation process with a Berkovich diamond indenter, and they were etched in $50\;wt\%$ HF solution. After etching process, convex structure was obtained due to the deformation-induced hillock phenomena. In this study, effects of indentation process parameters (normal load, loading rate) on the morphologies of the indented surfaces after isotopic etching were investigated from an angle of deformation energies.