• Title/Summary/Keyword: Analytical Society

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Data intercomparison and determination of toxic and trace elements in Algae using Instrumental Neutron Activation Analysis (중성자방사화분석에 의한 Algae중의 독성미량원소의 정량 및 실험실간 비교검증)

  • Chung, Yong-Sam;Moon, Jong-Hwa;Park, Kwang-Won;Lee, KiI-Yong;Yoon, Yoon-Yeol
    • Analytical Science and Technology
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    • v.12 no.4
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    • pp.346-353
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    • 1999
  • For the non-destructive multi-elemental analysis of environmental and biological materials, instrumental neutron activation analysis (INAA) was applied for the determination of toxic and trace elements in a set of three Algae samples provided by the International Atomic Energy Agency (IAEA). The analytical quality control was evaluated by comparing the analytical results of two standard reference materials of the National Institute of Standards and Technology (NIST); Oyster Tissue (SRM 1566a) and Citrus Leaves (SRM 1572). According to given analytical procedure, the concentration of 15-25 elements including spiked elements such as As, Cd, Cr and Hg in Algae samples were determined. To identify and validate these results, a data intercomparison program using more than 35 analytical methods in 150 laboratories was carried out and the estimated statistical data are summarized. Result of INAA is favorable, therefore, it is illustrated that can be applied for routine analysis of essential and toxic elements in algae samples as well as analytical quality assurance.

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The Significance of the Analytical Sciences In Environmental Assessment

  • Chung, Yong;Ahn, Hye-Won
    • Analytical Science and Technology
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    • v.8 no.4
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    • pp.1079-1087
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    • 1995
  • The quality of human life is directly related to the quality of the environment. To assess environmental quality we must first determine the MCLG(Maximum Contaminant Level Goal), MCL(Maximum Contaminant Level), environmental impact and so on. The MCLG is the concentration at which no known adverse health effects occur. The MCLG is determined by risk assessment identifying which process is hazardous assessing, dose-response, human exposure, and characteristics of risk. With consideration of analytical methods, treatment technology, cost and regulatory impact, the MCL is set as close to the MCLG as possible. In this way, determination of the concentration and national distribution of contaminants is important for assessment of environmental quality The analytical sciences pose potential problems in assessing environmental quality. Continuing improvement in the performance of analytical instruments and operating technique has been lowering the limits of detectability. Contaminant concentration below the detection limit has usually been reported as ND(Not-Detected) and this has often been misunderstood as equivalent to zero. Because of this, more the contaminant concentration in the past was below the detection limit, whereas contaminants can be quantified now even though the contaminant concentration might remain the same or may even have decreased. In addition, environmental sampling has various components due to heterogeneous matrices. These samples are used to overestimate the concentration of the contaminant due to large variability, resulting in excess readings for MCL. In this paper, the significance of the analytical sciences is emphasized in both a conceptual and a technical approach to environmental assessment.

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Consistent Displacement Load Method for Nonlinear Semi-Analytical Design Sensitivity Analysis (준해석적 비선형 설계민감도를 위한 보정변위하중법)

  • Lee, Min-Uk;Yoo, Jung-Hun;Lee, Tae-Hee
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.29 no.9 s.240
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    • pp.1209-1216
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    • 2005
  • Three methods for design sensitivity such as numerical differentiation, analytical method and semi-analytical method have been developed for the last three decades. Although analytical design sensitivity analysis is exact, it is hard to implement for practical design problems. Therefore, numerical method such as finite difference method is widely used to simply obtain the design sensitivity in most cases. The numerical differentiation is sufficiently accurate and reliable for most linear problems. However, it turns out that the numerical differentiation is inefficient and inaccurate because its computational cost depends on the number of design variables and large numerical errors can be included especially in nonlinear design sensitivity analysis. Thus semi-analytical method is more suitable for complicated design problems. Moreover semi-analytical method is easy to be performed in design procedure, which can be coupled with an analysis solver such as commercial finite element package. In this paper, implementation procedure for the semi-analytical design sensitivity analysis outside of the commercial finite element package is studied and computational technique is proposed, which evaluates the pseudo-load for design sensitivity analysis easily by using the design variation of corresponding internal nodal forces. Errors in semi-analytical design sensitivity analysis are examined and numerical examples are illustrated to confirm the reduction of numerical error considerably.

Analytical Prediction and Experimental Verification of Electromagnetic Performance of a Surface-Mounted Permanent Magnet Motor having a Fractional Slot/Pole Number Combination

  • Hong, Sang-A;Choi, Jang-Young;Jang, Seok-Myeong
    • Journal of Magnetics
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    • v.19 no.1
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    • pp.84-89
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    • 2014
  • This paper presents an analytical prediction and experimental verification of the electromagnetic performance of a parallel magnetized surface-mounted permanent magnet (SPM) motor having a fractional number of slots per pole combination. On the basis of a two-dimensional (2-D) polar coordinate system and a magnetic vector potential, analytical solutions for flux density produced by the permanent magnets (PMs) and stator windings are derived. Then, analytical solutions for back-electromotive force (emf) and electromagnetic torque are derived from these field solutions. The analytical results are thoroughly validated with 2-D nonlinear finite element (FE) analysis results. Finally, the experimental back-emf and electromagnetic torque measurements are presented to test the validity of the analysis.

MS-Based Technologies for the Study of Site-Specific Glycosylation

  • Kim, Unyong;Oh, Myung Jin;Lee, Jua;Hwang, Hee Yeon;An, Hyun Joo
    • Mass Spectrometry Letters
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    • v.8 no.4
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    • pp.69-78
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    • 2017
  • Glycosylation, which is one of the most common post-translation modification (PTMs) of proteins, plays a variety of crucial roles in many cellular events and biotherapeutics. Recent advances have led to the development of various analytical methods employing a mass spectrometry for glycomic and glycoproteomic study. However, site-specific glycosylation analysis is still a relatively new area with high potential for technologies and method development. This review will cover current MS-based workflows and technologies for site-specific mapping of glycosylation ranging from glycopeptide preparation to MS analysis. Bioinformatic tools for comprehensive analysis of glycoprotein with high-throughput manner will be also included.

Impact response analysis of delaminated composite laminates using analytical solution (이론 해를 이용한 층간 분리된 적층판의 충격거동 해석)

  • Kim, Sung-Joon;Shin, Jeong-Woo;Chae, Dong-Chul
    • Proceedings of the KSME Conference
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    • 2007.05a
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    • pp.315-320
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    • 2007
  • An analytical solution has been developed for the impact response of delaminated composite plates. The analysis is based on an expansion of loads, displacements, and rotations in a Fourier series which satisfies the end boundary conditions of simply-supported. The analytical formulation adopts the Laplace transformation technique, requiring a linearization of contact deformation. In this paper, the nonlinear contact stiffness is replaced by a linearized stiffness, to provide an estimate of the additional compliance due to contact area deformation effects. It has been shown that defects such as delaminations may be modeled as spring stiffness. The change in the impact characteristics as this spring stiffness has been investigated theoretically. Predicted impact responses using analytical solution are compared with the numerical ones from the 3-D non-linear finite element model. From the results, it is shown that analytical solution was found to be reliable for predicting the impact response.

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Launch Stage Thermal Analysis on a Mass Varying Satellite Box by Analytical Solutions (해석해를 이용한 질량변화가 있는 위성 부품에 대한 발사시 열해석)

  • Choi, Joon-Min;Kim, Hui-Kyung;Hyun, Bum-Seok
    • Proceedings of the KSME Conference
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    • 2003.11a
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    • pp.163-168
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    • 2003
  • Analytical approach is applied to predict temperature of satellite box under worst hot condition from fairing jettison to separation. The box is tried to solve analytically which is exposed to known environmental heating condition and has internal heating and irradiation to space. For a single thermal mass, governing equation for temperature is simplified to 1st order ordinary differential equation(ODE) by several assumptions. Two cases are considered. The one is for constant mass box and the other is for mass-varying box. Each case has three different analytical solution by sign of constant term in ODE. One analytical solution for constant mass is applied to physical launch stage condition. It is concluded that the present analytical method can be used to quick predict the temperature of a satellite box and check whether a satellite is safe against space environment during launch stage.

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Simple and Accurate Analytical Model for Predicting Cyclic Behavior of Rectangular Steel HSS Braces (간략하고 정확한 장방형 각형강관 가새부재 이력거동 예측 위한 해석모델)

  • Han, Sang Whan;Sung, Min Soo;Mah, Dongjun
    • Journal of the Earthquake Engineering Society of Korea
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    • v.21 no.3
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    • pp.145-152
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    • 2017
  • The objective of this study is to propose a simple and accurate analytical model for HSS braces. For this purpose, a physical theory model is adopted. Rectangular hollow section steel (HSS) braces are considered in this study. To accurately simulate the cyclic behavior of braces using the physical theory model, empirical equations calculating constituent parameters are implemented on the analytical model, which were proposed in the companion paper. The constituent parameters are cyclic brace growth, cyclic buckling load, and the incidence of local buckling and fracture. The analytical model proposed in this study was verified by comparing actual and simulated cyclic curves of brace specimens. It is observed that the proposed model accurately simulates the cyclic behavior of the braces throughout whole response range.

Analytical Solution for Flow Field by Arbitrarily-Located Multi Injection-Pumping Wells

  • Yoo, In-Wook;Lee, Kang-Kun
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2001.09a
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    • pp.79-82
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    • 2001
  • Analytical solutions have been derived to delineate the capture zone created by pumping wells for the remediation design of contaminated groundwater. These previous analytical solutions are often restricted to pumping wells only, specific well locations, a limited number of wells, and an isotropic aquifer. Analytical solution was developed to deal with arbitrarily located multi injection-pumping wells in an anisotropic homogeneous aquifer. The solution presented in this study provides a simple, easy method for determining tile complex flow field caused by multi injection-pumping wells at different rates, and will consequently be useful in pump-and-treat design.

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