• Title/Summary/Keyword: Average particle size

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Facile Synthesis of Highly Dispersed Ultra-fine ZrC Powders by Carbothermal Reduction Method Using Nanosized ZrO2 and Nanosized Graphite Powder Mixtures (나노크기의 ZrO2와 Graphite 분말 혼합체의 열탄소환원법에 의한 고분산 초미립 ZrC 분말의 합성)

  • Lee, Wha-Jun;Ryu, Sung-Soo
    • Journal of Powder Materials
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    • v.20 no.2
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    • pp.100-106
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    • 2013
  • Ultra-fine zirconium carbide (ZrC) powder with nano-sized primary particles was synthesized by the carbothermal reduction method by using nano-sized $ZrO_2$ and nano-sized graphite powders mixture. The synthesized ZrC powder was well dispersed after simple milling process. After heat-treatment at $1500^{\circ}C$ for 2 h under vacuum, ultra-fine ZrC powder agglomerates (average size, $4.2{\mu}m$) were facilely obtained with rounded particle shape and particle size of ~200 nm. Ultra-fine ZrC powder with an average particle size of 316 nm was obtained after ball milling process in a planetary mill for 30 minutes from the agglomerated ZrC powder.

Effects of $SiO_2$ Particle-size on Fabrication Properties of LPS-SiC Ceramics (LPS-SiC 세라믹스의 제조특성에 미치는 $SiQ_2$ 입자크기의 영향)

  • Kim, Seong-Hoon;Yoon, Han-Ki;Kim, Bu-An
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2006.11a
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    • pp.162-165
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    • 2006
  • In this study, Liquid Phase Sintered SiC (LPS-SiC) was fabricated by hot pressing method with $\beta$-SiC powder whose a particle size is 30nm and less on the average in argon condition at 1780 and $1800^{\circ}C$ under 20MPa. Alumina ($Al_2O_3$), yttria ($Y_2O_3$) and silica ($SiO_2$) were used for sintering additives. To investigate effects of particle-size and temperature on $SiO_2$, LPS-SiC was fixed $Al_2O_3$, $Y_2O_3$ and then particle-size of $SiO_2$ were changed as two kinds. The system of particle-size and temperature on sintering additives which affects a property of sintering os well os the influence depending on particle-size and temperature of sintering additives were investigated by measurement of sintering properties. Such as measurement of sintering density, vikers hardness and observing of microstructure were investigated to make sure of the optimum condition which is about matrix of $SiC_f/SiC$ composites. Base on the composition of sintering additives, microstructure and sintering property correlation, the effect of particle-size of sintering additives are discussed. An experimental method to investigate the dynamic characteristics of bums in extreme environmental condition is established.

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Effects of feed form and particle size on growth performance, nutrient digestibility, carcass characteristics, and gastric health in growing-finishing pigs

  • Jo, Yun Yeong;Choi, Myung Jae;Chung, Woo Lim;Hong, Jin Su;Lim, Jong Seon;Kim, Yoo Yong
    • Animal Bioscience
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    • v.34 no.6
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    • pp.1061-1069
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    • 2021
  • Objective: This study was conducted to evaluate the effects of feed processing and particle size on growth performance, nutrient digestibility, carcass characteristics, and gastric health in growing-finishing pigs. Methods: A total of 360 growing pigs (22.64±0.014 kg initial body weight [BW]) were allocated to 1 of 6 treatments with 6 replicates by BW and sex, and 10 pigs were housed in one pen in a randomized complete block design. The BW and feed intake were recorded to calculate growth performance. For the digestibility trial, a total of 24 barrows with an initial BW of 33.65±0.372 kg were split into 6 treatments with a completely randomized design. Dietary treatments were designed by a 2×3 factorial arrangement of treatments based on two main factors, particle size (600, 750, 900 ㎛) and feed form (mash and pellet) of diet. Experimental diets were formulated to contain the requirements of the NRC (2012). Results: The BW and average daily gain were not changed by dietary treatments, and the feed intake of finishing pigs (wks 6 to 12) was increased when the pigs were fed a mash diet (p<0.05). For the overall period, the feed efficiency of pigs was improved with the pellet diet (p<0.01) and reduced particle size (p<0.05). The pellet diet had effects on increasing crude fat digestibility (p<0.01) relative to a mash diet, but there was no considerable change in dry matter and crude protein digestibilities by dietary treatments. In the evaluation of gastric health, a trend for an increased incidence of keratinization in the esophageal region was observed as particle size decreased (p = 0.07). Conclusion: Feed efficiency could be improved by pellet diet and reduced particle size. Nutrient digestibility, carcass characteristics, and gastric health were not affected by feed form, and particle size ranged from 600 to 900 ㎛.

Preparation of Nano-Sized Tin Oxide Powder by Spray Pyrolysis Process (분무열분해(噴霧熱分解) 공정(工程)에 의한 주석(朱錫) 산화물(酸化物) 나노 분말(粉末) 제조(製造))

  • Yu, Jae-Keun;Cha, Kwang-Yong;Kim, Myung-Choun;Han, Joung-Su;Jang, Jae-Bum;Lee, Yong-Hwa;Kim, Dong-Hee
    • Resources Recycling
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    • v.17 no.6
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    • pp.79-88
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    • 2008
  • This study is the previous stage for the mass production technology development of the nano-sized tin oxide powder by the recycling of the wasted tin metal, and nano-sized tin oxide powder with the average particle size below 50 nm is prepared from the tin chloride solution by the spray pyrolysis process. As the reaction temperature increases from 800 to 850, the average particle size of the generated powder increases from 20 to 30 nm. As the reaction temperature increases to 900, the droplet type is composed of the particles with the average size of the 30 nm. while the average size of the independent particles increases up to $80{\sim}100$ nm and the surface microstructure becomes more solid. Until $900^{\circ}C$, as the reaction temperature increases, the XRD peak intensity increases, while the specific surface area decreases. When the reaction temperature increases to 950, most of the powder appears with the independent type and the average particle size decrease down to 70 nm. The XRD peak intensity greatly decreases and the specific surface area increases almost twice.

Degradation of TPHs, TCE, PCE, and BTEX Compounds for NAPLs Contaminated Marine Sediments Using In-Situ Air Sparging Combined with Vapor Extraction (증기추출법과 결합된 공기주입법을 이용한 비수용성액체 해양퇴적물의 TPHs, TCE, PCE 및 BTEX 정화)

  • Lee, Jun-Ho;Han, Sun-Hyang;Park, Kap-Song
    • Economic and Environmental Geology
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    • v.46 no.5
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    • pp.425-444
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    • 2013
  • This study was carried out in order to determine the remediation of total petroleum hydrocarbons (TPHs), trichloroethylene (TCE), perchloroethylene (PCE), benzene, toluene, ethylbenzene and xylenes (BTEX) compounds for non-aqueous phase liquids (NAPLs) using in-situ air sparging (IAS) / vapor extraction (VE) with the marine sediments of Mandol, Hajeon, Sangam and Busan, South Korea. Surface sediment of Mandol area had sand characteristics (average particle size, 1.789 ${\Phi}$), and sandy silt characteristics (average particle size, 5.503 ${\Phi}$), respectively. Sangam surface sediment had silt characteristics (average particle size, 5.835 ${\Phi}$). Sediment characteristics before experiment in the Busan area showed clay characteristics (average particle size, 8.528 ${\Phi}$). TPHs level in the B1 column of Mandol, Hajeon, Sangam, and Busan sediments were 2,459, 6,712, 4,348, and 14,279 ppm. B2 (3 L/min) to B5 (5 L/min) columns reduced 99.5% to 100.0% of TCE and 93.2% to 100.0% of PCE. Removal rates of TCE, PCE, and BTEX are closely correlated (0.90-0.99) with particle sizes and organic carbon concentrations. However, TPHs (0.76) and benzene (0.71) showed the poorer but moderate correlations with the same parameters.

Experimental Study and Modelling on Membrane Fouling in Taylor Vortex Flow Microfiltration (테일러 와류 정밀여과에서 막오염의 실험적 연구 및 모델링)

  • 박진용;김현우;최창균
    • Membrane Journal
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    • v.13 no.2
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    • pp.88-100
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    • 2003
  • A change of filtrate flux in Taylor vortex flow filtration was investigated experimentally by rotating speed of inner cellulose ester membrane cylinder (average pore size: 1.2 ${\mu}m$), slurry concentration, and particle size. The filtrate flux was a direct proportion relation with TMP, but an inverse relation with resistances. A change of cake resistance with time was examined by rotating speed, slurry concentration, and particle size. Initial resistance increased dramatically as raising slurry concentration, and the pseudo-steady state was maintained at high resistance value. However, times to reach the pseudo-steady state did not depend on slurry concentration. The resistance was larger as smaller particle size, because possibility of pore blocking inside membrane could be higher and shear effect should be lower as smaller particle size. A model equation suggested in this study was composed of particle deposition and removal terms, and could confirm well experimental data using average values of experimental coefficients.

The Unipolar Charging Characteristics of Submicron Particles by Using an Indirect Photoelectric Charging (간접 광대전에 의한 서브 마이크론 입자의 단극하전 특성)

  • Choi, Young-Joo;Kim, Sang-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.27 no.6
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    • pp.677-684
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    • 2003
  • A new unipolar aerosol charger was developed by using an indirect photoelectric charging. The charger consists of two coaxial tubes, the inner UV lamp wrapped with stainless mesh and the outer Al cylinder. In this study, the effects of flow rate, particle size, and electric field were examined to search the optimal charging conditions with experimental and numerical methods. Monodisperse NaCl particles were fed into an annular space and the particles were charged by negative ions generated from Al plate exposed to the UV light. According to experimental results, the average number of elementary charge on particles increases from 2.5 to 5.5 as particle size increases from 50nm to 130nm at 2.5 L/min and 100V. The average number of elementary charge on particles was maximized at 25V as the electric potential between the stainless mesh and Al plate was varied from 0V to 400V.

Effect of Ambient Air Pressure on the Preparation of Cobalt Oxide Powder with Average Particle Size below 50 nm by Spray Pyrolysis Process (분무열분해 공정에 의한 평균입도 50 nm 이하의 코발트 산화물 분체 제조에 미치는 공기압력의 영향)

  • Kim, Dong Hee;Yu, Jae Keun
    • Resources Recycling
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    • v.26 no.1
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    • pp.22-29
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    • 2017
  • When the ambient air pressure was $0.1kg/cm^2$, there were few spherically formed droplets, which showed very badly fragmented state. The average particle size of the particles constituting the droplet was about 40 nm. When the air pressure increased to $0.5kg/cm^2$, the ratio of the spherical droplet forms increased, but still showed a state of severe disruption. The average particle size of the particles was reduced to about 35 nm. As the air pressure increased to $3kg/cm^2$, the ratio of spherical droplet form significantly increased, the degree of fragmentation even further decreased and the average particle size decreased to 30 nm. When the air pressure increased from 0.1 to $1kg/cm^2$, the XRD peak intensity showed little change, but the specific surface area was decreased. As the air pressure increased to $3kg/cm^2$, the intensity of XRD peaks showed a little decrease, while the specific surface area increased.

Effect of Variation in Particle Size of WC and Co Powder on the Properties of WC-Co Alloys (WC와 Co원료 입자크기 변화에 따른 WC-Co계 초경합금의 특성 변화)

  • Chung, Tai-Joo;Ahn, Sun-Yong;Paek, Yeong-Kyeun
    • Journal of the Korean Ceramic Society
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    • v.42 no.3 s.274
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    • pp.171-177
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    • 2005
  • The effect of variation in particle size of WC and Co powder on the properties of WC-Co alloys was investigated. WC and Co powders having different particle sizes were used in the fabrication of $WC-10\;wt\%$Co composites. High hardness and low fracture toughness alloy was obtained with the decrease in WC particle size regardless of Co particle size. It was newly found in this investigation that the initial particle size of Co as well as WC had a great role in the microstructure and properties of WC-Co hard materials. The average grain size and fracture toughness of WC-Co alloys using same WC powder size increased and their hardness decreased with the use of relatively finer Co binder.

Effects of Particle Size on Properties of PZT -Based Thick Films (입자 크기가 PZT계 압전 후막의 물성에 미치는 영향)

  • 김동명;김정석;천채일
    • Journal of the Korean Ceramic Society
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    • v.41 no.5
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    • pp.375-380
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    • 2004
  • Pb(Ni$\_$1/3/Nb$\_$2/3/)O$_3$-PbZrO$_3$-PbTiO$_3$ thick films were screen-printed on platinized alumina substrates and fired at 800-1000$^{\circ}C$. Two kinds of powders with different particle size were prepared by attrition and ball milling methods. Effects of particle size of starting material on the microstructure and electrical properties of the thick films were investigated. Average particle size of attrition milled-powder (0.44 ${\mu}$m) was much smaller than that of ball milled-powder (2.87 ${\mu}$m). Average grain size of the thick film prepared from attrition-milled powder was smaller than that of the thick film prepared from ball-milled powder at the sintering temperature of 800$^{\circ}C$. However, the difference in average particle size became smaller with increasing the sintering temperature. Thick films prepared from attrition-milled powders showed more uniform and denser microstructures at all firing temperatures. Thick films prepared from attrition-milled powders had better electrical properties at the firing temperature above 900$^{\circ}C$ than thick films prepared from ball-milled powders. Dielectric constant, remanent polarization and coercive field of the thick film prepared from attrition-milled powders and fired at 900$^{\circ}C$ were 559, 16.3 ${\mu}$C/cm$^2$, and 51.3 kV/cm, respectively.