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Mechanical Properties and Microstructure of the Leucite-Reinforced Glass-Ceramics for Dental CAD/CAM

  • Byeon, Seon-Mi;Song, Jae-Joo
    • Journal of dental hygiene science
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    • v.18 no.1
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    • pp.42-49
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    • 2018
  • The computer-aided design/computer-aided manufacturing (CAD/CAM) system was introduced to shorten the production time of all-ceramic restorations and the number of patient visits. Among these types of ceramic for dental CAD/CAM, they have been processed into inlay, onlay, and crown shapes using leucite-reinforced glass-ceramics to improve strength. The purpose of this study was to observe the mechanical properties and microstructure of leucite-reinforced glass-ceramics for dental CAD/CAM. Two types of leucite-reinforced glass-ceramic blocks (IPS Empress CAD, Rosetta BM) were prepared with diameter of 13 mm and thickness of 1 mm. Biaxial flexural testing was conducted using a piston-on-three-ball method at a crosshead speed of 0.5 mm/min. Weibull statistics were used for the analysis of biaxial flexural strength. Fracture toughness was obtained using an indentation fracture method. Specimens were observed by field emission scanning electron microscopy to examine the microstructure of the leucite crystalline phase after acid etching with 0.5% hydrofluoric acid aqueous solution for 1 minute. The results of strength testing showed that IPS Empress CAD had a mean value of $158.1{\pm}8.6MPa$ and Rosetta BM of $172.3{\pm}8.3MPa$. The fracture toughness results showed that IPS Empress CAD had a mean value of $1.28{\pm}0.19MPa{\cdot}m^{1/2}$ and Rosetta BM of $1.38{\pm}0.12MPa{\cdot}m^{1/2}$. The Rosetta BM sample exhibited higher strength and fracture toughness. Moreover, the crystalline phase size and ratio were increased in the Rosetta BM sample. The above results are expected to elucidate the basic mechanical properties and crystal structure characteristics of IPS Empress CAD and Rosetta BM. Additionally, they will help develop leucite-reinforced glass-ceramic materials for CAD/CAM.

The Effect of Abnormal Intermetallic Compounds Growth at Component on Board Level Mechanical Reliability (컴포넌트에서의 비정상적인 금속간화합물 성장이 보드 레벨 기계적 신뢰성에 미치는 영향)

  • Choi, Jae-Hoon;Ham, Hyon-Jeong;Hwang, Jae-Seon;Kim, Yong-Hyun;Lee, Dong-Chun;Moon, Jeom-Ju
    • Journal of the Microelectronics and Packaging Society
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    • v.15 no.2
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    • pp.47-54
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    • 2008
  • In this paper, we studied how and why did abnormal IMC growth at component affect on board level mechanical reliability. First, interfacial reactions between Sn2.5Ag0.5Cu solder and electrolytic Ni/Au UBM of component side were investigated with reflow times and thermal aging time. Also, to compare mechanical reliability of component level, shear energy was evaluated using the ball shear test conducted with variation of shear tip speed. Finally, to evaluate mechanical reliability of board level, we surface-mounted component fabricated with each condition on PCB side. After conducting of 3 point bending test and impact test, we confirmed solder joint crack mode using cross-sectioning and dye & pry penetration method.

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Development and Performance Test of a Spherical Reaction Wheel Actuator with Magnetic Levitation (자기부상을 적용한 구체 반작용휠 구동기 개발 및 성능 시험)

  • Kim, Dae-Kwan;Yoon, Hyung-Joo;Kim, Yong-Bok;Kang, Woo-Yong;Choi, Hong-Taek
    • Journal of Advanced Navigation Technology
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    • v.16 no.5
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    • pp.731-737
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    • 2012
  • In the present study, a feasibility study on an innovative satellite attitude control actuator is performed. The actuator is specially designed to generate the reaction torque in an arbitrary axis, so that a satellite attitude can be controlled by using itself. It consists of a spherical flywheel and electromagnets for levitation and rotation control of the ball. As the earlier study, a rotating performance test on the spherical actuator is conducted in a single rotating axis and vertical levitation condition. From the test results, it can be confirmed that the maximum speed and torque of the innovative device are 7,200rpm and 0.7Nm, respectively. Using a velocity-voltage characteristic curve of the spherical motor, an open-loop control (V/f constant control) is performed, and the test results show excellent control performance in acceleration and deceleration phases.

Unsteady Flow with Cavitation in Viscoelastic Pipes

  • Soares, Alexandre K.;Covas, Didia I.C.;Ramos, Helena M.;Reis, Luisa Fernanda R.
    • International Journal of Fluid Machinery and Systems
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    • v.2 no.4
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    • pp.269-277
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    • 2009
  • The current paper focuses on the analysis of transient cavitating flow in pressurised polyethylene pipes, which are characterized by viscoelastic rheological behaviour. A hydraulic transient solver that describes fluid transients in plastic pipes has been developed. This solver incorporates the description of dynamic effects related to the energy dissipation (unsteady friction), the rheological mechanical behaviour of the viscoelastic pipe and the cavitating pipe flow. The Discrete Vapour Cavity Model (DVCM) and the Discrete Gas Cavity Model (DGCM) have been used to describe transient cavitating flow. Such models assume that discrete air cavities are formed in fixed sections of the pipeline and consider a constant wave speed in pipe reaches between these cavities. The cavity dimension (and pressure) is allowed to grow and collapse according to the mass conservation principle. An extensive experimental programme has been carried out in an experimental set-up composed of high-density polyethylene (HDPE) pipes, assembled at Instituto Superior T$\acute{e}$cnico of Lisbon, Portugal. The experimental facility is composed of a single pipeline with a total length of 203 m and inner diameter of 44 mm. The creep function of HDPE pipes was determined by using an inverse model based on transient pressure data collected during experimental runs without cavitating flow. Transient tests were carried out by the fast closure of the ball valves located at downstream end of the pipeline for the non-cavitating flow and at upstream for the cavitating flow. Once the rheological behaviour of HDPE pipes were known, computational simulations have been run in order to describe the hydraulic behaviour of the system for the cavitating pipe flow. The calibrated transient solver is capable of accurately describing the attenuation, dispersion and shape of observed transient pressures. The effects related to the viscoelasticity of HDPE pipes and to the occurrence of vapour pressures during the transient event are discussed.

Effect of Lubricant with Nanodiamond Particles in Sliding Friction

  • Adzaman, M.H.;Rahman, A.;Lee, Y.Z.;Kim, S.S.
    • Tribology and Lubricants
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    • v.31 no.4
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    • pp.183-188
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    • 2015
  • This paper presents the experimental effects of lubricant with nanodiamond particles in sliding friction. In order to improve the performance of lubricants many additives are used, such as MoS2, cadmium chloride, indium, sulfides, and phosphides. These additives are harmful to human health and to the environment, so alternatives are necessary. One such alternative is nanodiamond powder, which has a large surface area. In order to investigate the effect of nanodiamonds in lubricants under sliding friction, they are dispersed in the lubricant at a variety of concentrations (0 wt%, 0.1 wt%, 0.3 wt%, 0.5 wt%, and 1 wt%) using the matrix synthesis method. Friction and wear tests are performed according to the ASTM G99 method using a pin-on-disc tester at room temperature. The specimens used in this experiment are AISI 52100 ball bearings and AISI 1020 steel discs. During the test, lubricant mixed with nanodiamond is supplied constantly to keep the two bodies separated by a lubricant film. To maintain boundary lubrication, the speed is set to 0.18 m/s and a load of 294 N is applied to the disc through the pin. Results are recorded by using workbench software over the test duration of 10 minutes. Experimental results show that when the concentration of nanodiamond increases, the coefficient of friction decreases. However, above a nanodiamond concentration of 0.5 wt%, both the coefficient of friction and wear volume increase. From this experiment, the optimum concentration of nanodiamond showing a minimum coefficient of friction of 0.09 and minimum wear volume of 0.82 nm2 was 0.5 wt%.

Milling Behaviors of Al-B4C Composite Powders Fabricated by Mechanical Milling Process (기계적 밀링 공정에 의해 제조된 Al-B4C 복합분말의 밀링 거동 연구)

  • Hong, Sung-Mo;Park, Jin-Ju;Park, Eun-Kwang;Lee, Min-Ku;Rhee, Chang-Kyu;Kim, Ju-Myoung;Lee, Jin-Kyu
    • Journal of Powder Materials
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    • v.19 no.4
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    • pp.291-296
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    • 2012
  • In the present work, Al-$B_4C$ composite powders were fabricated using a mechanical milling process and its milling behaviors and mechanical properties as functions of $B_4C$ sizes ( $100{\mu}m$, 500 nm and 50 nm) and concentrations (1, 3 and 10 wt.%) were investigated. For achieving it, composite powders and their compacts were fabricated using a planetary ball mill machine and magnetic pulse compaction technology. Al-$B_4C$ composite powders represent the most uniform dispersion at a milling speed of 200 rpm and a milling time of 240 minutes. Also, the smaller $B_4C$ particles were presented, the more excellent compositing characteristics are exhibited. In particular, in the case of the 50 nm $B_4C$ added compact, it showed the highest values of compaction density and hardness compared with the conditions of $100{\mu}m$ and 500 nm additions, leading to the enhancement its mechanical properties.

Preparation of Calcium Powder from Eggshell and Use of Organic Acids for Enhancement of Calcium Ionization (난각칼슘의 제조 조건 및 유기산이 칼슘의 이온화에 미치는 영향)

  • Shin, Hyung-Soon;Kim, Kong-Hwan
    • Applied Biological Chemistry
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    • v.40 no.6
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    • pp.531-535
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    • 1997
  • An efficient process for recovery of calcium from the eggshell was developed and some organic acids were used in an attempt to enhance the degree of calcium ionization. Eggshell membrane was readily separated from crushed eggshell based on the differences in specific gravities. The conditions which allowed most efficient membrane removal were found to be 30 rpm of speed, 30 min of residence time and 0.08 of volume fraction. It took 3 hours for the eggshell powder prepared at $1000^{\circ}C$ to reach L value of 90 with the Hausner ratio being 1.43. The calcium ion concentrations were 990, 3500, 3900 and 4200 ppm in pure water, acetic acid, citric acid and lactic acid$(0.05{\sim}3%)$ aqueous solution, respectively. The degrees of ionization of calcium-citrate-malate complex(CCM), calcium-citric acid complex(CC) and calcium malic acid complex(CM) increased by 4 to 5 times compared to eggshell calcium powder.

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Thermoelectric Properties of Mg3-xZnxSb2 Fabricated by Mechanical Alloying (기계적 합금법으로 제조한 Mg3-xZnxSb2의 열전물성)

  • Kim, In-Ki;Jang, Kyung-Wook;Kim, Il-Ho
    • Korean Journal of Materials Research
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    • v.23 no.2
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    • pp.98-103
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    • 2013
  • $Mg_{3-x}Zn_xSb_2$ powders with x = 0-1.2 were fabricated by mechanical alloying in a planetary ball mill with a speed of 350 rpm for 24 hrs and then hot pressed under a pressure of 70 MPa at 773 K for 2 hrs. It was found that there were systematic shifts in the X-ray diffraction peaks of $Mg_3Sb_2$ (x = 0) toward a higher angle with increasing Zn for both the powder and the bulk sample and finally the phase of $Mg_{1.86}Zn_{1.14}Sb_2$ was formed at the Zn content of x = 1.2. The $Mg_{3-x}Zn_xSb_2$ compounds had nano-sized grains of 21-30 nm for the powder and 28-66 nm for the hot pressed specimens. The electrical conductivity of hot pressed $Mg_{3-x}Zn_xSb_2$ increased with increasing Zn content and temperature from 33 $Sm^{-1}$ for x = 0 to 13,026 $Sm^{-1}$ for x = 1.2 at 323 K. The samples for all the compositions from x = 0 to x = 1.2 had positive Seebeck coefficients, which decreased with increasing Zn content and temperature, which resulted from the increased charge carrier concentration. Most of the samples had relatively low thermal conductivities comparable to the high performance thermoelectric materials. The dimensionless figure of merit of $Mg_{3-x}Zn_xSb_2$ was directly proportional to the Zn content except for the compound with Zn = 1.2 at high temperature. The $Mg_{3-x}Zn_xSb_2$ compound with Zn = 0.8 had the largest value of ZT, 0.33 at 723 K.

${\mu}$BGA and ${\mu}$Spring Packages for Rambus DRAM Applications and Their Electrical Characteristics (Rambus DRAM실장용 ${mu}!$BGA (Ball Grid Array) 및 ${mu}!$Spring 패키지와 전기적 특성)

  • Kim, Jin-Seong;Yu, Yeong-Gap
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.38 no.4
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    • pp.243-250
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    • 2001
  • This paper presents the structure of a $\mu$Spring package, its fabrication process and an analysis of its electrical characteristics compared to that of a $\mu$BGA. It was found that both $\mu$BGA and $\mu$Spring packages provide with outstanding high speed signal transmission characteristics due to their lower inductance of package interconnection lines, smaller than half of inductance of TSOP package lines. Even the worst case substrate trace of a Rambus DRAM $\mu$Spring package yields the line inductance of 2.9nH, which provides with 25% margin compared to the Rambus DRAM specification of 4nH. The fabrication cost of $\mu$Spring package is lower than that of $\mu$BGA by 50%, passes 1000 thermal cycles, meets JEDEC Level 1 specification whereas $\mu$BGA does not, and thereby yields high reliability and strong competing power.

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A Comparative Study on the Putting Green Management for Tournament of Korean and Foreign Golf Courses during Tournament Play Week (공식 골프대회 기간중 한국과 외국의 골프코스들의 퍼팅그린 관리 방법 비교)

  • 장유비;이호순;심경구
    • Journal of the Korean Institute of Landscape Architecture
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    • v.31 no.3
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    • pp.91-106
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    • 2003
  • The objective of this study is to present management methods for Korean golf courses to achieve fast green that satisfies international golf tournament standards during an official golf tournament. The results of both the research and the comparative study on putting green management of 24 tournaments hosted in Korea and 12 tournaments hosted in overseas countries in 2002 are as follows: 1. As for the putting greens in Korean and foreign golf courses where official golf tournaments were held, Korean of official golf tournaments were mainly opened in two-green system golf courses contrary to the foreign cases, and the average size of the greens in Korean golf courses was shown to be greater than that of foreign golf courses to some extent, although there was no difference between the types of turf varieties. 2. Results have shown that unlike foreign golf courses, Korean golf courses were managing putting greens by using greens mowers mostly for general (non-tournament) management, and elaborate rolling attempts failed during official tournament flay week because of an insufficient number of rollers to be input. Therefore, Korean golf courses are required to make efforts to secure 21-inch working-behind greens mowers equipped with tournament bedknifes and 11 blades, which is the greens mowing equipment for professional tournaments, and rollers above all things in order to achieve fast green during tournament play week 3. In attempting to achieve green as fast as that of foreign golf courses, Korean golf courses need to consider the method of performing mowing at 3.0mm height or less with greens mowers for professional tournaments. This needs to be done more than two times, followed by a continuous practice of rolling for proper management.