• Title/Summary/Keyword: Aluminum particles

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Study on Tribological Behavior of Porous Anodic Aluminum Oxide with respect to Surface Coating (다공성 산화알루미늄의 표면코팅에 따른 트라이볼로지적 특성연구)

  • Kim, Young-Jin;Kim, Hyun-Joon
    • Tribology and Lubricants
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    • v.33 no.6
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    • pp.275-281
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    • 2017
  • In this work, we have fabricated anodic aluminum oxide (AAO) with ordered nanoscale porosity through an anodization process. We deposited gold and nano-organic thin films on the porous AAO surface to protect its structure and reduce friction. We investigated the tribological characteristics of the porous AAO with respect to the protective surface coatings using tribometers. While investigating the frictional characteristics of the samples by applying normal forces of the order of micro-Newton, we observed that AAO without a protective coating exhibits the highest friction coefficient. In the presence of protective surface coatings, the friction coefficient decreases significantly. We applied normal forces of the order of milli-Newton during the tribotests to investigate the wear characteristics of AAO, and observed that AAO without protective surface coatings experiences severe damage due to the brittle nature of the oxide layer. We observed the presence of several pieces of fractured particles in the wear track; these fractured particles lead to an increase in the friction. However, by using surface coatings such as gold thin films and nano-organic thin films, we confirmed that the thin films with nanoscale thickness protect the AAO surface without exhibiting significant wear tracks and maintain a stable friction coefficient for the duration of the tribotests.

Particle Behavior and Deformation During Compaction of Al Powder Using MPFEM (다입자유한요소법을 이용한 Al분말 압축공정에서 입자의 거동과 변형에 관한 연구)

  • Lee, Kyung-Hun;Lee, Jung-Min;Kim, Byung-Min
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.4
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    • pp.383-390
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    • 2010
  • This paper describes multiparticle finite element model (MPFEM)-based powder compaction simulations performed to demonstrate the densification of compacted aluminum powders. A 2D MPFEM was used to explore the densification of a collection of aluminum particles with different average particle sizes under various ram speeds. Individual particles are discretized using a finite element mesh for a detailed description of contact mechanics. Porous aluminum powders with average particle sizes of $20\;{\mu}m$ and $3\;{\mu}m$ were compressed uniaxially at ram speeds of 5, 15, 30, and 60 mm/min by using an MTS servo-hydraulic tester. The slow ram speed was of great advantage to powder densification in low compaction force due to sufficient particle rearrangement. Owing to a decrease in the average particle size of aluminum, the compaction force increased.

Effects of Aluminum Oxide Particles on the Erosion of Nozzle Liner for Solid Rocket Motors (고체 추진기관에서 산화알루미늄 입자가 노즐 내열재의 삭마에 미치는 영향)

  • 황기영;임유진;함희철
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.34 no.8
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    • pp.95-103
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    • 2006
  • The compositions, the gas properties in motor chamber and the aluminum oxide (Al2O3) particle size for two kinds of solid propellants with approximately 20% aluminum powder have been investigated. The SEM photographs of $Al_2O_3$ taken from nozzle entrance liner show that the aluminized PCP propellant with 47% volumetric fraction AP/HNIW and bimodal oxidizer 200-5 ${\mu}m$ can offer greater possibility for increasing aluminum agglomeration than the aluminized HTPB propellant with 64% volumetric fraction AP and trimodal oxidizer 400-200-6 ${\mu}m$. The nozzle entrance liner of solid rocket motor with the PCP propellant shows greater erosion at 4 circumferential sections in line with grain slots due to the impingement of large particles, but that with the HTPB propellant shows uniform erosion with circumferential angle.

Effects of Ca on the Refinement of Microstructure in Aluminum B390 Alloy (알루미늄 B390합금의 조직미세화에 미치는 Ca의 영향)

  • Kim, Heon-Joo
    • Journal of Korea Foundry Society
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    • v.22 no.5
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    • pp.257-264
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    • 2002
  • Effects of Ca content on the refinement of primary Si of Aluminum B390 alloy have been examined. Ca was found to have an effect on the refinement of primary Si particle. Primary Si particle size has been refined as Ca content of the melts decreased and cooling rate increased. A control of Ca content by the addition of $CuCl_2$ to the melt was the most efficient in the refinement of primary Si particles. The minimum size of primary Si particles in this study was $15.0\;{\mu}m$ when a residual content of Ca element in the alloy was 5ppm, Primary Si particle size was refined as primary Si crystallization temperature increased, which was attributed to the decrease of Ca content in the melts.

DETERMINATION OF TRANSIENT WEAR DISTANCE IN THE ADHESIVE WEAR OF A6061 ALUMINIUM ALLOY REINFORCED WITH ALUMINA PARTICLES

  • Yang, L.J.
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.10b
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    • pp.217-218
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    • 2002
  • An integrated adhesive wear model was proposed to determine the transient wear and steady-state wear of aluminium alloy matrix composites. The transient wear volume was described by an exponential equation, while the steady-state wear was governed by a revised Archard equation, in which both the transient wear volume and transient sliding distance were excluded. A mathematical method was developed to determine both the transient distance and the net steady-state wear coefficient. Experimental wear tests were carried out on three types of commercial A6061 aluminum alloy matrix composites reinforced with 10%, 15% and 20% alumina particles. More accurate wear coefficient values were obtained with the proposed model. The average standard wear coefficient, as determined by the original Archard equation, was found to be about 51% higher.

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A Study on the Sintering and Mechanism of Crystallization Prevention of Alumina Filled Borosilicate Glass (알루미나를 충전재로 첨가한 붕규산염 유리의 소결 및 결정화 방지기구에 대한 연구)

  • 박정현;이상진;성재석
    • Journal of the Korean Ceramic Society
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    • v.29 no.12
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    • pp.956-962
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    • 1992
  • The predominant sintering mechanisms of low firing temperature ceramic substrate which consists of borosilicate glass containing alumina as a filler are the rearrangement of alumina particles and the viscous flow of glass powders. In this system, sintering condition depends on the volume ratio of alumina to glass and on the particle size. When the substrate contains about 35 vol% alumina filler and the average alumina particle size is 4 $\mu\textrm{m}$, the best firing condition is obtained at the temperature range of 900∼1000$^{\circ}C$. The extensive rearrangement behavior occurs at these conditions, and the optimum sintering condition is attained by smaller size of glass particles, too. The formation of cristobalite during sintering causes the difference of thermal expansion coefficient between the substrate and Si chip. This phenomenon degradates the capacity of Si chip. Therefore, the crystallization should be prevented. In the alumina filled borosilicate glass system, the crystallization does not occur. This effect may have some relation with aluminum ions in alumina. For aluminum ions diffuse into glass matrix during sintering, functiong as network former.

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Composite Structures of $SiC_p$/6063 Aluminum Alloy by Rheo-Compocasting. (Rheo-Compocasting에 의한 $SiC_p$/6063 Al합금의 복합조직)

  • Choe, Jeong-Cheol
    • Journal of Korea Foundry Society
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    • v.10 no.4
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    • pp.309-315
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    • 1990
  • Aluminum alloy matrix composites reinforced by SiC particles were prepared by rheocompocasting, a process which consists of the incoporation and distribution of reinforcement by stirring within a semi-solid alloy. When the volume fraction of SiCp and stirring speed were fixed, the dispersion of SiCp in Al-matrix alloy depended on stirring time and solid volume fraction in slurry. The results were as follows : 1) As a dispersed SiCp during stirring at $647^{\circ}C$ in 6063-Al alloy, SiC was better dispersed than that other temperature, where solid volume fraction was 43% in slurry. 2) When increased solid fraction in slurry, rate of dispersing SiC increased during stirring and porosities decreased in matrix alloy after casting. 3) Inspite of stirring with 800rpm, since solid particles of matrix alloy in slurry joined each other and occured joining growth, so that SiC was not dispersed into solid particle.

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Recovery of ultrafine particles from Chemical-Mechanical Polishing wastewater discharged by the semiconductor industry

  • Tu, Chia-Wei;Wen, Shaw-Bing;Dahtong Ray;Shen, Yun-Hwei
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.715-718
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    • 2001
  • This study uses traditional alum coagulation and sedimentation process to treat CMP wastewater from cleaning after polishing. The primary goal is to successfully recycle both solid fines and water for semiconductor manufacturing. Results indicated that CMP wastewater may be successfully treated to recover clean water and fine particles by alum coagulation. The optimum operating conditions for coagulation are as fellowing: alum dosage of 10 ppm, pH at 5, rapid mixing speed at 800 rpm, 5 min rapid mixing time, and long slow mixing time. The treated water with low turbidity and an average residual aluminum ion concentration of 0.23 ppm may be considered for reuse. The settled sludge after alum coagulation contains mainly SiO$_2$particle with a minor content of aluminum (1.7 wt%) may be considered as raw materials for glass and ceramic industry.

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Effect of Annealing and Co contents on the Structural and Physical Properties in AlN Thin Films

  • Han, Chang-Suk;Han, Seung-Oh
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.6
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    • pp.331-337
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    • 2010
  • Aluminum nitride (AlN) thin films containing various amounts of Co content have been deposited by using a two-facing targets type sputtering (TFTS) system. The deposited films were also annealed successively and isothermally at different temperatures. Annealing treatment can control the physical properties as well as the microstructure of AlN films with Co particles. High magnetization and high resistivity are obtainable in AlN films containing dispersed Co particles. The coercivity of the films does not depend on annealing time, but it increases with increasing annealing temperature due to the increase of the grain size. A high saturation magnetization of 46 kG and resistivity of 2200 ${\mu}{\Omega}$-cm was obtained for AlN films containing 25 at% Co.

Life Prediction of Fatigue Crack Propagation and Nondestructive Evaluation in 5083 Aluminum Alloy (알루미늄 5083의 피로균열 진전에 따른 수명예측 및 비파괴평가)

  • 남기우
    • Journal of Ocean Engineering and Technology
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    • v.15 no.2
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    • pp.94-98
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    • 2001
  • fatigue life and nondestructive evaluation were examined experimentally using surface crack specimen and compact tension specimen of 5083 aluminium alloy. Acoustic emission signals emanated during failure of aluminum alloys has been the subject of numerous investigations. Possible sources of AE during deformation have been suggested as the dislocations, fracture of brittle particles and debonding of these particles from the alloy matrix. Fatigue life and penetration behavior of long surface crack can be evaluated quantitatively using K values proposed by authors. The influence of stress ratio on the frequency characteristics of AE signals were investigated.

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