• Title/Summary/Keyword: Ball-on-3-ball test

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Study on Ti-Cu-N thin film for improvement of mechanical propertiesn by copper doping (TiN 기지위에 Cu doping에 의한 Ti-Cu-N 박막의 기계적 특성 향상에 관한 연구)

  • 이혁민;김상식;박헌규;이호영;한전건
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2001.06a
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    • pp.13-13
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    • 2001
  • 현재 초고속 가공 공구의 국내 시장은 150억원이며 향후 3년 내에 1500억원으로 급성 장활 전망이다. 무윤활 초고속 가공을 실현하기 위해서는 윤활특성이 우수한 초고경도 코팅의 개발이 필요하며 이를 통해 기계설비의 수명향상과 폐유문제 해결을 기대할 수 있다. 기존의 고체윤활 코팅은 초고경도 코팅의 상부에 $MoS_2$, Graphite 등 윤활성 박막을 합성하였으나, 이들은 Hexagonal 구조의 연질 박막이며 수분이 존재하는 대기중에서는 윤활 및 내마모 특성이 급격히 저하된다. 환경친화 대체소재 개발의 일원으로 TiN, ZrN 박막 등이 이미 개발되었고 기계적 특성이 우수하여 널리 응용되고 있으나 아직 경도(약 20GPa 내외) 및 윤활성의 한계 (마찰계수 $\mu=O.6$)를 극복하지 못하고 있다. TiN박막 위의 Cu의 첨가는 TiN의 구조와 성질을 크게 변화시키는 것으로 알려져 있다. 따라서 본 연구에서는 TiN 기지 위에 Cu를 도핑함으로써 경도의 상승을 통환 내구력의 향상과 마찰계수의 감소를 통한 윤활성의 향상을 보고자하였다. TiN합성의 안정화를 위하여 magnetron sputtering과 arc ion pIatingd을 병용한 hybrid 공정을 이용하였다. Cu첨가에 따른 결정 성장 거동의 변화를 보기 위해 XRD 분석을 실행하였고, EDS 분석을 통해 Cu target 전류밀도에 의한 기지내의 Cu의 함량변화를 고찰하였으며, 경도 및 윤활특성을 고찰하기 위해서 경도 시험과 마모 시험(ball-on disc type test)를 하였다.

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The Formation of Nitride and Enhancement of Mechanical Properties of Al Alloy by Nitrogen Implantation (Al합금에서 질소이온주입에 의한 질화물 형성과 기계적 특성 향상)

  • Jeong, Jae-Pil;Lee, Jae-Sang;Kim, Kye-Ryung;Choi, Byung-Ho
    • Journal of the Korean institute of surface engineering
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    • v.39 no.5
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    • pp.235-239
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    • 2006
  • The aluminum nitride(AlN) layer on Al7075 substrate has been formed through nitrogen ion implantation process. The implantation process was performed under the conditions : 100 keV energy, total ion dose up to $2{\times}10^{18}\;ions/cm^2$. XRD analysis showed that aluminum nitride layers were formed by nitrogen implantation. The formation of Aluminum nitride enhanced surface hardness up to 265HK(0.02 N) from 150HK(0.02 N) for the unimplanted specimen. Micro-Knoop hardness test showed that wear resistance was improved about 2 times for nitrogen implanted specimens above $5\;{\times}\;10^{17}\;ions/cm^2$. The friction coefficient was measured by Ball-on-disc type wear tester and was decreased to 1/3 with increasing total nitrogen ion dose up to $1\;{\times}\;10^{18}ions/cm^2$. The enhancement of mechanical properties was observed to be closely associated with AlN formation. AES analysis showed that the maximum concentration of nitrogen increased as ion dose increased until $5\;{\times}\;10^{17}\;ions/cm^2$.

An enhancement in wear property of UHMWPE used in joint prosthesis (인공관절에 사용되는 UHMWPE의 내마모성 향상에 관한 연구)

  • Kim, K.T.;Lee, C.W.;Choi, J.B.;Choi, K.
    • Proceedings of the KOSOMBE Conference
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    • v.1996 no.11
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    • pp.3-6
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    • 1996
  • The Ultra-high molecular weight polyethylene (UHMWPE) is exclusivity used as the articulation component with metal or ceramic materials in artificial joint prosthesis because of its good mechanical properties. In the long term however, wear of UHMWPE causes complex problems and hence causes loosening of He prosthesis. In this study, we tried to enhance the wear property of UHMWPE by attaching a hydrophilic graft on the UHMWPE surface and by improving surface hardness without deteriorating the mechanical properties of UHMWPE. This was achieved by ion implantation and by ${\gamma}$-irradiation to the surface in acrylic acid solution and by photo-polymerization in divinylbenzen (DVB), diallysophthalate (DAIP) solution. The wear test was performed by a wear testing machine of ball-on-disk type devised by the authors. The UHMWPE with hydrophlic surface and increased surface hardness developed by above treatments showed less volumetric wear.

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Effects of Recreational Therapy on Dementia Behavior, Affection, and Activity of Daily Living of Senile People with Dementia (오락요법이 치매노인의 치매행동 및 정서와 일상생활수행능력에 미치는 영향)

  • Kim, Hee-Kyung;Choi, Eun-Sook
    • Korean Journal of Adult Nursing
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    • v.17 no.1
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    • pp.44-55
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    • 2005
  • Purpose: The purposes of this study were to examine the effects of recreational therapy (60 minutes * 3times/week * 6weeks) on dementia behavior & affection, and activity of daily living of senile people with dementia. Methods: The subjects were 27 senile people with dementia, 16 experimental group, 11 control group, admitted at K hospital in Chungnam province in quasi-experimental study. The recreational therapy program was developed, based on the recreational program for senile welfare made by athletics science research institute in Chungnam National University(1997). It consisted of rhythm game, ball play, and beanbag game. The data were collected through questionnaires from May 1st to June 10th 2003 and were analyzed using descriptive statistics, ${\chi}^2$-test, Fisher' exact test, and Man Whitney U test. Result: The dementia behavior and affection score was significantly different between the two groups (U=32.5, p=.005). The ADL score was significantly different between the two groups (U=12.0, p=.000). There were significant decrease in dementia behavior & affection, and improvement in ADL in the experimental group compared to the control group. Conclusion: Recreational therapy intervention was proved effect in decreasing dementia behavior & affection and promoting ADL of senile people with dementia. We recommended re-test in containing a communicating variable.

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Development and Performance Test of a Spherical Reaction Wheel Actuator with Magnetic Levitation (자기부상을 적용한 구체 반작용휠 구동기 개발 및 성능 시험)

  • Kim, Dae-Kwan;Yoon, Hyung-Joo;Kim, Yong-Bok;Kang, Woo-Yong;Choi, Hong-Taek
    • Journal of Advanced Navigation Technology
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    • v.16 no.5
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    • pp.731-737
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    • 2012
  • In the present study, a feasibility study on an innovative satellite attitude control actuator is performed. The actuator is specially designed to generate the reaction torque in an arbitrary axis, so that a satellite attitude can be controlled by using itself. It consists of a spherical flywheel and electromagnets for levitation and rotation control of the ball. As the earlier study, a rotating performance test on the spherical actuator is conducted in a single rotating axis and vertical levitation condition. From the test results, it can be confirmed that the maximum speed and torque of the innovative device are 7,200rpm and 0.7Nm, respectively. Using a velocity-voltage characteristic curve of the spherical motor, an open-loop control (V/f constant control) is performed, and the test results show excellent control performance in acceleration and deceleration phases.

Quantitative Analysis on the Damage of the Austenitic Stainless Steel under the Simultaneous Cavitation Bubble and Solid Particle Collapses (오스테나이트계 304 스테인리스강의 케비테이션 기포 및 고체 입자 동시 충격 손상의 정량적 고찰)

  • Hong, Sung-Mo;Park, Jin-Ju;Lee, Min-Ku;Rhee, Chang-Kyu
    • Korean Journal of Metals and Materials
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    • v.48 no.10
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    • pp.893-900
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    • 2010
  • In the present work, the impact loads and their effects on the surface damage under the simultaneous cavitation bubble and solid particle collapses in the sea water have been quantitatively investigated for the austenitic 304 stainless steel by using a vibratory cavitation test device. To do this, angular $SiO_2$ solid particles with an average size of $150{\mu}m$ were dispersed into the test liquid, and the measured impact amplitudes were converted into the impact loads by a steel ball drop test. The maximum impact load was determined to be 28.2 N in the absence of solid particles, but increased to 33.7 N in the presence of solid particles. In addition, the critical impact loads, $L_{crit}$, required to generate pits with sizes greater than $3{\mu}m$ were measured to be 19.6 N and 16.6 N, respectively, for the cavitation bubble collapse and solid particle collapse. As a result of the cavitation erosion test, the incubation time and erosion rate were 1.2 times lower and 1.5 times higher, respectively, by a solid particle collapse compared to those only by the cavitation bubble collapse, indicating a drastic decrease in a resistance to cavitation erosion by the solid particle collapse.

Study on the Improvement of BGA Solderability in Electroless Nickel/Gold Deposit (무전해 Ni/Au 도금에서의 BGA Solderability 특성 개선에 관한 연구)

  • 민재상;황영호;조일제
    • Journal of the Microelectronics and Packaging Society
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    • v.8 no.3
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    • pp.55-62
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    • 2001
  • With a spread of BGA, CSP and fine pitch devices, the need of flatter surface finish in bare board is becoming more critical in solderability. The electroless Ni/Au plating has a solution of these needs and also has being spread to apply to surface finish for bare board in many electronic goods. But, the electroless Ni/Au plating had several issues such as Ni oxidation and phosphorous contents. Before this study, we studied on the effect of BGA solderability in electroless Ni/Au plating and chose some major factors such as the oxidation property of NiP plating and warpage of board. Firstly, we made test board with various plating conditions and improved the plating property through the improvement of NiP oxidation reducing P content. Also, we minimized the warpage of board with the improvement of inner layer structure and the analysis of warpage. For the evaluation of solderability, we analyzed the warpage of board and the plating property after mounting BGA on the board with optimizing conditions. The solder joint of BGA is investigated by SEM(Scanning Electronic Microscope) and OM(Optical Microscope). The composition of joint is used by EDS(Energy Dispersive Spectroscopy). We analyzed the fracture strength and mode by ball shear teser.

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Rolling Contact Fatigue and Residual Stress Properties of SAE52100 Steel by Ultrasonic Nano-Crystalline Surface Modification (UNSM) (초음파 나노표면 개질처리를 통한 베어링강의 회전접촉피로 및 잔류응력 특성에 대한 연구)

  • Lee, Changsoon;Park, Ingyu;Cho, Insik;Hong, Junghwa;Jhee, Taegu;Pyoun, Youngsik
    • Journal of the Korean Society for Heat Treatment
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    • v.21 no.1
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    • pp.10-19
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    • 2008
  • To investigate the effect of ultrasonic nano-crystalline surface modification (UNSM) treatment on rolling contact fatigue and residual stress properties of bearing steels, this paper carried out a rolling contact fatigue test, measured residual stress and retained austenite, performed a wear test, observed microstructure, measured micro hardness, and analyzed surface topology. After the UNSM treatment, it was found that the surface became minute by over $100{\mu}m$. The micro surface hardness was changed from Hv730~740 of base material to Hv850~880 with about 20% improvement, and hardening depth was about 1.3 mm. The compressive residual stress was measured as high as -700~-900 MPa, and the quantity of retained austenite was reduced to 27% from 34%. The polymet RCF-6 ball type rolling contact fatigue test showed over 4 times longer fatigue lifetime after the UNSM treatment under 551 kgf load and 8,000 rpm. In addition, this paper observed the samples, which went through the rolling contact fatigue test, with OM and SEM, and it was found that the samples had a spalling phenomenon (the race way is decentralized) after the UNSM treatment. However, before the treatment, the samples had excessive spalling and complete exploration. Comparison of the test samples before and after the UNSM treatment showed a big difference in the fatigue lifetime, which seems to result from the complicated effects of micro particles, compressive residual stress, retained austenite, and surface topology.

Investigation of Structural Change of DLC Coating during Frictional Wear by Raman Spectroscopy (라만 분광법을 활용한 마모 중 DLC 코팅의 구조적 변화 조사)

  • Kim, Song-Hee;Jang, Jae Cheol
    • Journal of the Korean institute of surface engineering
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    • v.52 no.1
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    • pp.16-22
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    • 2019
  • The structural change of DLC coatings during long-term wear test and dicing test under the low loading condition was investigated. DLC coatings were applied for the precision injection molds of a modified SNCM steel for the extension of life and the micro-diamond blades for the high cutting efficiency and the increase in life. A ball-on-disc wear tests in the mold steel and a dicing tests in the micro-diamond blades were conducted to understand degradation of DLC coatings. The degradation of DLC coatings for the injection mold steel and the micro-diamond blades during the wear and dicing tests were studied with Raman Spectroscopy. Raman peaks were divided two bands(D band and G band) to study the degradation process of DLC structure. By the wear test, polished condition of wear marks were observed to be maintained until 10 hrs of wear test period is given, but small striation marks appeared in 20 hours wear test. It was observed that $I_D/I_G$ ratios changed as the degradation of DLC coatings is proceeded during the wear tests and the dicing tests. It is suggested that the change in $I_D/I_G$ value possibly reflected from the composition of $sp^2$ and $sp^3$ bondings in DLC layers relevant to the change in mechanical and physical property.

STUDIES ON THE UTILIZATION OF ANTARCTIC KRILL 2. Processing of Paste Food, Protein Concentrate, Seasoned Dried Product, Powdered Seasoning, Meat Ball, and Snack (남대양산 크릴의 이용에 관한 연구)

  • PARK Yeung-Ho;LEE Eung-Ho;LEE Kang-Ho;PYEUN Jae-Hyeung;KIM Se-Kweun;KIM Dong-Soo
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.13 no.2
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    • pp.65-80
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    • 1980
  • Processing conditions of the krill products such as paste food, krill protein concentrate, seasoned dried krill, powdered seasoning, meat ball, and snack have been examined and the quality was evaluated chemically and organoleptically. In the processing of paste food, krill juice was yielded $71\%$ and krill scrap $29\%$. The yields of paste and broth from the krill juice showed $53\%$ and $43\%$, respectively. In amino acid composition of the krill paste, proline, glutamic acid, aspartic acid, lysine, and leucine were abundant, while histidine, methionine, tyrosine, serine and threonine were poor. The optimum condition for solvent extraction in the processing of krill protein concentrate was the 5 times repetitive extraction using isopropyl alcohol at $80^{\circ}C$ for 5 mins. The yield of krill protein concentrate when used fresh frozen materials was $10.2\%$ in isopropyl alcohol solvent and $8.8\% in ethyl alcohol, and when used preboiled frozen materials, the yield was $13.0\%$ in isopropyl alcohol and $11.8\%$ in ethyl alcohol. Amino acid composition of krill protein concentrate showed a resemblance to that of fresh frozen krill meat. In quality comparison of the seasoned dried krill, hot air dried krill was excellent as raw materials and sun dried krill was slightly inferior to hot air dried krill, but preboiled frozen krill showed the poorest quality. The result of quality evaluation for seasoning made by combination of dried powdered krill, parched powdered sesame, salt, powdered beef extract, monosodium glutamate, powdered red pepper and ground pepper showed that the hot air dried krill was good in color and sundried krill was favorable in flavor. When krill meat ball was prepared using wheat flour, monosodium glutamate and salt as side materials, the quality of the products added up to $52\%$ of krill meat was good and the difference in quality upon the results of the organoleptic test for raw materials was not recognizable between fresh frozen and preboiled frozen krill. In the experiment for determining the proper amount of materials such as dried Powdered krill, $\alpha-starch$, sweet potato starch, sugar, salt, monosodium glutamate, glycine, potassium tartarate, ammonium bicarbonate, and sodium bicarbonate in processing krill snack, sample B(containing $7.7\%$ of dried powdered krill) and sampleC (containing $10.8\%$ of dried powdered krill) showed the most palatable taste from the view point of organoleptic test. Sweet potato starch in testing side materials was good in the comparison of suitability for processing krill snack. Corn starch and kudzu starch were slightly inferior to sweet potato starch, while wheat flour was not proper for processing the snack. In the experiment on frying method, oil frying showed better effect than salt frying and the suitable range of frying temperature was $210-215^{\circ}C$.

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