• Title/Summary/Keyword: Al-Si coating

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A Study on Ageing Characteristics of RTV Silicone Coating Materials by Corona Discharge (RTV 실리콘 코팅재의 코로나 방전 열화 특성)

  • 한세원;한동희;조한구
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.52 no.8
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    • pp.359-364
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    • 2003
  • Ageing characteristics of RTV coating materials by corona discharge have been studied. The hydrophobicity recovery of RTV coating materials with 300${\mu}{\textrm}{m}$ thickness was identical with a bulk silicone materials. The RTV coating materials hydrophobicity has been almost lost when its were discharged during 40 seconds by corona discharge of 10㎸, and recovered after about 45 hours. The resistivity of RTV coating materials has not been recovered after 45 hours, though after 80 hours the initiation resistivity value has been recovered up to 95%. There was no critical change of compounds(such as Si and Al) on RTV surfaces by the corona discharge treatment until 100 seconds. In the test of arc erosion, it was seen that the coating sample with silicone rubber as a base material have more longer burn-out time than other samples with FRP or glass base.

Effect of Al Alloy Composition on Physical and Crystallographical Properties of Plasma Electrolytic Oxidized Coatings I. Physical Properties of PEO Layer (플라즈마 전해 산화 코팅에 있어서 알루미늄 합금 모재 성분의 물리적, 결정학적 영향 I. PEO 층의 물성)

  • Kim, Bae-Yeon;Lee, Deuk-Yong;Kim, Yong-Nam;Jeon, Min-Seok;Song, Jun-Kwang;Kim, Sung-Youp;Kim, Kwang-Youp
    • Journal of the Korean Ceramic Society
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    • v.47 no.3
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    • pp.256-261
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    • 2010
  • Physical properties of Plasma electrolytic oxidized 8 different types of Al alloys, A-1100, A-2024, A-5052, A-6061, A-6063, A-7075, ACD-7B and ACD-12 were investigated. The electrolyte for PEO was $Na_2SiO_3$ solutions with NaOH and some alkali earthen metal salts. Porous layer near the surface of PEO coating was not found, and surface roughness Ra50 was below 2.5 ${\mu}m$. Surface roughness was affected by growth rate of plasma electrolytic oxidized layer, not by Si content in Al alloy.

Effect of Siliceous Slury Coating on Microstructure of Concrete under Damp Environment (규산질미분말혼합시멘트계도포방수재료가 습윤환경하의 콘크리트의 미세조직에 미치는 영향)

  • 오상근
    • Proceedings of the Korea Concrete Institute Conference
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    • 1992.10a
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    • pp.1-4
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    • 1992
  • This paper deals with the effect of siliceous slurry coating on concrete microstructure under damp environment. This material is mixed inorganic powder consisted of silica, cement and fine sand and water. Water pressure was given on the coated surface of concrete. for estimation on effect of siliceous slurry coating, microstructure of coated concrete was observed through SEM, and chemical components of crystals were analyzed with X-ray diffraction and EDX. A number of needle and fibrous crystals were produced in microstructure. And based on X-ray diffraction and EDX, needle crystal mainly consist of Al, Si, and Ca, and it is concluded to be ettringite. Fibrous crystals consist of Ca and Si, and it to be calcium silicate hydrate.

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Research on the Oxidation-Protective Coatings for Carbon/Carbon Composites

  • Li, He-Jun;Fu, Qian-Gang;Huang, Jian-Feng;Zeng, Xie-Rong;Li, Ke-Zhi
    • Carbon letters
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    • v.6 no.2
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    • pp.71-78
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    • 2005
  • Anti-oxidation coatings are the key technique for carbon/carbon (C/C) composites used as the thermal structural materials. The microstructure and oxidation behavior of several kinds of high-performance ceramic coatings for C/C composites prepared in Northwestern Polytechnical University were introduced in this paper. It showed that the ceramic coatings such as SiC, Si-$MoSi_2$, SiC-$MoSi_2$, $Al_2O_3$-mullite-SiC and SiC/yttrium silicate/glass coatings possessed excellent oxidation resistance at high temperatures, and some of these coatings were characterized with excellent thermal shock resistance. The SiC-$MoSi_2$ coating system has the best oxidation protective property, which can effectively protect C/C composites from oxidation up to 1973 K. In addition, the protection and failure reasons of some coatings at high temperature were also provided.

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Effect of Hot-stamping on Microstructures and Tensile Properties of Al-Si Coated Boron Steel Welds with Laser Source (Al-Si 도금된 보론강 레이저 소스에 따른 레이저 용접부의 미세조직과 기계적 성질에 미치는 핫스탬핑 처리의 영향)

  • Oh, Myeong-Hwan;Kong, Jong-Pan;Kwon, Min-Suck;Kang, Chung-Yun
    • Journal of Welding and Joining
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    • v.31 no.6
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    • pp.96-106
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    • 2013
  • In this study, the effect of laser source($CO_2$ and Nd:YAG) on the microstructure and tensile properties of laser welded Al-Si coated boron steel(1.2mmt) was investigated with before and after hot-stamping. In case of as welds condition, fracture occurred in base metal unrelated to the laser source. It could be explained that tensile strength of fusion zone composed of martensite and bainite is higher than that of base metal that contains a lot of ferrite despite dilution of Al and Si from coating layer to fusion zone. In case of hot-stamping condition, the fracture occurred in fusion zone irrelevant to laser source and the tensile strength was lower than hot stamped base metal. In the $CO_2$ laser welds, $Fe_3$(Al,Si) formed near the bond line was transformed into ferrite during hot-stamping. Therefore tensile strength of bond line is lower than that of base metal and center of fusion zone and the fracture occurred in the bond line. On the other hand, in the Nd:YAG laser welds, the higher concentration of Al formed the ferrite in the fusion zone during hot-stamping treatment. Also, the thickness of centerline was thinner than that of base metal. Therefore, it is considered that fracture occurred in centerline of fusion zone due to effect of concentration stress, and it leaded to a lower tensile strength and elongation.

Study on the Surface Properties of Arc Ion Plated Ti-Al-Cr-N Thin Layers (아크 이온 증착된 Ti-Al-Cr-N 도포층의 표면 물성 연구)

  • Gang, Bo-Gyeong;Choe, Yong;Gwon, Sik-Cheol;Zang, Shi-Hong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2015.05a
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    • pp.125-125
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    • 2015
  • Ti-Al-Cr-N thin layer was prepared on Fe-Si thin sheet by arc ion plating to improve corrosion and mechanical properties. The compositions ratios of Fe : Cr : Al : Ti : Si : N of the thin layers at $500^{\circ}C$ was 1.24 : 0.56 : 36.82 : 32.72 : 0.59 : 28.07 [wt.%], respectively. The higher arc ion plating temperature was, the higher corrosion resistance and nano-hardness were observed due to chromium content. Corrosion potential and corrosion rate in artificial sea water of the coating layer were in the range of $-39mV_{SHE}$ and $2mA/cm^2$, respectively. Passivity was not observed in the artificial sea water. Nano-hardnesses of the thin layers was increased by adding Cr from 23.6 to 25.8 [GPa]. The friction coefficients and fatigue limits of the layers were 0.388, 0.031, respectively.

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The In-situ Dressing of CMP Pad Conditioners with Novel Coating Protection

  • Sung, James-C.;Kan, Ming-Chi
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1142-1143
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    • 2006
  • Kinik Company pioneered diamond pad conditioners protected by DLC barrier ($DiaShield^{(R)}$ Coating) back in 1999 (Sung & Lin, US Patent 6,368,198). Kink also evaluated Cermet Composite Coating (CCC or $C^3$, patent pending) with a composition that grades from a metallic (e.g. stainless steel) interlayer to a ceramic (e.g. $Al_2O_3$ or SiC) exterior. The metallic interlayer can form metallurgical bond with metallic matrix on the diamond pad conditioner. The ceramic exterior is both wear and corrosion resistant. The gradational design of $C^3$ coating will assure its strong adherence to the substrate because there is no weak boundary between coating and substrate.

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Fabrication and Properties of $VF_2$-TrFE/Si(100) Structure by using Spin Coating Method (Spin Coating 법을 이용한 $VF_2$-TrFE/Si(100) 구조의 제작 및 특성)

  • Lee, Woo-Seok;Jeong, Sang-Hyun;Kwak, No-Won;Kim, Ga-Ram;Yun, Hyeong-Sun;Kim, Kwang-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.115-116
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    • 2008
  • The ferroelectric vinylidene fluoride-trifluoroethylene ($VF_2$-TrFE) and $Al_2O_3$ passivation layer for the Metal/Insulator/Ferroelectric/Semiconductor (MIFS) structure were deposited using spin coating and remote plasma atomic layer deposition (RPALD), respectively. A 2.5 ~ 3 wt % diluted solution of purified vinylidene fluoride-trifluoroethylene ($VF_2$: TrFE=70:30) in a DMF solution were prepared and deposited on silicon wafer at a optimized spin speed. After annealing in a vacuum ambient at 150 ~ $200^{\circ}C$ for 60 min, upper insulator layer were deposited at temperature ranging from 100 ~ $150^{\circ}C$ by RPALD. We described electrical and structural properties of MIFS fabricated by spin coating and RPALD methods.

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Properties of Polymethyl methacrylate (PMMA) for Polymer Gate Dielectric Thin Films Prepared by Spin Coating (Spin coating 공정을 이용한 Polymethyl methacrylate (PMMA) 박막의 polymer gate dielectric layer로써의 특성평가)

  • Na, Moon-Kyong;Kang, Dong-Pil;Ahn, Myeog-Sang;Myoung, In-Hye;Kang, Young-Taec
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.05b
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    • pp.29-32
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    • 2005
  • Poly (methyl methacrylate) (PMMA) is one of the promising representive of polymer gate dielectric for its high resistivity and sutible dielectric constant. PMMA (Mw=96700) films were prepared on p-Si by spin coating method. PMMA were coated compactively and flatly as observeed by AFM. MIS(Al/PMMA/p-Si) structure was made and capacitance-voltage (C-V) and current-voltage (I-V) measurements were done with PMMA films for different thermal treatment temperature. PMMA films were showed proper dielectric constant and breakdown voltage. Above the glass transition temperature PMMA films degraded. C-V measured at various frequencies, dielectric constant increased a little. The absence of hysteresis in the C-V characteristics, which eliminate the possibility of mobile charges in the PMMA films. The observed thermal stability, smooth surfaces, dielectric constant, I-V behavior implies PMMA formed by spin coating can be used as an efficient gate dielectric layer in OTFTs.

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Effects of Nitrate Electrolyte as the MAO process for Ceramic Coating treatments of AZ31 alloy (MAO법을 이용한 산화피막처리에서 질산염 전해액성분 첨가에 따른 AZ31합금의 표면코팅 특성)

  • Cho, Young-Hee;Jang, Kyong-Soo;Park, Sei-He;Lee, Ho-Jeong;Lee, Tae-Haeng
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.10
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    • pp.4365-4370
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    • 2012
  • AZ31 Mg alloy were coated by Macro Arc Oxidation(MAO) with 3 types of electrolyte and various coating times at 4A/$cm^2$. The Surface morphology of coatings became lager pores and surface crack initiated as the coating time increased. The thickness and micro-hardness of coatings increased as the coating time increased. also. The phase of coatings on AZ31 alloy consisted of MgO, $Mg_2SiO_4$ and $MgAl_2O_4$ oxides. The salt spray corrosion resistance of coated AZ31 alloys revealed excellent corrosion resistance in 5% NaCl solution for 168hr.