• Title/Summary/Keyword: Annealing of amorphous

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The Magnetic Properties of $Fe_{87}Zr_{7}B_{5}Ag_{1}$(at.%) Amorphous Alloy ($Fe_{87}Zr_{7}B_{5}Ag_{1}$ 비정질합금의 연자기 특성)

  • 김병걸;송재성;김현식;오영우
    • Journal of the Korean Magnetics Society
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    • v.5 no.1
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    • pp.8-14
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    • 1995
  • The magnetic properties of an $Fe_{87}Zr_{7}B_{5}Ag_{1}$(at.%) amorphous alloy have been investigated as a function of annealing temperatures to clarify its application potential as a core material for high-frequency use by adding a small amount of insoluble element of Ag. A new excellent soft magnetic material was developed. The amorphous alloy produced by relatively low temperature annealing at $T_{a}=400^{\circ}C$ exhibited very high initial permeability$(\mu_{i})$ of 288,000 at 1kHz and 2mOe, very low coercivity$(H_{c})$ of 15mOe and low core loss$(W_{c})$ of 50W/kg at 100kHz and 1,000G which is comparable with Co-based amorphous alloys, respectively. It is notable that the values obtained in the present study are the best magnetic properties among various kinds of Fe-based soft amorphous materials reported up to date. The reasons for the achievement of good soft magnetic properties are presumably due to the homogeneous formation of very fine $\alpha$-Fe clusters with the size of 2~3nm in an amorphous matrix, which can be deduced from the increase of resistivity and the TEM observation. The very fine $\alpha$-Fe clusters embedded in an amorphous matrix had a great influence on reduction of magnetostriction and refinement of magnetic domain.

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Solid Phase Crystallizations of Sputtered and Chemical Vapor Deposited Amorphous Hydrogenated Silicon (a-Si:H) Thin Film (스퍼터링 및 화학기상 증착 비정질 수소화 실리콘박막의 고상결정화)

  • 김형택
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.11 no.4
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    • pp.255-260
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    • 1998
  • Behavior of solid phase crystallizations (SPC) of RF sputtered and LPCVD amorphous hydrogenated silicon film were investigated. LPCVD films showed the higher degree of crystallinity and larger grain size than sputtered films. The applicable degree of crystallinity was also obtained from sputtered films. The deposition method of amorphous silicon film influenced the behavior of post annealing SPC. Observed degree of crystallinity of sputtered films strongly depended on the partial pressure of hydrogen in deposition. The higher deposition temperature of sputtering provided the better crystallinity after SPC. Due to the high degree of poly-crystallinity, the retardation of larger grain growth was observed on sputtering film.

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Characterization of Solid Phase Crystallization in Sputtered and LFCVD Amorphous Silicon Thin Film (스퍼터링 및 저압화학기상증착 비정질 실리곤 박막의 고상 결정화 특성)

  • 김형택
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1995.11a
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    • pp.89-93
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    • 1995
  • Effects of hydrogenation in amorphous silicon rile growths on Solid Phase Crystallization (SPC) was investigated using x-ray diffractometry, energy dispersive Spectroscopy, and Raman spectrum. Interdiffusion of barium(Ba) and aluminum(Al) compounds of corning substrate was observed in both of rf sputtering and LFCVD films under the low temperature(580$^{\circ}C$) annealing. Low degree of crystallinity resulted from the interdiffusion was obtained. Highly applicable degree of crystallinity was obtained through the mechanical damage induced surface activation on amorphous silicon films. X-ray diffraction intensity of (111) orientation was used to characterize the degree of crystallinity of SPC. Nucleation and growth rate in SPC could be controllable through the employed surface treatment. IIydrogenated LPCVD films showed the superior crystallinity to non-hydrogenated sputtering films. Insignificant effects of activation treatment in sputtered film was of activation treatment in sputtered film was observed on SPC.

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Preparation and Magnetic Properties of Co-system Amorphous Thin Film by the Sputter method (스파터법에 의한 Co-계 비정질박막의 제작과 자기특성)

  • 임재근;문현욱;서강수;신용진
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1994.11a
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    • pp.190-191
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    • 1994
  • In this paper, We study on the fabrication of amorphous this film of zeromagnetostriction material and the magnetic properties. This films are fabricated by using sputtering method with input power of 400∼607[W], Ar gas pressure of 3∼ 9[mTorr] and target composition of Fe$\sub$4.7/ Co$\sub$74.3/Si$_2$B$\sub$19/. Sample this films with diameter of 14[mm ] and thickness of 27-30[$\mu\textrm{m}$] were obtained through experiments. When we analyzed the magnetic properties before and after annealing with sample thin films, we confirmed that magnetic domain wall amorphous thin films consisted for Neel magnetic domain wall with the width of about 1[$\mu\textrm{m}$].

Bulk Processing of an Amorphous $AI_{85}Ni_{10}Y_{5}$ Alloy Ribbon and Mechanical Properties by Annealing Treatment (비정질 $AI_{85}Ni_{10}Y_{5}$ 합금 리본의 벌크화와 어닐링에 따른 기계적 특성)

  • 고병철;김종현;유연철
    • Transactions of Materials Processing
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    • v.8 no.6
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    • pp.626-633
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    • 1999
  • $Al_{85}Ni_{10}Y_5$ (at. %) amorphous alloy ribbons have been produced by rapidly solidification process and consolidated by the conventional powder metallurgy method. The grains with ∼90 nm were obtained in the Al85Ni10Y5 alloy extrudates by hot-pressing followed by hot-extusion. To investigate the effect of heat treatment on microstructural change of the extrudates, heat treatment was carried out from 200℃ to 400℃ at the step of 50℃. In addition, mechanical properties of the extrudates were analysed from torsion test at the temperature range or 400∼500℃ under a strain rates of 0.2, 0.5, and 1.0/sec. The extrudates showed a flow stress of ∼190 MPa and low elongation of ∼150% at 400℃, contributing to the enhancement of ductility and hardness for extrudates. Also, grain boundary sliding was occurred in the $Al_{85}Ni_{10}Y_5$ alloy during hot deformation.

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Magnetic Properties of Amorphous FeSiB and Nanocrystalline $Fe_{73}Si_{16}B_7Nb_3Cu_1$ Soft Magnetic Sheets

  • Cho, H.J.;Cho, E.K.;Song, Y.S.;Kwon, S.K.;Sohn, K.Y.;Park, W.W.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.786-787
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    • 2006
  • The magnetic inductance of nanocrystalline $Fe_{73}Si_{16}B_7Nb_3Cu_1$ and an amorphous FeSiB powder sheet has been investigated to identify RFID performance. The powder was mixed with binder and solvent and tape-casted to form films. Results show annealing significantly influenced on the inductance of the material. The surface oxidation of the particles was the main reason for the reduced inductance. The maximum inductance of $Fe_{73}Si_{16}B_7Nb_3Cu_1$ alloy was about $88{\mu}H$ at 17.4 MHz, about 65% greater compared to the FeSiB alloy. The higher inductance in the nanocrystalline alloy indicates it may be used as a potential replacement of current RFID materials.

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Stress Effects on Magnetic Properties of Amorphous Fe-B-Si Ribbon (Fe-B-Si 비정질 리본의 자기특성에 미치는 응력의 영향)

  • 송재성;김기욱;임호빈
    • The Transactions of the Korean Institute of Electrical Engineers
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    • v.40 no.5
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    • pp.496-500
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    • 1991
  • The effects of annealing with and without magnetic field on magnetic properties of amorphous Fe-B-Si cores have been investigated as a function of toroidal stress. By decreasing the toroidal stress, the magnetic properties of the amorphous ribbon have beenimproved. Near 180 domain walls exist in the thermally annealed toroidal cores, but the domain walls exist in the thermally annealed toroidal cores, but the domain walls are not parallel to the longitudinal direction of the ribbon. In the specimen annealed with a magnetic field strength of 10 Oe in the longitudinal ribbon length axis, the domains are nearly parallel to the longitudinal direction due to the field induced uniaxial anisotropy resulting in further increase in the remanent magnetization and decrease in the coercive force and loss.

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Current sensor application of giant magnetoimpedance in amorphous materials (교류자기저항효과를 이용한 비정질 리본 전류센서)

  • Rheem, Y.W.;Kim, C.G.;Kim, C.O.;Kim, G.D.;Park, Y.T.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.04a
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    • pp.11-13
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    • 2002
  • The performance of DC current sensor based on giant magnetoimpedance (GMI) effect in amorphous ribbon has been tested. The ribbon after field annealing shows the maximum GMI ratio of 30 % at 100 kHz measuring frequency. In the sensor element of sample wound the circular form, GMI ratio and sensitivity are decreased due to internal stress. The sensor voltage output increases with applied DC current up to 1 A with a good linearity, of which direction can be known due to asymmetric characteristics.

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Magneto-Impedance Effect of CoFeSiBNi Amorphous Magnetic Films according to the size (CoFeSiBNi 아몰퍼스 합금의 소자 크기에 대한 자기-임피던스 효과 관찰)

  • Park, Byung-Kyu;Hwang, Sung-Woo;Moon, Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.339-341
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    • 2007
  • Soft ferromagnetic materials are very useful for many sensors using magnetic materials with high permeability, low coercivity and low hysteresis loss. Among them, FeCoSiBNi amorphous magnetic films show us a good impedance change(about 3.05%/Oe, at 12MHz) by the exterior magnetic field in this experiment. These are produced by rapid solidification from the melt and the material is ejected in a jet from a nozzle and quenched in a stream of liquid. After that, we make them a shape of wire with different sizes of width. Thus, we can find that the impedance change (122.16%, at 12MHz) is occurred and the fabricated magnetic wire has the characteristics of good sensor element.

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APPLICATIONS OF ASYMMETRIC HYSTERESIS LOOPS IN AMORPHOUS ALLOYS

  • Jr., C.D. Graham;Shin, K-H.;Zhou, Peter Y.
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.579-582
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    • 1995
  • The use of amorphous magnetic alloys as tags or targets in electronic article surveillance systems such as antishoplifting desvices is briefly reviewed. Improved tags became possible with the discovery in 1988 of asymmetric magnetization reversal (AMR) in certain amorphous alloys annealed in applied field approximately equal to the earth's field. These asymmetric hysteresis loops are highly unusual, if not unique, and so greatly diminish the probability of false alarms in a detection system. furthermore, the jump field Hj, which is the coercive field in negative applied fields, can be controlled over a useful range by controlling the field applied to the sample during annealing. By applying several tags to an object, each with a different jump field, it is possible to identify the object with a numeric code that can be remotely read by nonoptical means.

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