• 제목/요약/키워드: Ball-Milling Method

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Water Splitting Capacity Improvement of Mn-Fe Oxide Prepared by Ball Milling with $ZrO_2$

  • Kang, Kyoung-Soo;Cho, Mi-Sun;Kim, Chang-Hee;Park, Chu-Sik
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1122-1123
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    • 2006
  • Mn-Fe oxide and Mn-Fe oxide/$ZrO_2$(50wt%/50wt%) were prepared by ball milling method. XRD data of the prepared samples revealed that hematite and ferrite phase coexisted. Water splitting at 1273K, after thermal reduction at 1573K, was performed 4 times for the samples. Hydrogen production amount was analyzed by GC with TCD detector. Water splitting capacity of Mn-Fe oxide was improved by ball milling with $ZrO_2$.

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볼엔드밀 절삭에서 전해복합에 의한 절삭력 저감 특성 (Cutting Force Reduction Characteristics by Compounding Electrolytic Machining in Ball End Milling)

  • 이영표;박규열
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 2000년도 추계학술대회논문집 - 한국공작기계학회
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    • pp.268-273
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    • 2000
  • In this report, a new method compounding the electrolytic machining with ball end milling process to increase the machining efficiency was introduced. And the cutting characteristics by electrolytic machining conditions was examined. From the experimental results, it was confirm-ed that effect of cutting force reduction obtained at the condition of transpassive state of electrolytic machining conditions.

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나노-마이크로 크기 하이브리드 구조 텅스텐 분말특성에 미치는 분말혼합 공정의 영향 (Effect of Powder Mixing Process on the Characteristics of Hybrid Structure Tungsten Powders with Nano-Micro Size)

  • 권나연;정영근;오승탁
    • 한국분말재료학회지
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    • 제24권5호
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    • pp.384-388
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    • 2017
  • The effect of the mixing method on the characteristics of hybrid-structure W powder with nano and micro sizes is investigated. Fine $WO_3$ powders with sizes of ${\sim}0.6{\mu}m$, prepared by ball milling for 10 h, are mixed with pure W powder with sizes of $12{\mu}m$ by various mixing process. In the case of simple mixing with ball-milled $WO_3$ and micro sized W powders, $WO_3$ particles are locally present in the form of agglomerates in the surface of large W powders, but in the case of ball milling, a relatively uniform distribution of $WO_3$ particles is exhibited. The microstructural observation reveals that the ball milled $WO_3$ powder, heat-treated at $750^{\circ}C$ for 1 h in a hydrogen atmosphere, is fine W particles of ~200 nm or less. The powder mixture prepared by simple mixing and hydrogen reduction exhibits the formation of coarse W particles with agglomeration of the micro sized W powder on the surface. Conversely, in the powder mixture fabricated by ball milling and hydrogen reduction, a uniform distribution of fine W particles forming nano-micro sized hybrid structure is observed.

노우즈반경에 따른 엔드밀의 가공특성 및 절삭시간의 비교 (Comparison of precision Machinabilities and Cutting Time in Inclined Milling Process)

  • 김병희;최영석;주종남
    • 대한기계학회논문집
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    • 제19권9호
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    • pp.2114-2121
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    • 1995
  • Surface generation model of three types of endmills is introduced to analyse the cutting mechanism of an endmill more accurately. Superposition method is introduced to define the effective cusp including the effects of cutter mark. Through the comparison of three endmills, it is shown that the ball-nose endmill is superior to the ball endmill and the flat endmill for inclined milling process in 3-or 5-axis machining modes. By using the objective function minimizing the machining time, appropriate nose radius is selected for various cutter radiuses and cutter inclination angles.

고에너지 볼 밀에 의한 LaAlO3 세라믹스의 제조와 특성 (Preparation and Characterization of LaAlO3 Ceramics from High Energy Ball Milling Powders)

  • 최상수;서병준;여기호;정수태
    • 한국전기전자재료학회논문지
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    • 제17권1호
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    • pp.39-45
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    • 2004
  • Fine LaAlO$_3$ powders wore successfully synthesized from La$_2$O$_3$ and ${\gamma}$ $Al_2$O$_3$ powders milling for 10∼50 hours via the high energy milling technique (mechanochemical method) in room temperature and air. The particle size of LaAlO$_3$ powder were estimated from XRD patterns and SEM images to be 160∼180 nm. The LaAlO$_3$ ceramics arc derived for the synthesized powders (milling for 10, 30 and 50 hours) by sintering at 140$0^{\circ}C$ and 150$0^{\circ}C$. The micrographs of grains showed an agglomeration and the degree of agglomeration increased with the milling time. The LaAlO$_3$ made from synthesized powders milling for 50 hours can be sintered to 99.5% of theoretical density at 150$0^{\circ}C$ for 1 hour. These ceramics exhibits a dielectric constant of 20, a dielectric loss of 0.0003 and a temperature coefficient of capacitance of 15 ppm/$^{\circ}C$ at 1 MHz.

분말야금법을 이용한 Bi-materials의 제조 (Preparation of Bi-materials by Powder Metallurgy Method)

  • 이인규;이광식;장시영
    • 한국분말재료학회지
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    • 제11권6호
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    • pp.462-466
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    • 2004
  • The bi-materials composed of $Al-5wt{\%}Mg$ and its composite reinforced with SiC particles were prepared by ball-milling and subsequent sintering process. The size of powder in Al-Mg/SiCp mixture decreased with increasing ball-milling time, it was saturated above 30 h when the ball and powder was in the ratio of 30 to 1. Both $Al-5wt{\%}Mg$ powders mixture and $Al-5wt{\%}Mg/SiCp$ mixture were compacted under a pressure of 350MPa and were bonded by sintering at temperatures ranging from 873K to 1173K for 1-5h. At 873k, the sound bi-mate-rials could not be obtained. In contrast, the bi-materials with the macroscopically well-bonded interface were obtained at higher temperatures than 873K. The length of well-bonded interface became longer with increasing temperature and time, indicating the improved contact in the interface between unreinforced Al-Mg part and Al-Mg/SiCp composite part. The relative density in the bi-materials increased as the sintering temperature and time increased, and the bi-materials sintered at 1173K for 5h showed the highest density.

보헤마이트 졸겔법에 의한 알루미나 세라믹스의 저온소결 I. 상전이 및 소결거동 (Low Temperature Sintering of Alumina by Boehmite Sol-Gel Method I. Phase Transformation and Sintering Behavior)

  • 이형민;이홍림
    • 한국세라믹학회지
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    • 제34권11호
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    • pp.1187-1197
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    • 1997
  • Dry gel composed of primary particles more homogeneous than starting boehmite powder was prepared by dispersing and gelling the boehmite powder. The transformation temperatures of boehmite powder, dry gel seeded with 0, 1, 3, 5 wt% $\alpha$-Al2O3, and ball milled gel were 1192$^{\circ}C$, 1184$^{\circ}C$, 1141$^{\circ}C$, 1119$^{\circ}C$, 1117$^{\circ}C$, and 1106$^{\circ}C$, respectively. Sintering behavior of dry gel without seed was similar to that of boehmite powder, but the sintered density of dry gel was improved as much as 10%~15% than boehmite powder. In the case of dry gel seeded with 5 wt% $\alpha$-Al2O3, sintering behavior was much improved. The relative density of the gel seeded with 5 wt% $\alpha$-Al2O3 was 96% when sintered at 140$0^{\circ}C$ for 1h. On the other hand, ball milling of the non-seeded sol for 48h resulted in the relative density of 97% when sintered at 130$0^{\circ}C$ for 1h. The size and amount of $\alpha$-Al2O3 particles added by ball milling were 0.107 ${\mu}{\textrm}{m}$ and 0.5 wt%.

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밀링작업에서 보조장치를 이용한 자유곡면의 표면거칠기 향상에 관한 연구 (A Study on the Improvement of Sculptured surface Sopography in Milling Operation by Using Tertiary Motion Attachment)

  • 홍민성
    • 한국생산제조학회지
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    • 제5권3호
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    • pp.66-72
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    • 1996
  • The applicability of a new method, termed the whirling motion concept, for the improvement of the surface finish in milling three-dimensional sculptured surfaces has been investigated. A method for implementing this concept o conventional NC machines that utilize a suitably configured attachment has been proposed. The tool path equation for the ball-end milling process, based on the surface-shaping system, has been obtained. Both results of the computer simulation and the experiment verified the proposed approach.

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밀링작업에서 보조장치를 이용한 자유곡면의 표면거칠기 향상에 관한 연구 (A Study on the Improvement of Sculptured Surface Topography in Milling Operation by using tertiary Motion Attachment)

  • 홍민성
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 1996년도 춘계학술대회 논문집
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    • pp.149-154
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    • 1996
  • The applicability of a new method, termed the whirling motion concept, for the iprovement of the surface finish in milling three-dimensional sculptured surfaces has been investigated. A method for implementing this concept on conventional NC machines that utilize a suitably configured attachment has been proposed. The tool path equation for the ball-end milling process, based on the Surface-Shaping system, has been obtained. Both results of the computer simulation and the experiment verified the computer simulation and the experiment verified the proposed approach.

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