• 제목/요약/키워드: Annealing Texture

검색결과 141건 처리시간 0.025초

수소 분위기 중 열처리법을 이용한 고자기이방성 L10 FePt 박막 제작 (Preparation of tetragonal phase L10 FePt thin films with H2 annealing atmosphere)

  • 공석현;김경환
    • 한국진공학회지
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    • 제16권5호
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    • pp.343-347
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    • 2007
  • Glass disk상에 대향 타겟식 스퍼터링(Facing Target Sputtering) 방식을 이용하여 $0.1\;{\AA}/s$의 낮은 증착속도로 증착시킬 경우 b.c.c. (100)면 우선배향성을 확인하였으며, 그 위에 Pt박막을 증착시킨 경우 hetero-epitaxial 성장에 의해 Pt박막이(111)의 조밀면이 아닌 (100)면이 우선배향 되었다. 이렇게 형성된 Fe (100)/Pt (100) 이층막(두께 각 3 nm)을 $600\;^{\circ}C$ 수소분위기에서 열처리함에 의해 막전체에 걸쳐서 f.c.t. (00n)면을 형성시키는 데 성공하고, 또한 Fe (100)면 상에 Pt 박막을 증착시키는 동안 열처리를 하고 증착 이후 수소분위기에서 열처리함에 의해 열처리 시간 및 온도를 크게 낮출 수 있음을 확인하였다.

주조 후 냉간 압연된 Al-6.5Mg-1.5Zn계 합금의 어닐링 특성 (Annealing Characteristics of an Al-6.5Mg-1.5Zn Alloy Cold-Rolled After Casting)

  • 오성준;이성희
    • 한국재료학회지
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    • 제28권9호
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    • pp.534-538
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    • 2018
  • The annealing characteristics of a cold rolled Al-6.5Mg-1.5Zn alloy newly designed as an automobile material is investigated in detail. The aluminum alloy in the ingot state is cut to a thickness of 4 mm, a total width of 30 mm and a length of 100 mm and then reduced to a thickness of 1 mm (reduction of 75 %) by multi-pass rolling at room temperature. Annealing after rolling is performed at temperatures ranging from 200 to $400^{\circ}C$ for 1 hour. The tensile strength of the annealed material tends to decrease with the annealing temperature and shows a maximum tensile strength of 482MPa in the material annealed at $200^{\circ}C$. The tensile elongation of the annealed material increases with the annealing temperature, while the tensile strength does not, and reaches a maximum value of 26 % at the $350^{\circ}C$ annealed material. For the microstructure, recovery and recrystallization actively occur as the annealing temperature increases. The recrystallization begins to occur at $300^{\circ}C$ and is completed at $350^{\circ}C$, which results in the formation of a fine grained structure. After the rolling, the rolling texture of {112}<111>(Cu-Orientation) develops, but after the annealing a specific texture does not develop.

Simulated Annealing의 수렴속도 개선에 관한 연구 (Fast Simulated Annealing Algorithm)

  • 정철곤;김중규
    • 한국통신학회논문지
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    • 제27권3A호
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    • pp.284-289
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    • 2002
  • 본 논문에서는 MRF(Markov Random field)를 이용해 영상을 분할할 때, 에너지 최적화를 위해 사용되는 simulated annealing의 수렴속도를 개선하는 방법을 제안하였다. Simulated annealing은 잡음이 포함된 영상이나, 텍스쳐 영상에서 좋은 분할 결과를 나타내지만, 수렴속도가 길다는 단점이 있다. 본 논문에서는 수렴속도를 개선하기 위해 픽셀 레이블의 초기값을 픽셀의 intensity에 따라 adaptive하게 부여하여 simulated annealing을 수행하였다. 이 방법으로 모의실험을 수행한 결과, 기존의 방법보다 수렴 속도를 크게 향상시킬 수 있었다.

알루미늄 1050계 판재에서 결정립 성장 집합조직에 미치는 재결정 집합조직의 영향 (Effect of Primary Recrystallization Texture on the Formation of Grain Growth Texture in Aluminum 1050 Sheet)

  • 김현철;강형구;허무영
    • 대한금속재료학회지
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    • 제47권6호
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    • pp.356-362
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    • 2009
  • In order to vary the primary recrystallization textures, AA 1050 sheets were cold rolled in two different manners. Differences in cold rolling schedule gave rise to the formation of different cold rolling textures also leading to the formation of different primary recrystallization textures. Upon annealing for grain growth, changes in microstructure and texture hardly occurred in the sample depicting Cube recrystallization texture, while grain growth was accompanied with the development {001}<100> Cube texture in the sample displaying a recrystallization texture comprising of weak rolling texture components. The selective growth of Cube oriented grains is attributed to the high mobility of their grain boundaries.

Effects of Hot Rolling on Microstructures and Magnetic Properties

  • Hong, Byung-Deug;Kim, Jae-Kwan;Cho, Kyung-Mox
    • Journal of Magnetics
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    • 제11권3호
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    • pp.111-114
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    • 2006
  • We electroplated copper-cobalt thin films on a silicon substrate, which had 150 nm thick copper seed layer. The adhesion between the two metallic layers could be increased by utilizing a proper organic additive, pulse plating technique, and high temperature annealing. The thin films exhibited columnar growth of the deposits and enhanced adhesion. This is attributed to the grain growth mechanism introduced by the additive and annealing.

이속압연에 의해 제조된 AA1100 판재의 소성변형비 예측 (Prediction of the Macroscopic Plastic Strain Ratio in AA1100 Sheets Manufactured by Differential Speed Rolling)

  • 최재권;조재형;김형욱;강석봉;최시훈
    • 대한금속재료학회지
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    • 제48권7호
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    • pp.605-614
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    • 2010
  • Conventional rolling (symmetric) and differential speed rolling (DSR) were both applied to AA1050 sheets at various velocity ratios, from 1 to 2 between the top and bottom rolls. An electron backscatter diffraction (EBSD) technique was used to measure texture inhomogeneity through the thickness direction. After the annealing process, the annealing texture of the DSR processed sheets was different from that of conventionally rolled sheets. The velocity ratio between the top and bottom rolls affected the texture inhomogeneity and macroscopic plastic strain ratio of the AA1050 sheets. A prediction for the macroscopic plastic strain ratio of AA1050 sheets was carried out using a visco-plastic self-consistent (VPSC) polycrystal model. The strain ratio directionality that was predicted using the VPSC polycrystal model was in good agreement with experimental results.

Texture Development in Liquid-Phase-Sintered β -SiC by Seeding with β -SiC Whiskers

  • Kim, Won-Joong;Roh, Myong-Hoon
    • 한국세라믹학회지
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    • 제43권3호
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    • pp.152-155
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    • 2006
  • Silicon carbide ceramics seeded with 10-30 wt% SiC whiskers are fabricated by hot pressing and annealing. A quantitative texture analysis including calculation of the Orientation Distribution Function (ODF) is used for obtaining the degrees of preferred orientation of the fabricated samples. The microstructure and crystallographic texture are discussed with respect to the effect of ${\beta}-SiC$ whisker seeds on the resulting fracture toughness values. The SEM microstructures and the texture data reveal a correlation between texture and fracture toughness anisotropy.

Evolution of Cube Texture in the Nickel-Silver-Stainless steel Multi-layer Sheet

  • Lee, Hee-Gyoun;Jung, Yang-Hong;Hong, Gye-Won
    • Progress in Superconductivity
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    • 제1권1호
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    • pp.51-55
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    • 1999
  • A Ni/Ag/Stainless steel 310S(SS310S) multi-layer sheet has been fabricated by a combination of vacuum brazing, cold rolling and texture annealing processes. After heat-treating the thin Ni/Ag/SS310S multi-layer sheet at $900^{\circ}C$ for 2h, development of (100)<001>cube texture on Ni surface was revealed by (111) pole figure. Quantitative chemical analysis was made by EPMA for the cross-section of the Ni/Ag/SS310S multi-layer sheet. EPMA results showed that Ag diffusion into the Ni layer, which may suppress the cube texture development, was negligible. A small amount of Cr atoms were detected in the Ni layer. It showed that Ag can be used as a chemical barrier of alloying element atoms in Ni layer for the Ni/Ag/SS310S multi-layer sheet and a strong cube texture was developed for the Ni layer in the Ni/Ag/SS310S multi-layer sheet.

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분말법과 주조법으로 제조한 coated conductor용 Ni 기판 개발 (Fabrication of textured Ni substrates for coated conductor prepared by powder metallurgy and plasma arc melting method)

  • 임준형;김정호;김규태;장석헌;주진호;나완수;홍계원;지봉기;김찬중
    • Progress in Superconductivity
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    • 제5권1호
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    • pp.70-74
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    • 2003
  • We fabricated cube textured Ni substrate for YBCO coated conductor and evaluated the effects of processing parameters on microstructural evolution and texture formation. Ni-rods as an initial specimen were prepared by two different methods, i.e., powder metallurgy(PM) and plasma arc melting(PAM). Subsequently, the rods were cold rolled to 100 $\mu\textrm{m}$ thick substrate and annealed at temperatures of $700∼1200^{\circ}C$. The texture of the substrate was characterized by pole-figure. It was observed that the texture of substrate made by P/M did not significantly varied with annealing temperature of 600∼$l100^{\circ}C$ and the full-width at half-maximums (FWHM) of both in-plane and out-of-plane were 9$^{\circ}$$10^{\circ}$. On the other hand, the texture of substrate made by PAM was more dependent on the annealing temperature and the corresponding values were $9^{\circ}$$13^{\circ}$ at the temperature range. In addition, recrystallization twin texture, (221)<221>, was formed as the temperature increased further. OM profiles showed that the grain size of substrate made by P/M was smaller than that made by PAM and this difference was correlated to the microstructure of initial specimens.

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Al 박막의 underlayer로서의 Ionized Physical Vapor Deposition (I-PVD) Ti 또는 I-PVD Ti/Metal-Organic Chemical Vapor Deposition TiN (Ti Prepared by ionized physical vapor deposition (I-PVD) and TiN prepared by metal-organic chemical vapor deposition(MOCVD) as underlayers of aluminum TiN)

  • 이원준;나사균
    • 한국진공학회지
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    • 제9권4호
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    • pp.394-399
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    • 2000
  • Underlayer의 종류 및 두께가 Al 박막의 texture 및 면저항 변화에 미치는 영향을 연구하였다. Al의 underlayer로는 ionized physical vapor deposition(I-PVD)에 의해 제조된 Ti와 I-PVD Ti 위에 metalorganic chemical vapor deposition(MOCVD)에 의해 제조된 TiN을 적층한 구조가 사용되었으며, 각각에 대해 두께를 변화시키면서 Al 박막의 배향성, 면저항을 조사하고, $400^{\circ}C$, $N_2$분리기에서 열처리하면서 면저항의 변화를 조사하였다. I-PVD Ti만을 Al의 underlayer로 사용한 경우, Ti두께가 5 nm이어도 Al 박막이 우수한 <111> 배향성을 나타내었으나, Al-Ti반응 때문에 열처리 후 Al 배선의 면저항이 크게 상승하였다. I-PVD 와 Al 사이에 MOCVD TiN을 적용함에 의해 Al <111> 배향성의 큰 저하없이 Al-Ti 반응에 의한 면저항의 증가를 억제할 수 있었으며, MOCVD TiN의 두께가 4 nm 이하일 때 특히 우수한 Al <111> 배향성을 나타내었다.

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