• Title/Summary/Keyword: B13

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The 1H and 13C NMR Data of 19 Methoxyflavonol Derivatives

  • Park, Young-Hee;Moon, Byoung-Ho;Lee, Eun-Jung;Hong, Sun-Hee;Lee, Sun-Hee;Lim, Yoong-Ho
    • Bulletin of the Korean Chemical Society
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    • v.29 no.1
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    • pp.81-84
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    • 2008
  • In the present study, we report 1H and 13C NMR data of 19 methoxyflavonol derivatives with different substitution patterns on A- and B-ring. In addition, the influence of the methoxy substituents in A- and B-ring on the 1H and 13C NMR chemical shifts is discussed: the 1H and 13C chemical shifts of and the number of methoxyl groups provided information allowing elimination of many structural isomers from consideration and in certain instances greatly simplified structural elucidation.

Isolation and Structure of $[Ph_3P(OH)]^+[ $N_3$]^-$ ($[Ph_3P(OH)]^+[ $N_3$^-$의 분리 및 구조)

  • Beom Jun Lee;Won Seok Han;Soon Won Lee
    • Korean Journal of Crystallography
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    • v.12 no.3
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    • pp.141-144
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    • 2001
  • From the reaction of Na[Ga(N₃)₄] with PPh₃, an ionic compound [Ph₃P(OH)]/sup +/[N₃]/sup -/ (1) was isolated. Compound 1 was characterized by spectroscopy (¹H-NMR, /sup 13C{¹H}-NMR, and IR) and X-ray diffraction. Crystallographic data for 1 : orthorhombic space group P2₁2₁2₁, a = 10.491 (4) Å, b=11.603(5)Å, c=13.149(5)Å, Z=4, R(wR₂)=0.0547(0.0978).

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Isolation and characterization of two unrecorded yeast species in the phylum Basidiomycota

  • Jieun Seok;Jaewoo Bai;Sathiyaraj Srinivasan
    • Journal of Species Research
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    • v.13 no.1
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    • pp.105-110
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    • 2024
  • The purpose of this study was to isolate and identify wild yeasts from soil samples collected in Seoul and Daejeon, Republic of Korea. To identify wild yeast strains, pairwise sequence comparisons of D1/D2 region of the 26S rRNA gene sequence were done using Basic Local Alignment Search Tool (BLAST). The cell morphologies were observed by phase contrast microscope and carbon source assimilation test were done using API 20C AUX kit. Among the 13 isolated strains, 11 strains were previously reported, but two strains have never been reported from Republic of Korea. The 13 strains were assigned to the phylum Basidiomycota. The two unrecorded yeast strains B2UV-201 and DJ1-5-B-10C belong to the genera Rhodotorula and Rhodosporidiobolus, respectively. The two unrecorded yeast strains are oval shaped and polar budding cells. This research focuses on the morphological and biochemical properties of the two unreported yeast species that have not officially been reported in Korea.

The effect of a static magnetic field of Nd-Fe-B magnet on alkaline phosphatase activity of MC3T3-E1 cells (Nd-Fe-B 자석의 정자기장이 MC3T3-E1 세포의 alkaline phosphatase 활성도에 미치는 영향)

  • Kim, Sook-Hee;Kwon, Oh-Won;Ryoo, Hyun-Mo
    • The korean journal of orthodontics
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    • v.30 no.2 s.79
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    • pp.205-214
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    • 2000
  • Recently, the magnetic force has been considered as a method for a more efficient tooth movement. The purpose of this study was to evaluate the effects of different static magnetic fields of Nd-Fe-B magnet on MC3T3-E1 cells by measuring the alkaline phosphatase activity and observing the amount of stained alkaline phosphatase. For measuring of alkaline phosphatase activity, MC3T3-E1 cells were seeded in first and third row of 12 well culture plates. And Nd-Fe-B magnets were positioned under the first column of first and third row to apply different static magnetic fields(first column:100mT ; second column:4.6mT ; third column:0.5mT ; forth column:0.0mT) to the cells for 7, 13, 19, and 25 days. For staining of alkaline phosphatase, MC3T3-E1 cells were seeded in 100mm culture plates. And Nd-Fe-B magnets were positioned under the corner of plates to apply different static magnetic fields(magnet side:100mT : the opposite side:0.5mT) to the cells for 7, 13, 19, and 25 days. The results were as follows : 1. ALP activity was increased until day 19 in biochemical determination as well as in histochemical staining, 2. The application of higher magnetic field(100mT) suppressed ALP activity at day 13, 19, 25. On the contrary, the application of the lower magnetic field(4.6mT, 0.5mT) significantly enhanced the ALP activity. 3. Consistent with enzyme assay, histochemical staining of ALP also demonstrated that higher magnetic field(100mT) suppressed ALP activity, lower one(0.5mT) enhanced.

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Soyasapogenols B and E from melilotus afficinalis

  • Ksng, Sam-Sik;Lim, Chae-Hyun;Lee, Sook-Yeon
    • Archives of Pharmacal Research
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    • v.10 no.1
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    • pp.9-13
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    • 1987
  • From the aerial parts of Melilotus officinalis (Leguminosae) soyasapogenols B, mp 259-260.deg., and E, mp 246-247, were isolated along with coumarin and kaempferol. This is the first report of the isolation of soyasapogenols from the genus Meliotus.

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B-ISDN과 ATM

  • 김재근;최준균
    • 전기의세계
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    • v.44 no.12
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    • pp.13-20
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    • 1995
  • 본 고에서는 ATM(Asynchronous Transfer Mode)기반으로 개발되고 있는 광대역 종합정보통신망(B-ISDN: Broadband Integrated Services Digital Network)의 구조 및 이를 기반으로 제공할 수 있는 광대역 서비스의 형태에 대해 기술한다. 또한 B-ISDN의 기술적 목표가 되는 ATM 기술과 관련된 최근의 표준 동향, ATM 통신 장비의 개발 및 서비스 개발 현황에 대하여 살펴본다.

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Hybrid Representations for Enveloping Modeling in Gearing

  • Voznyuk, Roman
    • International Journal of CAD/CAM
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    • v.3 no.1_2
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    • pp.13-17
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    • 2003
  • Hybrid method of representing geometric entities as combination of boundary (B-rep) and functional (F-rep) representations is presented which can be used as a basis of solid modeling kernel. It contains whole functionality of classic B-rep kernel, and also supports enveloping (sweep of solid body). Principles and keysolutions are considered. Example of a real task that comes from gearing is provided.