• Title/Summary/Keyword: Alpha-particle

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Effect of the Process Parameters on the Fe Nano Powder Formation in the Plasma Arc Discharge Process (플라즈마 아크 방전법에서 Fe 나노 분말 형성에 미치는 공정변수의 영향)

  • 이길근;김성규
    • Journal of Powder Materials
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    • v.10 no.1
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    • pp.51-56
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    • 2003
  • To investigate the effect of the parameters of the plasma arc discharge process on the particle formation and particle characteristics of the iron nano powder, the chamber pressure, input current and the hydrogen volume fraction in the powder synthesis atmosphere were changed. The particle size and phase structure of the synthesized iron powder were studied using the FE-SEM, FE-TEM and XRD. The synthesized iron powder particle had a core-shell structure composed of the crystalline $\alpha$-Fe in the core and the crystalline $Fe_3O_4$ in the shell. The powder generation rate and particle size mainly depended on the hydrogen volume fraction in the powder synthesis atmosphere. The particle size increased simultaneously with increasing the hydrogen volume fraction from 10% to 50%, and it ranged from about 45nm to 130 nm.

Measurement of Detection Efficiency of Plastic Track Detector to ${\alpha}-particle$ (고체비적검출기의 알파선 검출효율 측정에 관한 연구)

  • Park, Young-Woong;Yang, Hyun-Soo
    • Journal of Radiation Protection and Research
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    • v.21 no.3
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    • pp.167-173
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    • 1996
  • The calibration method for the detection efficiency of solid state track detector to alpha is presented, and the detection efficiency of CN-85 and LEXAN to alpha is measured by this method. The results are 97% and 57% in CN-85 and LEXAN, respectively. The reason for a better result in CN-85 in not only the high sensitivity but also the low energy dependency with comparing for LEXAN. The peak detection efficiency is 3MeV and 1.8MeV in CN-85 and LEXAN, respectively.

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Effect of pH of Aluminum Hydroxides Gel Obtained by Hydrolysis of Al2(SO4)3 Solution on Crystal Growth of α−Al2O3 (Al2(SO4)3 용액의 가수분해에 의해 얻어진 Aluminum Hydroxides Gel의 pH가 판상 α−Al2O3의 결정성장에 미치는 영향)

  • Choe, Dong-Uk;Park, Byung-Ki;Han, Myung-Wan
    • Journal of the Korean Ceramic Society
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    • v.44 no.10
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    • pp.562-567
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    • 2007
  • To precipitate the complex gels of the pH 6, 7, 8, 9 included in a flux and an aluminum hydroxides gel, an aqueous solution of a mixture of $Na_2CO_3\;and\;Na_2PO_4{\cdot}12H_2O$ was added with stirring in an aqueous solution of a mixture of $Al_2(SO_4){_3}{\cdot}18H_2O,\;Na_2SO_4\;and\;K_2SO_4$, and then the complex gels were aged in 20 h at $90^{\circ}C$. As the hydrolysis pH changed, it had an effect on the physical properties such as the crystal structure, crystal morphology and a phase transition temperature of the AlO(OH) gel, and also on the crystal structure, crystal morphology, particle size and particle size distribution of the ${\alpha}-Al_2O_3$ platelets prepared by molten-salt precipitation. Also, in this study, the complex gels were crystallized at $1,200^{\circ}C$ and thereafter dried at $110^{\circ}C$, and then it was investigated to effect of the hydrolysis pH on the crystal structure, morphology and particle size distribution of the ${\alpha}-Al_2O_3$ platelets crystals using XRD, DTA, SEM and particle size analyzer.

Kinetics of Thermal Dehydration of Ha-dong Kaolin (하동카오린의 열분해속도에 관한 연구)

  • 박희찬;손명모
    • Journal of the Korean Ceramic Society
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    • v.18 no.1
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    • pp.35-40
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    • 1981
  • The kinetics of the dehydration of Ha-dong kaolin was studied isothermally at various temperatures. Dehydration rate was measured by thermogravimetry method in the temperature range of 440~50$0^{\circ}C$ and the particle size range of 170~325mesh. The general equation f($\alpha$)=kt, where $\alpha$ is the fraction reacted in the time and the function f($\alpha$) depends on the reaction mechanism, was applied to this reaction. The function, f($\alpha$) was obtained by application of reduced-time plot and plot of lnln (1-$\alpha$) vs. ln (time), and expressed as (1-$\alpha$) ln (1-$\alpha$)+$\alpha$=kt. The dehydration followed the diffusion-controlled reaction model and gave activation energy of 30Kcal/mole.

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Preparation of corundum ($\alpha$-Al_{2}O_{3}$) by hydrothermal growing process : I. A study on the effects of reaction temperature and seed crystal (수열성장법에 의한 코런덤($\alpha$-Al_{2}O_{3}$) 제조 : I. 반응온도와 종자결정의 영향에 관한 연구)

  • 반종성;이기정;서경원;목영일;이철경
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.6 no.2
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    • pp.129-140
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    • 1996
  • In this study, we have prepared corundum ($\alpha$-Al_{2}O_{3}$) single crystals from aluminum hydroxides by hydrothermal growing process and have investigated the reaction conditions. The hydrothermal conditions were mainly affected by reaction temperature, seed crystal and reaction time. Especially, seed crystal has strong effects on the particle size and crystallity of products. By adding seed crystal in Japanese gibbsite solution as the nutrient, hydrothermal reaction was performed for 2 hours at the reaction temperature of $460^{\circ}C$, to produce corundum powders which had weight mean particle diameter of $11\;\mu\textrm{m}$ with hexagonal crystal, Without adding seed crystal in Russian gibbstite solution, corundum powders that have weight mean particle diameter of $6\;\mu\textrm{m}$ with hexagonal crystals were also formed after 2 hours operation at the reaction temperature of $420^{\circ}C$.

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Influence of Rumen Escape Starch on α-Amylase Activity in Pancreatic Tissue and Small Intestinal Digesta of Lambs

  • Xu, M.;Yao, J.H.;Wang, Y.H.;Wang, F.N.
    • Asian-Australasian Journal of Animal Sciences
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    • v.19 no.12
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    • pp.1749-1754
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    • 2006
  • Two slaughter experiments were conducted to determine the effects of rumen escape starch, by altering dietary starch concentration and corn particle size, on ${\alpha}$-amylase activity in the pancreas and the small intestinal digesta of lambs. In experiment 1, 18 wether lambs (28.5${\pm}$1.6 kg) were fed low, medium or high starch diets for 35 d and slaughtered. Dietary starch concentrations linearly increased rumen escape starch (p<0.05). Pancreatic ${\alpha}$-amylase activity was lower (p<0.05) in lambs fed the low starch diet. When expressed per gram of digesta, ${\alpha}$-amylase activity was lower in lambs fed the low starch diet. However, expressed as total activity, ${\alpha}$-amylase in the digesta was greater in lambs fed the medium starch diet. In experiment 2, 12 wether lambs (23.5${\pm}$0.3 kg) were fed diets with finely cracked corn, coarsely cracked corn and whole corn. These dietary treatments continued for 35 d before tissue collection. Rumen escape starch increased with increasing corn particle size (p<0.05). ${\alpha}$-amylase activity in the pancreas and the small intestinal digesta was significantly greater (p<0.05) in lambs fed the coarsely cracked corn. These data suggest that increasing rumen escape starch results in a quadratic increase in total ${\alpha}$-amylase activity in the pancreas and the small intestinal digesta. Maximum ${\alpha}$-amylase activity is reached when rumen escape starch is about 100-120 g/d in 25-30 kg lambs.

Study on Catalytic Activity of the Selective CO Oxidation and Characterization Using $La_{0.5}Ce_{0.5}Co_{1-x}Cu_xO_{3-{\alpha}}$ Perovskite Catalysts ($La_{0.5}Ce_{0.5}Co_{1-x}Cu_xO_{3-{\alpha}}$ Perovskite촉매의 선택적 CO 산화반응 및 특성 분석에 관한 연구)

  • Sohn, Jung-Min
    • Transactions of the Korean hydrogen and new energy society
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    • v.18 no.2
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    • pp.116-123
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    • 2007
  • [ $La_{0.5}Ce_{0.5}Co_{1-x}Cu_xO_{3-{\alpha}}$ ](X=0, 0.1, 0.3, 0.5) perovskites were prepared by coprecipitation method at pH 7 or pH 11 and its catalytic activity of selective CO oxidation was investigated. The characteristics of these catalysts were analyzed by $N_2$ adsorption, X-ray diffraction(XRD), SEM, $O_2$-temperature programmed desorption(TPD). The pH value at a preparation step made effect on particle morphology. The smaller particle was obtained with a condition of pH 7. The better catalytic activity was observed using catalysts prepared at pH 7 than pH 11. The maximum CO conversion of 98% was observed over $La_{0.5}Ce_{0.5}Co_{0.7}Cu_{0.3}O_{3-{\alpha}}$ at $320^{\circ}C$. Below $200^{\circ}C$, the most active catalyst was $La_{0.5}Ce_{0.5}Co_{0.9}Cu_{0.1}O_{3-{\alpha}}$, of which conversion was 92% at $200^{\circ}C$. By the substitution of Cu, the evolution of ${\alpha}$-oxygen was remarkably enhanced regardless of pH value at preparation step according to $O_2$-TPD. Among the different ${\alpha}$-oxygen species, the oxygen species evolved between $400^{\circ}C$ and $500^{\circ}C$, gave the better catalytic performance for selective CO oxidation including $La_{0.5}Ce_{0.5}CoO_3$ in which Cu was absent.

A study on the Mechanical Properties of $Al_2O_{3(p)}$/LXA Composites by Melt-stirring Method (용탕교반법에 의한 $Al_2O_{3(p)}$/LXA복합재료의 기계적 성질에 관한 연구)

  • 이현규;공창덕
    • Journal of the Korean Society of Propulsion Engineers
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    • v.4 no.1
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    • pp.65-73
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    • 2000
  • Casting of metal matrix composites is an attractive process since it offers a wide selection of materials and processing conditions. Among the casting methods, melt-stirring technology is much attractive route in industrial application because it is more simple and inexpensive compared to squeeze casting or powder metallurgy. In the present work, effects of particle size, volume fraction of particles and mg addition on mechanical properties and thermal expansion coefficients of $\alpha$ -$Al_2O_{3(p)}$/LXA composites were studied. It is shown that $\alpha$ -$Al_2O_3$ particles formed at the interface of $\alpha$ -$Al_2O_3$ particles and matrix made an important role on mechanical properties. Ultimate tensile strength of most composite materials was not increased. But in the case of 5vol% addition of 16$\mu\textrm{m}$ $\alpha$ -$Al_2O_3$ Particle, Ultimate tensile strength of composite materials with 3wt.% Mg was increased. Volume fraction of reinforcements and mg content were thermal expansion coefficients of composite materials were decreased.

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$\alpha$-halo formation in semi-solid state processed hypereutectic Al-Si alloy (반고상 가공과 공정 Al-Si 합금에서 $\alpha$-halo의 형성)

  • 김인준;김도향
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1997.06a
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    • pp.183-195
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    • 1997
  • The micorstructural characteristics, particularly $\alpha$-halo formation, in semi-solid state processed hypereutectic Al-Si alloy was investigated. The microstructural changes during reheating of wedge type mold cast ingot, hot-rolled sheet, and Si particulate reinforced Al composite was compared with those occurred during stirring of semi-solid state hypereutectic alloy. In the case of semi-solid state reheating of wedge type ingot and hot-rolled sheet, fine particles of Si as well as $\alpha$-halo formed after heat treatment. Although there seemed to be no coarsening with variations of holding time, the region of $\alpha$-halo decreased due to homogenization. Nucleation and recrystallization was accelerated with the addition of alloying elements during hot rolling resulting in primary Si particle size decrease and $\alpha$-halo formation. In the case of extruded specimens, very little morphological change of reinforcing Si particles was observed. Almost no $\alpha$-halo formed during reheating because of the oxide film formed on the reinforcing Si particles which acted as a diffusion barrier between the matrix and the primary Si particles.

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211At and 211At-labeled radiopharmaceuticals for targeted alpha therapy

  • Kang, Choong Mo;Lee, Kyo Chul;Lee, Yong Jin
    • Journal of Radiopharmaceuticals and Molecular Probes
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    • v.4 no.2
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    • pp.99-105
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    • 2018
  • $^{211}At$ is an alpha emitting radionuclide, which can be produced using cyclotron with alpha beam. In addition, its strong linear energy transfer and iodine-like chemistry make that $^{211}At$ is one of the most attractive radionuclide in the field of targeted alpha therapy. In this review, production, labeling, and radiopharmaceuticals of $^{211}At$ will be discussed.