• 한국표면공학회지
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• 제50권2호
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• pp.108-113
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• 2017

We investigated the effect of graphite electrode geometry and combination on nanocarbon material synthesis using underwater discharge plasma(UDP). The UDP system consists of two graphite electrodes and beaker filled with de-ionized water. A high voltage of 15 kV with a frequency of 25 kHz is applied to produce UDP using an alternating-current power source. The UDP system with conical electrodes produced the largest amount of products due to the concentration of electrical fields between electrodes. In addition, hollow-shaped stationary electrode and conical-shaped moving electrode stores discharge-induced bubbles and maintains longer reaction time. We found from Raman spectroscopy and electron microscopy that high quality carbon nanomaterials including carbon nanotubes are synthesized by the UDP system.

• 보존과학회지
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• 제36권6호
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• pp.494-504
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• 2020

한국토지주택공사 경기지역본부에서 시행 중인 화성 향남 2지구 동서간선도로 건설 부지 내에서 총 10개소(A~J) 유적지가 확인되었다. 화성 요리 고분군 유적은 H지점에 해당하는 곳으로 조사 결과, 다양한 삼국시대 고분군이 확인되었고 그중 목곽묘에서 금동식리와 금동관모 등이 출토되었다. 본 연구 대상 토기는 목곽묘에서 출토된 유일한 토제 유물로 태토는 연질이며, 적갈색의 느슨한 기질에 1 mm 미만의 석영, 장석이 비짐으로 첨가되었다. 토기의 소성 온도는 운모류가 소멸되지 않고 석영의 상전이 광물인 트리디마이트(tridimite)가 생성되지 않았으며, 800℃에서 견운모의 탈수 작용에 의한 흡열피크가 미약하게 확인되는 점으로 보아 800~870℃로 추정된다. 토기는 유적 위로 지층이 형성되면서 발생된 토압, 동결과 융해의 반복 등 여러 원인에 의해 매우 약화된 상태였다. 토기만 단독으로 수습하기 불가능한 상황이었으므로 토기를 고정하고 있던 주변 토양을 같이 수습하고 보존처리실로 이동하여 체계적으로 안전하게 보존처리하였다.

• Journal of Biosystems Engineering
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• 제28권4호
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• pp.351-360
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• 2003

This study was carried out to settle the plugging problem which occurs frequently when agricultural wettable powder is used in pest control work using the crushing and the dispersing effects caused by irradiation of ultrasonic wave. Sonication was applied to the wettable powder suspension in a beaker for 30 seconds using a 28 kHz, 200 W PZT BLT, and the image of suspension before and after sonication was observed using a microscope and a SEM. The image of tow commercial wettable powder suspensions in water observed using an optics microscope showed that the agglomerated particles were irregularly distributed over the whole observed region when stirred mechanically, while showing more uniform distribution composed of comparatively single particles in the whole observed region after sonication. Concerning the above, the projected areas of particles in the four suspensions after sonication were decreased distinctively in the observed range of the microscope and the atomization of crystals was much developed. Over the measured range of 5.6∼4,157 ${\mu}$m particle size, the overall projected area of particles was decreased to 58.3∼89.6% on the average after sonication. When the SEM images of sonicated wettable powder suspensions dissolved in water and CH$_3$OH were compared to the suspensions before sonication, such phenomena as the atomization of particles, the expansion of voids between particles, the reduction and the decrease of agglomerated particle groups, and the progress of crack developments on the surface of flake-shaped particles were observed. It seemed possible that the plugging problem that occurs frequently in pest control machine when using wettable powder would be settled by the use of sonication.