• Title/Summary/Keyword: Aluminum hydroxide

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Effect of formalin killed vaccine of atypical Aeromonas salmonicida for black rockfish (Sebastes schlegeli) (조피볼락(Sebastes schlegeli)에 대한 비정형 Aeromonas salmonicida 포르말린 사균 백신의 효과)

  • Kim, Wi-Sik;Lee, Hyeon-Ho;Oh, Myung-Joo;Han, Hyun-Ja
    • Journal of fish pathology
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    • v.31 no.1
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    • pp.35-39
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    • 2018
  • Atypical furnculosis caused by atypical Aeromonas salmonicida, is an emerging problem of farming of rockfish (Sebastes schlegeli) in Korea. In this study, protection against atypical furunculosis was compared in rockfish vaccinated with A. salmonicida formalin killed cell (FKC) and adjuvant containing FKC. The formalin inactivated A. salmonicida vaccine provided a low protection of 20% and 10% relative percent survival (RPS) at 44 and 58 days post vaccination. However, addition of adjuvant (squalene and aluminum hydroxide) into inactivated A. salmonicida vaccine clearly enhanced the level of protection showing 70% and 50% RPS at 44 and 58 days post vaccination.

Study on Manufacture and Properties of Polymer Compounds for Cable Sheath (전선피복용 고분자 컴파운드의 제조 및 물성 연구)

  • Li, Xiangxu;Lee, Sang Bong;Cho, Ur Ryong
    • Journal of the Semiconductor & Display Technology
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    • v.18 no.1
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    • pp.42-47
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    • 2019
  • The four different polymer compounds were manufactured to make cable sheath for ship industry. Two kinds of ethylene-vinyl acetate (EVA) were selected as main matrix polymers for compounding with fire retardant, crosslinking agent, filler, plasticizer, and other additives. The properties of the four compounded materials were investigated with the contents of fire retardant, silane coated aluminum hydroxide (S-ATH). Rheology, Mooney viscosity, and tensile strength increased with S-ATH contents by reinforcing effect. With increasing fire retardant amount, fire resistance increased, but cold resistance didn't show an obvious enhancement due to polar effect of vinyl acetate in EVA.

Studies on the Surface Charge Characteristics and Some Physico-Chemical Properties of two Synthetic Iron Hydrous Oxides and one Aluminum Hydroxide Minerals (합성(合成) 수산화(水酸化) 철(鐵) 광물(鑛物)과 수산화(水酸化) 알루미늄 광물(鑛物)의 표면(表面) 전하(電荷) 및 물리화학적(物理化學的) 특성(特性)에 관(關)한 연구(硏究))

  • Lim, Sookil H.
    • Korean Journal of Soil Science and Fertilizer
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    • v.17 no.2
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    • pp.147-154
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    • 1984
  • Two Fe-hydrous oxide A,B and one Al-hydroxide minerals were synthesized precipitating Fe $Cl_3$ and $AlCl_3$ with alkali solution(NaOH) at pH 6.0, 12.0 and 4.5 respectively, for precise understanding of physico-chemical and surface charge characteristics of soils in which these minerals are dominant. Identification of these final products, effect of free and amorphous materials on X-ray diffraction analysis, particle size distribution and surface change characterics of these minerals were performed. Fe-hydroxide A and B were identified as great deal of X-ray amorphous material and as goethite with large amount of X-ray amorphous material, respectively. Dehydration by oven at $105^{\circ}C$ of these minerals exhibited akaganeite peaks with low X-ray amorphous hump and pure goethite peaks for Fe-hydroxide A and B, respectively. Both minerals, however, turned into hematite upon firing at $550^{\circ}C$. On the other hand, Al-hydroxide identified as mixture of gibbsite and bayerite of around 7:3 ratio. Application of sodium dithionite and ammonium oxalate solutions for removal of free or amorphous Fe and Al from these minerals revealed that only peak intensities of Al-hydroxide system were enhanced upon Al-extraction by oxalate solution even though dithionite solution was much powerful to extract Fe from Fe-hydrous oxide systems. Original(wet) Fe-hydrous oxide A has the highest specific surface and surface charge development(negative and positive), and the greatest amount of less than $2{\mu}m$ sized particles. Specific surface and clay sized particles(less than $2{\mu}m$) of Fe-hydrous oxide A, however, were drastically reduced upon dehydration($P_2O_5$ and oven drying) compare to the rest minerals. The Z.P.C. of these synthetic minerals were 8.0-8.5, 7.5-8.0 and 5.5-6.0 for Fe-hydrous oxide A, B and Al-hydroxide, respectively.

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Characterization of ZSM-5 Zeolite synthesized from Serpentine (사문석으로부터 합성된 ZSM-5 제올라이트의 특성분석)

  • Kim, Dong-Jin;Jeong, Heon-Saeng;Lee, Jae-Cheon;Kim, In-Hoe;Lee, Ja-Hyeon
    • Korean Journal of Materials Research
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    • v.10 no.3
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    • pp.191-198
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    • 2000
  • A serpentine mineral was treated in hydrochloric acid solution to obtain amorphous silica residue with high surface area. The highly porous silica with aluminum hydroxide and sodium hydroxide was hydrothermally reacted in an autoclave. A numerous experiments were performed in terms of reaction time, temperature, alkalinity, and calcinations temperature. As a result, a ZSM-5 zeolite of the highest crystallinity was produced under such conditions as $^170{\circ}C$ of the reaction temperature, 24 hours of the reaction time, and $11.7Na_2O{\cdot}Al_2O_3{\cdot}90SiO_2{\cdot}3510H_2O{\cdot}10.8(TPA)_2O$ the composition along with 3 hours of the calcinations at $600^{\circ}C$.

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Layered Metal Hydroxides Containing Calcium and Their Structural Analysis

  • Kim, Tae-Hyun;Heo, Il;Paek, Seung-Min;Park, Chung-Berm;Choi, Ae-Jin;Lee, Sung-Han;Choy, Jin-Ho;Oh, Jae-Min
    • Bulletin of the Korean Chemical Society
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    • v.33 no.6
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    • pp.1845-1850
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    • 2012
  • Layered metal hydroxides (LMHs) containing calcium were synthesized by coprecipitation in solution having two different trivalent metal ions, iron and aluminum. Two mixed metal solutions ($Ca^{2+}/Al^{3+}$ and $Ca^{2+}/Fe^{3+}$ = 2/1) were added to sodium hydroxide solution and the final pH was adjusted to ~11.5 and ~13 for CaAl-and CaFe-LMHs. Powder X-ray diffraction (XRD) for the two LMH samples showed well developed ($00l$) diffractions indicating 2-dimensional crystal structure of the synthesized LMHs. Rietveld refinement of the X-ray diffraction pattern, the local structure analysis through X-ray absorption spectroscopy, and thermal analysis also confirmed that the synthesized precipitates show typical structure of LMHs. The chemical formulae, $Ca_{2.04}Al_1(OH)_6(NO_3){\cdot}5.25H_2O$ and $Ca_{2.01}Fe_1(OH)_6(NO_3){\cdot}4.75H_2O$ were determined by inductively coupled plasma-atomic emission spectroscopy (ICP-AES). Particle morphology and thermal behavior for the synthesized LMHs were examined by field emission scanning electron microscopy and thermogravimetricdifferential scanning calorimetry.

Effect of Filter and Shrinkage Reducing Agent Influencing on Setting Shrinkage and Strength Properties of MMA-Modified Polymer Paste (충전재와 수축저감제가 MMA개질 폴리머 페이스트의 경화수축 및 강도특성에 미치는 영향)

  • Yeon, Kyu-Seok;Beck, Jong-Man;Jin, Xing-Qi;Lee, Chi-Won
    • Journal of the Korea Concrete Institute
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    • v.18 no.2 s.92
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    • pp.227-232
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    • 2006
  • This article presents the results of experimental study that investigates the effect of filler and shrinkage reducing agent influencing on the strength properties of MMA-modified polymer paste that was produced to develop the surface-repair and coating materials of the concrete structures. Results show that the flexural and compressive strengths of the polymer paste increased 29 and 27%, respectively, when the aluminum hydroxide completely replaced the calcium carbonate as the filler Furthermore, when the shrinkage reducing agent was used 30%, both strengths decreased about 29% comparing to when the agent was not used. As in the cases of flexural and compressive strengths, the adhesive strength increased as the content of aluminum hydroxide as the filler increased, and it decreased as the content of shrinkage reducing agent increased. The adhesive strength with a dry concrete substrate turned out to be $30{\sim}40%$ higher than that with a wet concrete substrate.

Sintered properties of silicon carbide prepared by using the alumina and yttria-coated SiC powder (알루미나 및 이트리아로 코팅된 분말을 사용하여 제조한 탄화규소의 소결물성)

  • Um, Ki-Young;Kim, Hwan;Kang, Hyun-Hee;Lee, Jong-Kook
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.4
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    • pp.645-650
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    • 1998
  • Alumina- and yttria-coated SiC powder was prepared by the surface-induced precipitation method, and sintered properties of silicon carbide prepared from this powder were investigated. After a well dispersion of SiC powders in the aqueous solution of $Al_2(SO_4)_3$ and $Y_2(SO_4)_3$, the mixed precursors of aluminum hydroxide, aluminum carbonate, yttrium hydroxide, and yttrium carbonate were precipitated on the surfaces of SiC particles through the hydrolysis reaction of urea. SiC specimens with alumina and yttria exhibit, 97.8% of theoretical density after the sintering at $1900^{\circ}C$ for 2 hrs. During annealing at $2000^{\circ}C$, $\beta$longrightarrow$\alpha$ phase transformation of SiC had taken place and resulted with a rodlike microstructure. Toughness of sintered SiC was enhanced by crack deflection around the rodlike grains. In case of annealing less than that of 3 hr, the fracture toughness of SiC was slightly improved with increasing the amount of sintering aid. However, annealed specimens for a long time showed constant fracture toughness even though the amount of sintering aid increased. It is resulted that the main factor for toughening in annealed SiC for a long time is the pullout effect of rodlike grains during the propagation of cracks, and the amount of sintering aids is less effective on the fracture toughness of SiC.

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Membrane fouling reduction using electro-coagulation aided membrane bio-reactor (전기응집 분리 막 생물반응기의 막 오염 저감)

  • Kim, Wan-Kyu;Hong, Sung-Jun;Chang, In-Soung
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.8
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    • pp.105-114
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    • 2018
  • Membrane fouling in EC-MBR (Electro-Coagulation aided Membrane Bio-Reactor) processes was evaluated according to the operating parameters, such as current density and contact time. In addition, the fouling mechanism was investigated. Compared to the control (i.e., no electro-coagulation), membrane fouling for filtration of the activated sludge suspension after electro-coagulation was reduced significantly. Membrane fouling was improved further when the contact time was doubled under a low current density of $2.5A/m^2$. On the other hand, membrane fouling was not mitigated further, as expected, even though the contact time was doubled from 12 to 24 hr. at a current density of $10A/m^2$. This indicates that the overall decrease in membrane fouling is a function of the product of the current density and contact time. The particle size of the activated sludge flocs after electro-coagulation was changed slightly, which means that the membrane fouling reduction was not attributed to a larger particle size resulting from electro-coagulation. The experimental confirmed that the dynamic membrane made from aluminum hydroxide, Al(OH)3, and/or aluminum phosphate, Al(PO4), which had been formed during the electro-coagulation, played a key role on the reduction of membrane fouling. The dynamic membrane prevents the particles in the feed solution from deposition to the membrane pores and cake layers. Dynamic membrane formation as a result of electro-coagulation plays a critical role in the mitigation of membrane fouling in EC-MBR.

Sintering Characteristics of Si/SiC Mixtures from Si Waste of Solar Cell Industry (태양광(太陽光) 산업(産業)에서 발생(發生)하는 Si/SiC 혼합물(混合物)의 소결특성(燒結特性) 연구(硏究))

  • Kwon, Woo Teck;Kim, Soo Ryong;Kim, Younghee;Lee, Yoon Joo;Kim, Jong Il;Lee, Hyun Jae;Oh, Sea Cheon
    • Resources Recycling
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    • v.22 no.3
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    • pp.28-35
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    • 2013
  • The recycling of the Si/SiC mixture sludge obtained from solar cell industry is very significant, environmentally and economically. The sintering characteristics of Si/SiC mixture sludge was studied for the purpose of recycling. In this study, to understand sintering behavior, SiC content in the Si/SiC mixture was controlled using an air separator. Various Si/SiC mixtures having different SiC contents were sintered using carbon black, clay and aluminum hydroxide as sintering aids. Physical properties of Si/SiC mixture and sintered bodies have been characterized using SEM, XRD, particle size analyzer and apparent density measurement. SEM and particle size analysis result confirmed that the fine particles less than 1 ${\mu}m$ decreased or removed more effectively through the air separator in the case of 95% SiC sample compared than the case of 75% SiC sample or original SiC sample. Further, with addition of the Aluminum Hydroxide, ${\beta}$-cristobalite phase gradually decreased while mullite phase gradually increased. The addition of the carbon black improved the sintering characteristics.

Effects of Chemical Composition and Particle Size of Starting Aluminum Source on the Spheroidization in the Flame Fusion Process (화염용융법에 의한 구상 알루미나 제조에 미치는 초기 알루미나 원료의 화학조성과 입도의 영향)

  • Eom, Sun-Hui;Pee, Jae-Hwan;Lee, Jong-Keun;Hwang, Kwang-Taek;Cho, Woo-Seok;Kim, Kyeong-Ja
    • Journal of Powder Materials
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    • v.16 no.6
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    • pp.431-437
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    • 2009
  • Various inorganic fillers improve the thermal conductivity and physical properties of organic products. Alumina has been used a representative filler in the heat radiation sheet for the heat radiation of electric device. The high filling rate of alumina increases the thermal conductivity and properties of products. We successfully developed the spherical alumina by flame fusion process using the oxygen burner with LPG fuel. In the high temperature flame (2500$\sim$3000$^{\circ}C$) of oxygen burner, sprayed powders were melting and then rotated by carrier gas. This surface melting and rotation process made spherical alumina. Especially effects of chemical composition and particle size of stating materials on the melting behavior of starting materials in the flame and spheroidization ratio were investigated. As a result, spheroidization ratio of boehmite and aluminum hydroxide with endothermic reaction of dehydration process was lower than that of the sintered alumina without dehydration reaction.