• 한국세라믹학회지
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• 제54권2호
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• pp.108-113
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• 2017

The use of aluminum-based coagulants in water pretreatment is being carefully considered because aluminum exposure is a risk factor for the onset of Alzheimer's disease. Lightly burned-dolomite kiln dust (LB-DKD) was evaluated as an alternative coagulant because it contains high levels of the healthful minerals calcium and magnesium. An organic pore forming agent (OPFA) was incorporated to prepare porous granules after OPFA removal through a thermal decomposition process. A spray drying method was used to produce uniform and reproducible spherical granules with low density, since fine dolomite particles have irregular agglomeration behavior in the hydration reaction. The use of fine dolomite powder and different porosity granules led to a visible color change in raw algae (RA) containing water, from dark green to transparent colorlessness. Also, dolomite powders and granules exhibited a mean removal efficiency of 48.3% in total nitrogen (T-N), a gradual increase in the removal efficiency of total phosphorus (T-P) as granule porosity increased. We demonstrate that porous dolomite granules can improve the settling time and water quality in summer seasons for the emergent treatment of excessive algal blooms in eutrophic water.

• 자원리싸이클링
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• 제26권3호
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• pp.39-46
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• 2017

탄소환원질화법을 이용하여 질화알루미늄(Aluminum Nitride: AlN)을 제조하는 연구를 실험실 규모로 수행하였다. 고품위 알루미나 분말과 탄소(carbon black)를 배합하여 흑연 도가니에 장입하고, 노내 분위기를 진공으로 한 다음 질소 가스를 흘려주어 온도($1,600{\sim}1,700^{\circ}C$), 시간(0.5~6 hr), $N_2$유량($4.7{\times}10^{-6}{\sim}20{\times}10^{-6}m^3/sec$), 장입 시료층 높이(0.5~20 mm)를 변화시키면서 AlN을 합성하였다. 실험결과, 고순도 알루미나와 탄소 혼합물을 질소 분위기의 $1600{\sim}1700^{\circ}C$ 온도 범위에서 반응시킬 때 반응 온도가 높을수록 생성된 AlN의 1차 입자 크기가 커지고, 반응 활성화 에너지는 382 kJ/mol로 화학 반응이 율속 단계로 판단되었다. 시험 제조한 AlN들의 산소 함량은 0.71~0.96 wt%였고, 질소는 30.7~35.1 wt%로서 상용 제품과 근접한 결과를 나타내었다.

• 폴리머
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• 제38권6호
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• pp.782-786
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• 2014

세라믹 방열 복합체의 특성 비교를 위해 casting method로 제작하였으며, 이들의 광학적 이미지와 단면 FE-SEM 분석을 실시하였다. 각각의 복합체의 열전도성 특성을 비교 분석하였으며, silicon carbide(SiC)의 분산도 문제를 해결하기 위해 wetting process를 도입하여 SiC/epoxy 복합체를 제작하였다. 기존의 방법에서 발견된 복합체 내공극과 분산도 문제가 wetting process를 통해 향상되었으며, 충전제 함량에 따른 열전도성 특성을 분석하였다. SiC 복합체의 함량에 따른 공극률 해석을 통해 70 wt% SiC 복합체에서 가장 높은 열전도도 값을 보였으며, 이들의 단면 FE-SEM 분석을 통해 복합체 내의 충전제 분산도를 확인하였다.

• 한국자기학회지
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• 제4권1호
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• pp.25-31
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• 1994

코발트와 철의 이온을 혼합한 산성수용액 중에서, 알루미늄 양극산화피막에 전해석출 하여 제작된 자성막은, 코발트조성이 증가함에 따라 발크합금의 경우와 마찬가지로 상전이(phase shifting) 하였다. 입자직경이 $150\;{\AA}$의 시료의 경우 조성이 25-35 at% Co에서 큰 포화자화, 고항자력, 큰 자기이방성 에너지 및 우수한 각형비 등에 기인하는 큰 자기에너지 적($BH_{max}$)이 얻어진다. 그러나 입자직경이 $450\;{\AA}$의 경우에는, 코발트가 50-70 at% 일때 초기석출부 에 강자성체인 FeC가 아주 강하게 배향하므로, 입자의 큰 형상이방성(수직자기이방성)이 없어지고 면내 방향의 자기이방성을 나타낸다. 그리고 같은 조성에서 초기석출부를 제거하여 FeC의 영향을 없앨때, 주직자기이방성이 회복되었다.

• Advances in materials Research
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• 제12권4호
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• pp.263-271
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• 2023

In this study, AA1060/Alumina composites were fabricated by combined stir casting and accumulative press bonding (APB). The APB process was repeated up to six press bonding steps at 300Ċ. As the novelty, potential dynamic polarization in 3.5Wt% NaCl solution was used to study the corrosion properties of these composites. The corrosion behavior of these samples was compared and studied with that of the annealed aluminum alloy 1060 and versus the number of APB steps. So, as a result of enhancing influence on the number of APB process, this experimental investigation showed a significant enhancement in the main electrochemical parameters and the inert character of the Alumina particles. Together with Reducing the active zones of the material surfaces could delay the corrosion process. Also, at higher number of steps, the corrosion resistance of composites improved. The sample produced after six number of steps had a low corrosion density in comparison with high corrosion density of annealed specimens. Also, the scanning electron microscopy (SEM), was used to study the corrosion surface of samples.

• 대한기계학회논문집B
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• 제34권4호
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• pp.423-428
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• 2010

반도체 공정에서 배출되는 미세입자를 포집하기 위하여 전기집진장치가 적용되고 있으나, 배출가스 내 포함된 강부식성 오염원에 의한 전기집진장치 내부 오염 및 부식 문제가 심각하여, 이를 해결하기 위한 방안이 절실하다. 본 연구에서는 탄소섬유로 이루어진 하전부와 PET 필름 사이에 금속 박막이 삽입된 집진부로 이루어진 내부식 전기집진장치를 개발하여, 하전부 및 집진부 인가전압, 처리유량, 하전부 채널 수 등의 운전 조건에 따른 전기집진기의 초미세입자 집진 성능을 평가하였다. 평균입경이 100 nm인 KCl 입자를 시험입자로 사용하였으며, 전기집진기 전/후단 입자 농도 변화를 측정하기 위하여 SMPS를 사용하였다. 본 연구에서 개발된 9채널 하전부와 65 mm 집진부로 구성된 전기집진기의 성능평가 결과, $500\;m^3/hr$ 유량조건에서 하전부 및 집진부에 7 kV와 10 kV를 각각 인가하였을 때, 300 nm입자에 대한 포집효율이 90% 이상으로 높게 나타났다.

• 한국주조공학회지
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• 제14권3호
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• pp.240-247
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• 1994

TiC particulate reinforced magnesium matrix composites were fabricated by melt stirring method. The effect of alloying elements on TiC particulate dispersion into molten magnesium and mechanical properties were investigated. The incorporation time is defined as the time required for dispersion of solid particles into molten metal. The incorporation time of TiC particles into molten pure magnesium was remarkably shorter and the particulated dispersion was more uniform than that of pure aluminum which was reported previously. The incorporation time was, prolonged by the addition of Al, Bi, Ca, Ce, Pb, Sn or Zn. The tensile strength increased and elongation decreased by the addition of Cu or Sn into the matrices and composites. Although, the tensile strength of the matrices and composites increased by alloying with Ca or Ce, the maximum elongation was observed at a content of about 1% for the matrices. By alloying with Zn, the tensile strength increased for the matrices and composites, but the elongation of the matrices increased. The pure magnesium and its alloy matrix composites reinforced with 20vol% TiC have the tensile strength of about 400MPa. This value is compared with the tensile strength of SiC whisker reinforced magnesium matrix composites fabricated by liquid infiltration method at the same volume fraction. There fore, the melt strirring method which has the advantages of simple process is considered to be efficient in fabricating magnesium matrix composites.

• 한국환경보건학회지
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• 제38권2호
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• pp.128-135
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• 2012

Objectives: This study was aimed at determining the optimum coagulation dosage in a high turbid kaolin water sample using streaming current detection (SCD) as an alternative to the jar test. Methods: SCD is able to optimize coagulant dosing by titration of negatively charged particles. Kaolin particles were used to mimic highly turbid water ranging from 50 to 600 NTU, and polyaluminum chloride (PAC, 17%) was applied as a titrant and coagulant. The coagulation consisted of rapid stirring (5 min at 140 rpm), reduced stirring (20 min at 70 rpm), and settling (60 min). To confirm the coagulation effect, a jar test was also compared with the SCD titration results. Results: SCD titration of kaolin water samples showed that the dose of PAC increased as the pH rose. However, supernatant turbidity less than 1 NTU after coagulation was not achieved for high turbid water by SCD titration. Instead, a conversion factor was used to calculate the optimum PAC dosage for high turbid water by correlating a jar test result with that from an SCD titration. Using this approach, we were able to successfully achieve less than 1 NTU in treated water. Conclusions: For high turbid water influent in a water treatment plant, particularly during summer, the application of SCD control by applying a conversion factor can be more useful than a jar test due to the rapid calculation of coagulation dosage. Also, the interpolation of converted PAC dose could successfully achieve turbidity in the treated water of less than 1 NTU. This result indicates that an SCD system can be effectively used in a water treatment plant even for high turbid water during the rainy season.

• Composites Research
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• 제30권5호
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• pp.310-315
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• 2017

본 연구에서는 액상가압공정을 통해 고체적율의 SiC 입자가 균일 분산된 알루미늄 금속복합재료를 제조하고, 미세조직, 기계적 특성 및 내마모 특성에 대해 분석하였다. 입자크기가 다른 이종 SiC 입자가 약 60 vol.% 이상의 체적율로 균일하게 분산된 SiC/Al7075 복합재료는 단일 SiC 입자로 강화된 복합재료에 비해 체적율이 약 12% 이상 높았으며 압축강도가 200 MPa 이상 증가하였다. 내마모시험 결과 이종 SiC 입자 금속복합재료의 경우 마모너비와 깊이가 각각 $285.1{\mu}m$, $0.45{\mu}m$이며, 마찰계수는 0.16으로 내마모 특성이 가장 우수하였다.

• Tribology and Lubricants
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• 제26권1호
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• pp.7-13
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• 2010

This experimental study presents tribological characteristics under boundary lubrication contacts associated with electrorheolocal (ER) fluid. ER fluid is prepared by using phosphorated starch particles and silicone oil. Experimental apparatus of tribological tester is designed and constructed to evaluate tribological characteristics of pin specimens. Wear tests under boundary lubrication of ER fluid are experimentally performed under consideration of several operational factors such as normal load, sliding distance, sliding speed and specimen materials: steel, copper and aluminum. After wear test, microscopic surface changes of the worn pin specimens are analyzed in order to investigate measured wear characteristics by using the scanning electron microscope (SEM) as well as surface profilometer. In addition, the chemical wear characteristics are investigated by using energy dispersive x-ray spectroscopy (EDS). Moreover, friction coefficient measurements under different materials of pin specimens are conducted for the tribological investigations. In order to verify the effect of starch phosphate particles in ER fluid, the wear test results with ER fluid are compared with test results with only silicone oil. The results clearly present that the phosphorated starch based ER fluid shows the stabilized wear as well as friction characteristics after run-in operations, but the wear rate under ER fluid is increased.