• Title/Summary/Keyword: Atmosphere temperature

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The Electrical Improvement of PZT Thin Films Etched into CF4/(Cl2+Ar) Plasma

  • Koo Seong-Mo;Kim Kyoung-Tae;Kim Chang-Il
    • Transactions on Electrical and Electronic Materials
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    • v.5 no.6
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    • pp.223-226
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    • 2004
  • The PZT thin films are one of well-known materials that has been widely studied for ferroelectric random access memory (FRAM). We etched the PZT thin films by $CF_{4}/(Cl_{2}+Ar)$ plasma and investigated improvement in etching damage by $O_{2}$ annealing. The maximum etch rate of the PZT thin films was 157 nrn/min and that the selectivity of the PZT thin films to Pt was 3.1 when $CF_{4}(30{\%})$ was added to a $Cl_{2}(80{\%})/Ar(20{\%})$ gas mixing ratio. To improve the ferroelectric properties of PZT thin films after etching, the samples were annealed for 10 min at various temperatures in $O_{2}$ atmosphere. After $O_{2}$ annealing, the remanent polarization of the asdeposited films was $34.6{\mu}/cm^{2}$ and the sample annealed at 650, 550, and $450^{\circ}C$ was 32.8, 22.3, and $18.6{\mu}/cm^{2}$, respectively. PZT thin films with $O_{2}$ annealing at $450^{\circ}C$ retained $77{\%}$ of their original polarization at 106 cycles. Also as the annealing temperature increased, the fatigue properties improved. And the leakage current was decreased gradually and almost recovered to the as-deposited value after the annealing at $450^{\circ}C$.

Growth of ZnO Thin films Depending on the Substrates by RF Sputtering and Analysis of Their Microstructures (기판의 결정구조에 따른 RF 스퍼터링 ZnO 박막의 성장과 미세구조 분석)

  • Yoo In-Sung;So Soon-Jin;Park Choon-Bae
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.19 no.5
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    • pp.461-466
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    • 2006
  • To investigate the ZnO thin films which are interested in the next generation of short wavelength LEDs and Lasers, the ZnO thin films were deposited by RF sputtering system. At sputtering process of ZnO thin films, substrate temperature, work pressure respectively is $100^{\circ}C$ and 15 mTorr, and the purity of target is ZnO 5 N. The ZnO thin films were in-situ annealed at $600^{\circ}C$ in $O_2$ atmosphere. The thickness of ZnO thin films has implemented about $1.6{\mu}m$ at SEM analysis after in-situ annealing process. We have investigated the crystal structure of substrates, and so structural properties of ZnO thin films has estimate by using XRD, FWHM, FE-SEM and AFM. XRD and FE-SEM showed that ZnO thin films grown on substrates had a c-axis preferential orientation in the [0001] crystal direction. XPS spectra showed that ZnO thin film was showed a peak positions corresponding to the O1s and the Zn2p. As form above XPS, we showed that the atom ratio of Zn:O related 1:1.1504 on ZnO thin film, so we could obtained useful information for p-type ZnO thin film.

Effect of Ignition Delay Time on Autoignited Laminar Lifted Flames (자발화된 층류 부상화염에 대한 점화지연시간의 영향)

  • Choi, Byung-Chul
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.35 no.10
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    • pp.1025-1031
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    • 2011
  • Autoignition characteristic is an important parameter for designing diesel or PCCI engines. In particular, diesel spray flames are lifted from the nozzle and the initial flame is formed by an autoignition phenomenon. The lifted nature of diesel spray flames influences soot formation, since air will be entrained into the spray core by the entrainment of air between the nozzle region and the lifted flame base. The objective of the present study was to identify the effect of heat loss on the ignition delay time by adopting a coflow jet as a model problem. Methane ($CH_4$), ethylene ($C_2H_4$), ethane ($C_2H_6$), propene ($C_3H_6$), propane ($C_3H_8$), and normal butane (n-$C_4H_{10}$) fuels were injected into high temperature air, and the liftoff height was measured experimentally. As the result, a correlation was determined between the liftoff height of the autoignited lifted flame and the ignition delay time considering the heat loss to the atmosphere.

Development of 10 kW Dish-Stirling System for Commercialization and Analysis of Operating Characteristics (10 kW급 접시형 태양열발전시스템 사업모델 개발 및 운전특성 분석)

  • Kim, Jong-Kyu;Lee, Sang-Nam;Kang, Yong-Heack
    • Journal of the Korean Solar Energy Society
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    • v.30 no.6
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    • pp.118-124
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    • 2010
  • In order to develop commercial model of 10kW dish-Stirling solar thermal power system, modification for the exiting facility was taken for a year as a Leading Project in KIER. During the project, solar tracking system, control and monitoring system and high durability reflector were developed and long term operation were performed. The solar tracking system was tested for four months to investigate the degree of precision and adapted to the control system for an actual operation from October in 2009. The sun tracking accuracy of ${\pm}4$ mrad using modified control system was obtained and the system operated successfully during the experimental period. The monitoring system displays engine pressure, electric generation amounts, generator RPM, receiver temperatures, and etc. from Stirling engine and weather data of Direct Normal Irradiation, Horizontal Global Insolation, wind speed & direction, and atmosphere temperature from weather station. According to the operating results in a clear sky day, electric power of 6,890 W was generated at the DNI value of 850 W/$m^2$ and the averaged solar-to-electricity efficiency during a whole day reached to 18.99%. From the overall operating results, linear power generation trend could be observed with increasing DNI value. The solar-to-electricity efficiency achieved to 19% around the DNI value of 700 W/$m^2$ and increased to 20% when the DNI value goes up to 900 W/$m^2$.

Satisfaction with School Food Service of Middle School Students in Daegu (대구지역 중학생들의 학교 급식 만족도 조사)

  • Jang Mi-Ae;Choi Mi-Ja
    • Journal of the East Asian Society of Dietary Life
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    • v.15 no.2
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    • pp.226-234
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    • 2005
  • A study was conducted to improve satisfaction to school food service and to furnish source materials for nutrient education by researching degree of satisfaction of middle school students to school food service. Following results are from the study that targeted 215 male students and 173 female students in 5 middle schools in Daegu. Satisfaction rates regarding taste of foods, smell, proper temperature, use of seasonal food, cafeteria atmosphere, numbers of side dishes, and kindness of the cook in a cafeteria were higher than dissatisfaction. And dissatisfaction rates were higher in quantity and quality of foods, sanitation, purity of table wares, opening to nutrient education and related informations for students, opinion reflection of students, food serving time and gratification to food serving than the opposite. But the degree of general satisfaction on school food service were higher than the degree of general dissatisfaction. Sanitation was the first thing to be changed in school food service, then quantity of food and taste for the last. And there were notable differences between male students and female students in sanitation satisfaction. The variables that influence on satisfaction to school food service were sanitary administration, numbers of side dishes, quantity of foods, nutrient, smell and taste when ranked. And the main three things that have similar rate in quantity with satisfaction rate are taste, smell and nutrient of school food service. Through these followed results, degree of general satisfactions to school food service were higher than degree of general dissatisfactions. But sanitation, quantity and quality of foods, taste, and food serving size were not satisfactory for students in rate. Therefore it has to be improved to enhance satisfactions to middle school food service.

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Development of Estimating Method for Areal Evapotranspiration using Satellite Data (인공위성 자료를 활용한 광역증발산량의 산정방법 개발)

  • Shin, Sha-Chul;An, Tae-Young
    • Journal of the Korean Association of Geographic Information Studies
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    • v.10 no.2
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    • pp.71-81
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    • 2007
  • One of the most important hydrologic components is evapotranspiration. It is a process by which water is evaporated from moist land surfaces and transpired into atmosphere by plants. There are many methods of estimating evapotranspiration rate and its potential such as the methods of soil-moisture sampling, lysimeter measurements, water balance, energy balance, groundwater fluctuations and evapotranspiration. But it is very difficult to estimate evapotranspiration in terms of regional discrete characteristics of topography and/or vegetation. The evapotranspiration is strongly affected by ground covering vegetation, and the degree of vegetation growth. In order to grasp vegetation condition over a vast study area, NDVI (Normalized Difference Vegetation Indices) calculated from the data obtained from NOAA/AVHRR were utilized. Through multi-regression analysis, we developed a model equation to estimate the evapotranspiration using NDVIs and temperature data.

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Magnetic Properties of NdFeB Powders Prepared by Mechanical Alloying (기계적합금법으로 제조한 NdFeB계 분말의 자기적 성질)

  • Kim, Taek-Soo;Hwang, Yeon;Lee, Hyo-Sook
    • Journal of the Korean Magnetics Society
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    • v.8 no.4
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    • pp.210-215
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    • 1998
  • $Nd_{15}Fe_{77}B_8$ and $Nd_{16}Fe_{76}B_8$ powders were prepared by mechanical alloying in Ar atmosphere, and their phases and magnetic properties were investigated with as a function of the annealing temperature. It was found that the mechanical alloyed $Nd_{16}Fe_{76}B_8$ powder for 450 hours was amorphous phase with a part of $\alpha$-Fe crystallites. The obtained powders at 700 $^{\circ}C$ for 30 minute resulted in two phase of $Nd_2Fe_{14}B$ and $NdB_6$ by the solid-state reaction. The mechanical alloyed $Nd_{16}Fe_{76}B_8$ powder for 450 hour and annealed at 700 $^{\circ}C$ for 30 minute was showed $_iH_c\;of\;9.91\;kOe,\; B_{max}\;of\;12.93\;kG,\;Br\;of\;7.6\;kG\;and\;(BH)_{max}\;10.1\;MGOe$.

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Float Zone Growth of Superconduction $Bi_2Sr_2CaCu_2O_8$ Fiber with Halogen Lamp (할로겐 램프 열원을 이용한 초전도성 $Bi_2Sr_2CaCu_2O_8$ Fiber의 Float Zone 성장)

  • 김철진;정준기
    • Korean Journal of Crystallography
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    • v.7 no.2
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    • pp.147-155
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    • 1996
  • Floating Zone Image furnace with halogen lamps as heat source has been made and applied to the growth of high-Tc superconductor Bi2Sr2CaCu2O8. The manufactured crystal growth equipment is composed of holder unit for setting the halogen lamps at the focal point of the elliptical mirror, image furnace with maximum temperature of 1800℃ with 1kW halogen lamps, cooling unit, feeding unit for supplying source material to the molten zone, pulling unit for crystal growth, and the control unit in the range of 2mm/hr -40 mm/hr vertical movement and 15rpm - 12rpm rotation. Bi2Sr2CaCu2O8 fibers have been grown with 300W halogen lamps and characterized with XRD, SEM and EDS. The growth condition was air atmosphere, growth speed 3∼4mm/hr, rotation speed of upper and lower part 20∼25 rpm. The fiber was composed of 20∼25 rpm matrix phase and secondary phases such as (Sr,Ca)CuO2 and (Sr,Ca)2CuO3.

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Corrosion Cost and Corrosion Map of Korea - Based on the Data from 2005 to 2010

  • Kim, Y.S.;Lim, H.K.;Kim, J.J.;Hwang, W.S.;Park, Y.S.
    • Corrosion Science and Technology
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    • v.10 no.2
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    • pp.52-59
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    • 2011
  • Corrosion of metallic materials occurs by the reaction with corrosive environment such as atmosphere, marine, soil, urban, high temperature etc. In general, reduction of thickness and cracking and degradation are resulted from corrosion. Corrosion in all industrial facilities and infrastructure causes large economic losses as well as a large number of accidents. Economic loss by corrosion has been reported to be nearly 1-6% of GNP or GDP. In order to reduce corrosion damage of industrial facilities, corrosion map as well as a systematic investigation of the loss of corrosion in each industrial sector is needed. The Corrosion Science Society of Korea in collaboration with 15 universities and institutes has started to survey on the cost of corrosion and corrosion map of Korea since 2005. This work presents the results of the survey on cost of corrosion by Uhlig, Hoar, and input-output methods, and the evaluation of atmospheric corrosion rate of carbon steel, weathering steel, galvanized steel, copper, and aluminum in Korea. The total corrosion cost was estimated in terms of the percentage of the GDP of industry sectors and the total GDP of Korea. According to the result of Input/output method, corrosion cost of Korea was calculated as 2.9% to GDP (2005). Time of wetness was shown to be categories 3 to 4 in all exposure areas. A definite seasonal difference was observed in Korea. In summer and fall, time of wetness was higher than in other seasons. Because of short exposure period (12 months), significant corrosion trends depending upon materials and exposure corrosion environments were not revealed even though increased mass loss and decreased corrosion rate by exposure time.

The Effect of Shielding N2 gas on The Pitting Corrosion of Seal-welded Super Austenitic Stainless Steel by Autogenous Welding

  • Kim, Ki Tae;Chang, Hyun Young;Kim, Young Sik
    • Corrosion Science and Technology
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    • v.16 no.2
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    • pp.49-58
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    • 2017
  • Many research efforts on the effect of nitrogen on the corrosion resistance of stainless steels have been reported, but little research has been conducted on the effect of nitrogen for the weldment of stainless steels by the seal-weld method. Therefore, this work focused on the determining the corrosion resistance of tube/tube sheet mock-up specimen for sea water condensers, and elucidating the effect of shielding nitrogen gas on its resistance. The pitting corrosion of autogenously welded specimen propagated preferentially along the dendritic structure. Regardless of the percent of shielding nitrogen gas, the analyzed nitrogen contents were very much lower than that of the bulk specimen. This can be arisen because the nitrogen in shielding gas may partly dissolve into the weldment, but simultaneously during the welding process, nitrogen in the alloy may escape into the atmosphere. However, the pitting resistance equivalent number (PREN) of the interdendrite area was higher than that of the dendrite arm, regardless of the shielding gas percent; and the PREN of the interdendrite area was higher than that of the base metal; the PREN of the dendrite arm was lower than that of the base metal because of the formation of (Cr, Mo) rich phases by welding.