• Title/Summary/Keyword: Basic alumina

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Basic Experimental Investigations to UV Laser Micro-Machining of Nano-Porous Alumina Ceramic Material (나노 다공 구조를 가진 알루미나 재료의 UV 레이저 미세가공에 관한 실험적 기초 연구)

  • Shin, Bo-Sung;Lee, Jung-Han
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.11 no.1
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    • pp.62-67
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    • 2012
  • Recently UV laser is widely used to process micro parts using various materials such as polymers, metals and ceramics because it has a very high intensity at the focused spot area. It is generally known that there are still some difficulties for alumina($Al_2O_3$) ceramics to directly make micro patterns like holes and lines on the surface of working material using 355nm UV laser because the alumina has a very low absorption coefficient at that wavelength. But nowadays new alumna with nano-porous holes is developed and applied to advanced micro functional parts of IT, BT and BT industries. In this paper, we are going to show the mechanism of photo-thermal ablation for nano-porous ceramics. Inside hole there is a lot of multiple reflections along the depth of hole. Experimentally we can find the micro hole drilling and micro grooving on the surface of nano-porous alumina.

Removal of I- and IO3- from Aqueous Solution (활성알루미나를 이용하여 방사성 폐수 중 I-와 IO3-를 제거하는 방법)

  • Lim, Heon-Sung;Lee, Sueg-Geun
    • Analytical Science and Technology
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    • v.22 no.6
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    • pp.519-523
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    • 2009
  • $^{129}I$ is especially one of the most harmful radioactive elements because of its long half-life ($t_{1/2}$=$1.7{\times}10^7$ yr). The efficient removal of iodide ($I^-$) and iodate (${IO_3}^-$) in a aqueous solution by adsorption using activated alumina and activated carbon was studied. The removal efficiency was over 99% for iodide ion with silver treated basic alumina and iodate ion with acidic alumina or silver treated acidic alumina without any chemical addition or physical treatments.

Nitrate Removal and Recycling Technique (질산 제거 및 재이용 기술)

  • Sim, Sang Jun;Lee, Kyung Hee;Cho, Young Sang
    • Clean Technology
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    • v.3 no.2
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    • pp.31-33
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    • 1997
  • Nitrate contamination in surface water and ground water have increased in Korea. This trend has raised concern because nitrates caused methemoglobinemia in infants. To remove nitrates from waters, various purification processes including ion-exchange, biological denitrification, and chemical denitrification are currently in use for the treatment of water. However, little economically advantageous process exists for the industrial scale treatment of effluents highly polluted with nitrates. A new process has been developed for nitrate and other salts removal from polluted waters. Alumina cement and lime served as precipitating agents to remove nitrate with stirring at basic pH. Decreasing alumina content in alumina cement result in a increasing in nitrate removal yield. Stable removal of nitrate(1000mg/L) was readily achieved by two-stage removal process.

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Studies on Wear Mechanism of High Alumina Brick for Arc-furnace Roof (아-크로 천정용 고알루미나질 벽돌의 용손기구에 관한 연구)

  • 허삼덕;오기동
    • Journal of the Korean Ceramic Society
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    • v.23 no.2
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    • pp.55-63
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    • 1986
  • In variuos physcial and chemical cause of damage of refractories for steel makin the clarification of the wear mechanism of brick is situated on important factor. In the present paper the wear mechanism of high alumina brick for the arc-furnace roof were inves-tigated by means of XRD, EPMA. SEM and microscopy. The results obtained were summerized as follows : (1) The altered layers which exist in high alumina brick used for arc-furnace roof were verified by mineral chemical analysis and EPMA. (2) The diffusion of materials combined with slag dust and iron oxide from furnace atmosphere in high basic process from hot face to interior was verified. (3)Activation energy for the synthesized slag permeated into the unused brick texture was 47-51 kcal per mole.

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Thermal and Mechanical Properties of Alumina Cementitious Composite Materials (알루미나 시멘트에 기반한 복합재료의 열역학적 특성)

  • Yang, In-Hwan;Lee, Jung-Hwan;Choi, Young-Cheol
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.3 no.3
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    • pp.199-205
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    • 2015
  • The mechanical and thermal properties of high temperature aluminate cementitious thermal storage materials were investigated in this paper. Alumina cement was used as basic binder and the effect of the replacement of fly ash, silica fume, calcium sulfo-aluminate and graphite for alumina cement was investigated. Experiments were performed to measure mechanical properties including compressive strength before and after thermal cycling, and split tensile strength, and to measure thermal properties including thermal conductivity and specific heat. Test results show that the residual compressive strengths of mixtures with alumina cement only, or alumina cement and silica fume were greater than those of the others. Additionally, the specific heat of mixture with graphite was largest in all the mixtures used in the study. The results of this study could be used to provide realistic information for material properties in thermal energy storage concrete in the future.

Effects of the Content of MgO Additive and Sintering Temperature on the Densification of Alumina Insulator (인슐레이터용 알루미나의 치밀화에 미치는 MgO의 함량과 소결 온도의 영향)

  • Ri Joo Kim;Han Gyeol Jeong;Ye Ji Son;Sang Ki Ko;Hyun Seon Hong
    • Journal of Powder Materials
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    • v.30 no.3
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    • pp.249-254
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    • 2023
  • The influence of MgO addition on the densification and microstructure of alumina (Al2O3) was studied. Compacted alumina specimens were manufactured using ball-milling and one-directional pressing followed by sintering at temperatures below 1700℃. Relative density, shrinkage, hardness, and microstructure were investigated using analytical tools such as FE-SEM, EDS, and XRD. When the MgO was added up to 5.0 wt% and sintered at 1500℃ and 1600℃, the relative density exhibited an average value of 97% or more at both temperatures. The maximum density of 99.2% was with the addition of 0.5 wt% MgO at 1500℃. Meanwhile, the specimens showed significantly lower density values when sintered at 1400℃ than at 1500℃ and 1600℃ owing to the relatively low sintering temperature. The hardness and shrinkage data also showed a similar trend in the change in density, implying that the addition of approximately 0.5 wt% MgO can promote the densification of Al2O3. Studying the microstructure confirmed the uniformity of the sintered alumina. These results can be used as basic compositional data for the development of MgO-containing alumina as high-dielectric insulators.

Cross-sectional TEM Specimen Preparation of GaN-based Thinfilm Materials Using Alumina Dummy Filler (Alumina dummy 충전재를 이용한 GaN 기반 박막재료의 단면 TEM 시편준비)

  • Oh, Sang-Ho;Choi, Joo-Hyoung;Song, Kyung;Jeung, Jong-Man;Kim, Jin-Gyu;Yu, In-Keun;Yoo, Suk-Jae;Kim, Young-Min
    • Applied Microscopy
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    • v.39 no.3
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    • pp.277-281
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    • 2009
  • Practical difficulties for preparing a good crosssectional specimen of GaN-based materials for transmission electron microscopy have arisen due to large difference of mechanical properties between hard ceramic substrate and soft GaN-layered materials. Uneven polishing, sudden cracking, delamination, and selective sputtering during the conventional wedge polishing technique are often encountered as experimental hindrances. The preparation technique based on Strecker's method can be applied to overcome these difficulties, which eventually leads to mechanically stable TEM samples independent of the mechanical properties of materials. The basic idea is to use hard ceramic dummy filler for embedding the sample of interest into the dummy frame. In this study, we applied this technique into preparing cross-sectional TEM specimen of the GaN-based materials with mechanical instability and demonstrated usefulness of this hard dummy filler method in which the possible modifications of the sample of interest during the preparation must be avoidable. In addition, practical precautions during the preparation were discussed.

Properties of Repair Cement Mortar with C12A7-based Alumina Cement and Nitrite for Low Temperature Curing (C12A7계 알루미나시멘트 및 아질산염을 사용한 저온환경 보수시공용 시멘트 모르타르의 특성)

  • Park, Jung-Hoon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.4
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    • pp.124-131
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    • 2017
  • The purpose of this study is to evaluate the basic performance of cement mortar for repair using alumina cement and nitrite can be cured in low temperature environment. For this purpose, the repair mortar used in the domestic construction site was selected and the experimental evaluation was carried out by adjusting the mixing amount by substituting alumina cement and nitrite for the blending ratio. The experimental test results confirmed that alumina cement and nitrite were replaced with the repair mortar, the initial strength was improved. Also, the chemical resistance was improved, the shrinkage behavior was decreased, and the resistance to freezing and thawing was increased. As a result, applying alumina cement and nitrite at a ratio of 2:1 at 7.5%, the surface condition was maintained for 5 months or longer and it was judged to be excellent in practical use for external structures.

Properties of inorganic components in the specified waste (지정폐기물 내 미량 무기물질의 특성)

  • Kwon, Young-Hyun;Shon, Byung-Hyun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.12 no.7
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    • pp.3327-3333
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    • 2011
  • The interest on the recovery of thermal energy using the industrial waste has been rising to solve the problems of continuous increase of waste generation and the depletion of the fossil fuel recently. To recovery from the waste among the new recyclable energies has been proved as the most favorable when the potential value of energy source is compared. The RDF made from the industrial waste has been approved as the most economical method. This research has analyzed the heavy metal components containing in the industrial waste. The concentration of Cl and S in the industrial waste generated in C-industrial complex are slightly high than that of the B- and A-industrial complex. The main components generated from A-industrial complex, B-industrial complex, and C-industrial complex are alumina-silicates, calcium alumina silicates, and the mixture of lime and calcium alumina silicate. These results could be used to reveal the origin of inorganic components in industrial waste and utilized as a basic data to improve the performance of the RDF as fuel.