• Title/Summary/Keyword: Analytical Analysis

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Development and Verification of Analytical Model of a Main Control Valve (메인 컨트롤밸브의 해석모델 개발 및 검증)

  • Kim, D.M.;Lee, J.M.;Jung, W.J.;Jang, J.S.
    • Journal of Drive and Control
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    • v.12 no.2
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    • pp.39-48
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    • 2015
  • In order to control the actuators of hydraulic machinery such as excavators, various control valves are typically assembled in a single block. Such a control block is called a main control valve(MCV). In this paper, we analyzed the working principle and the particular purpose of the design of all valves included in the MCV system. To Examine the reliability of the analysis model, the pressure drop of the MCV at each port was measured. The authors developed an analytical model of the control valve(main spool, load poppet, pressure relief, make up, and regeneration). The authors considered the notch shape of the spool while developing the analytical models of the main spool valve. Most importantly, at the stage before the analysis model was applied in the design tuning, the reliability was ensured by comparing the analysis results with the test results. This paper showed a process of developing an analysis model that can be utilized in the design and tuning stages.

Analysis of Trace Elements in Mud Flat with Neutron Activation Analysis (NAA) and Atomic Spectroscopy (중성자 방사화 분석법과 원자 분광법을 이용한 갯벌 시료 중 미량원소 분석법에 관한 연구)

  • Nam, Sang-Ho;Kim, Min-Jae;Chung, Yong-Sam;Kim, Sun-Ha
    • Analytical Science and Technology
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    • v.15 no.6
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    • pp.521-528
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    • 2002
  • Neutron Activation Analysis (NAA) and Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) have been applied for the determination of inorganic elements in mud flat of south seaside in Korea. The analytical results of Al, Ca, Fe, Mg, K and Na by NAA were compared with those by ICP-AES. The results show that NAA is superior to ICP-AES for the determination of minor elements in sediment. Accordingly, NAA will play an important role in the analysis of environment samples such as mud flat and sediment having complex matrix.

Torque Prediction of Ball Bearings Considering Cages using Computational Fluid Dynamics (전산유체역학을 이용한 케이지가 고려된 볼 베어링의 토크 예측)

  • Jungsoo Park;Jeongsik Kim;Seungpyo Lee
    • Tribology and Lubricants
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    • v.40 no.1
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    • pp.1-7
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    • 2024
  • Ball bearings are a major component of mechanical parts for transmitting rotation. Compared to tapered roller bearings, ball bearings offer less rolling resistance, which leads to reduced heat generation during operation. Because of these characteristics, ball bearings are widely used in electric vehicles and machine tools. The design of ball bearing cages has recently emerged as a major issue in ball bearing design. Cage design requires pre-verification of performance using theoretical or experimental formula or computational fluid dynamics (CFD). However, CFD analysis is time-consuming, making it difficult to apply in case studies for design decisions and is mainly used in performance prediction following design confirmation. To use CFD in the early stages of design, main-taining analytical accuracy while reducing the time required for analysis are necessary. Accordingly, this study proposes a laminar steady-state segment CFD technique to solve the problem of long CFD analytical times and to enable the use of CFD analysis in the early stages of design. To verify the reliability of the CFD analysis, a bearing drag torque test is performed, and the results are compared with the analytical results. The proposed laminar steady-state segment CFD technique is expected to be useful for case studies in bearing design, including cage design.

Application of Laser-Induced Breakdown Spectroscopy (LIBS) for In-situ Detection of Heavy Metals in Soil (토양내 중금속 실시간 탐지를 위한 레이저 유도붕괴 분광법의 활용에 대한 소개)

  • Ko, Eun-Joung;Hamm, Se-Yeong;Kim, Kyoung-Woong
    • Economic and Environmental Geology
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    • v.40 no.5
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    • pp.563-574
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    • 2007
  • Laser induced breakdown spectroscopy (LIBS) is a recently developed analytical technique that is based upon the measurement of emission lines generated by atomic species close to the surface of the sample, thus allowing their chemical detection, identification and quantification. With powerful advantages of LIBS compared to the conventional analytical methodology, this technique can be applied in the detection of heavy metals in the field. LIBS allows the rapid analysis by avoiding laborious chemical steps. LES have already been applied for the determination of element concentration in a wide range of materials in the solid, liquid and gaseous phase with simplicity of the instrument and diversity of the analytical application. These feasibility of rapid multi elemental analysis are appealing proprieties for the in-situ analytical technique in geochemical investigation, exploration and environmental analysis. There remain still some limitations to be solved for LIBS to be applied in soil environment as an in-situ analytical technology. We would like to provide the basic principle related to the plasma formation and laser-induced breakdown of sample materials. In addition, the matrix effect, laser properties and the various factors affecting on the analytical signal of LIBS was dealt with to enhance understanding of LIBS through literature review. Ultimately, it was investigated the feasibility of LIBS application in soil environment monitoring by considering the basic idea to enhance the data quality of LIBS including the calibration method for the various effects on the analytical signal of LIBS.

A Study on Counseling Process and Counseling Techniques Applying Analytical Psychology (분석심리학을 적용한 상담과정과 상담기법에 관한 연구)

  • Park, Won-Jin;Kim, Bo-Ki
    • Industry Promotion Research
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    • v.4 no.1
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    • pp.67-78
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    • 2019
  • This study is to study Jung's analytical psychology and to study counseling process and counseling techniques based on the counseling theory derived from it. Jung divides the counseling process into four stages based on analytical psychology. The first stage is confession, and the prototype of analysis therapy is confession. The first step in the treatment process is to share secrets and reveal suppressed emotions. The second stage is elucidation, a process that clarifies by shedding light on the contents induced by the transfer. The third stage is the level of education. Explanation makes my counselors intelligent, but leaves them still in an incompetent state. At this stage, treatment goes beyond insight to train as a responsible client. The fourth stage is transformation. In the transformation phase with inner counselors, not only the debaters, but also the therapist is in the "in-analysis." Jung's counseling technique uses six things: dream analysis, use of symbols, word link test, symptom analysis, case history and MBTI. In conclusion, analytical psychology counseling has enabled, first, a more in-depth approach and understanding of the human mind, especially the unconscious world. Second, analytical psychology counseling has enabled us to recognize that all humans are human communities with a common mental structure through the concept of unconsciousness and archetypes. Third, analytical psychology counseling has allowed you to look at the meaning and purpose of life from a new perspective. Therefore, Jung emphasized that he should not be seen as having a pathological problem with patients, but as an omnipotent human being who wants to realize its fullness on his own.

Structural Equation Modeling Using R: Mediation/Moderation Effect Analysis and Multiple-Group Analysis (R을 이용한 구조방정식모델링: 매개효과분석/조절효과분석 및 다중집단분석)

  • Kwahk, Kee-Young
    • Knowledge Management Research
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    • v.20 no.2
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    • pp.1-24
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    • 2019
  • This tutorial introduces procedures and methods for performing structural equation modeling using R. To do this, we present advanced analysis methods based on structural equation model such as mediation effect analysis, moderation effect analysis, moderated mediation effect analysis, and multiple-group analysis with R program code using R lavaan package that supports structural equation modeling. R is flexible and scalable, unlike traditional commercial statistical packages. Therefore, new analytical techniques are likely to be implemented ahead of any other statistical package. From this point of view, R will be a very appropriate choice for applying new analytical techniques or advanced techniques that researchers need. Considering that various studies in the social sciences are applying structural equations modeling techniques and increasing interest in open source R, this tutorial is expected to be useful for researchers who are looking for alternatives to existing commercial statistical packages.

Development Rapid Analytical Methods for Inositol as a Trace Component by HPLC and LC-MS/MS in Infant Formula

  • Shin, Jin-Ho;Park, Jung-Min;Kim, Ha-Jung;Ahn, Jang-Hyuk;Kwak, Byung-Man;Kim, Jin-Man
    • Food Science of Animal Resources
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    • v.35 no.4
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    • pp.466-472
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    • 2015
  • A rapid and simple analytical method, using liquid chromatography tandem mass spectrometry (LC-MS/MS), was developed to detect myo-inositol (MI) in infant formulas. For protein removal: acid hydrolysis and lipid removal through organic solvent extraction. The operating conditions for instrumental analysis were determined based on previously reported analogous methods that used LC-MS/MS. Quantitative analysis was used for the detection limit test, infant formula recovery test, and standard reference material (SRM) 1849a to verify the validity of our LC-MS/MS analytical method, which was developed to quantify MI. For validation, the results of our method were compared with the results of quantitative analyses of certified values. The test results showed that the limit of detection was 0.05 mg/L, the limit of quantitation was 0.17 mg/L, and the method detection limit was 17 mg/kg. The recovery test exhibited a recovery between 98.07-98.43% and a relative standard deviation between 1.93-2.74%. Therefore, the result values were good. Additionally, SRM 1849a was measured to have an MI content of 401.84 mg/kg and recovery of 98.25%, which is comparable to the median certified value of 409 mg/kg. From the aforementioned results, we judged that the instrumental analysis conditions and preparation method used in this study were valid. The rapid analytical method developed herein could be implemented in many laboratories that seek to save time and labor.

Study on the analytical method using GC-MS for the accident preparedness substances (실험실 GC-MS를 이용한 사고대비물질 분석방법 연구)

  • Kim, Kijoon;Lee, Jinseon;Lee, Suyeong;Hwang, Seungryul;Kim, Younghee;Seok, Gwangseol
    • Analytical Science and Technology
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    • v.26 no.1
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    • pp.80-85
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    • 2013
  • The sixty nine accident preparedness substances (APS) having high probability of chemical accident are controlled under the Toxic Chemicals Control Act (TCCA). Around the world, there has been a growing interest in the analysis of chemical warfare agent (CWAs). When a chemical accident occurs, it is generally required to detect and identify APS. However, the quantitative analytical data remain limited in Korea. In this study, an analytical method using GC/MS for volatile organic chemicals was established and a quantitative analysis method was studied. The calibration curve for 25 chemicals were obtained and 21 chemicals showed higher coefficient of determination ($r^2$ >0.998).

Study of the hydrogen concentration of SiNx film by Fourier transform infrared spectroscopy (Fourier transform infrared spectroscopy를 이용한 SiNx박막의 수소농도 연구)

  • Lee, Seok-Ryoul;Choi, Jae-Ha;Jhe, Ji-Hong;Lee, Lim-Soo;Ahn, Byung-Chul
    • Journal of the Korean Vacuum Society
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    • v.17 no.3
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    • pp.215-219
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    • 2008
  • The bonding structure and composition of silicon nitride (SiNx) films were investigated by using Fourier transform infrared spectroscopy (FT-IR). SiNx films were deposited on Si substrate at $340^{\circ}C$ using a conventional PECVD system. The compositions of Si and N in SiNx films were confirmed by using Rutherford backscattering spectroscopy (RBS) and photoluminescence (PL) analysis. The surface morphology of SiNx films was also analyzed by using atomic force microscopy (AFM). It was found that the contents of NH(at. %) is the reverse related with those of SiH corresponding to the result of FT-IR. we conclude that a quantitative analysis on SiNx films can be possible through a precise detection of the contents of H in SiNx films with a FT-IR analysis only.

Determination of Inorganic Elements in Women Blood Serum using Instrumental Neutron Activation Analysis (중성자방사화분석법을 이용한 성인여성 혈청중의 무기 원소 분석)

  • Moon, Jong-Hwa;Chung, Yong-Sam;Lee, Ok-Hee
    • Analytical Science and Technology
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    • v.15 no.6
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    • pp.509-513
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    • 2002
  • In this study, instrumental neutron activation analysis was used to assess the concentration level of inorganic trace elements in Korean women blood serum. It was found out that high concentration of Na and Cl incurs analytical interference, but 12 elements of Br, Ca, Cl, Co, Cr, Cs, Fe, K, Na, Rb, Se, Zn can be determined under the condition of interference minimization. Serum samples collected from 63 women were analyzed and the concentration level and range of the elements were evaluated. NIST SRMs were analyzed simultaneously for analytical quality control. The average values of Na and Cl determined in serum samples are around 3000 mg/L, Ca is 100 mg/L and K is 200 mg/L. Besides, Br, Se and Zn have concentration level of 6.0, 0.1 and 1.0 mg/L, respectively. It was found that there is no significant difference between the present values and reported values.