• 한국표면공학회지
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• 제24권4호
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• pp.179-186
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• 1991

The effects of silicone contents and flow rates(agitation rates) of electrolyte on the formation and mechanical properties of hard anodized film of Al-Si alloy have been studied in 12% H2SO4 + 1% Oxalic acid with varying the silicone contents in the rance of 0 to 11.6% and the flow rates of electrolyte in the range of 0 to 90cm/sec. The film forming voltage required to maintain an equivalent current density significantly increase with the silicone content of Al-Si alloys due to a low conductivity of silicone. Hardness and wear resistance of the anodized film of Al-Si alloys decreases wit increasing the silicone content. The increase in the flow rate of electrolyte has a similar influence on the formation and mechanical properties of anodized film as does the decrease in bath temperature. Hardness of anodized film is rapidly increased with the flow rate being increased from 10cm/sec. It is observed that the increase in the flow rate from 11cm/sec. It is observed that the increase in the flow from 11cm/sec to 48cm/sec is more effective in enhancing the hardness of film than is the decrease in bath temperature from 1$0^{\circ}C$ to $0^{\circ}C$.

• 한국주조공학회지
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• 제37권4호
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• pp.101-107
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• 2017

This study investigated the effect of Pd on the microstructure, tensile and creep properties of Mg-4Al-2Sn (AT42) alloy at a high temperature for transportation-related industrial applications. AT42-xPd (x = 0, 1 and 2 wt. %) alloys were prepared using a permanent mould casting method. The microstructures of the as-cast alloys were characterized by the presence of the intermetallic phases $Mg_{17}Al_{12}$, $Mg_2Sn$ and $Al_4Pd$. The addition of Pd was found to improve the tensile properties of AT42 at room and at elevated temperatures, and to increase the creep resistance at elevated temperatures. A small amount of Pd could markedly improve the tensile properties of AT42 by means of grain-refinement and the dispersion of secondary phase strengthening. Moreover, the thermally stable phase $Al_4Pd$ effectively improves the creep resistance of AT42 due to the strengthened grain boundaries and the suppressed formation of $Mg_{17}Al_{12}$.

• 동력기계공학회지
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• 제7권3호
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• pp.74-79
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• 2003

Alumina($Al_2O_3$) and Al 6061 were brazed by using Al-12wt% Si filler metal in a high vacuum environment. The interfacial microstructure and mechanical properties of the joints were investigated. The results obtained were as follows. (1) The maximum tensile strength of 54Mpa was acquired at the processing conditions of high vacuum ($3{\times}10^{-6}Torr$), $620^{\circ}C$ and 10min, but this condition will not be used in the industrial area due to high evaporation of Al alloy composition. (2) Reaction products for holding time and brazing temperature worked as stress relieve layer and the fractures after the mechanical properties test were occurred to the ceramic side or reaction layer. (3) The glancing angle X-ray diffraction analysis for the reaction product of $Al_2O_3/Al$ 6061 were processed. the joint strengths were low due to existed $Al_2Si_5\;and\;SiO_2$.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2000년도 춘계학술강연 및 발표대회 강연 및 발표논문 초록집
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• pp.16-16
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• 2000

분무주조법으로 제조된 Al-25Si-(Fe,V) 합금빌렛의 미세조직을 광학현미경, 주사전자현미경, 투과전자현미경으로 분석하였으며, 빌렛내에서 관찰되는 2차상의 형성거동을 정확히 분석하기 위해 over-sprayed 분말의 미세조직을 분무주조 빌렛과 함께 관찰하였다. 먼저 분무주조 빌렛을 표면으로부터 중심부까지 관찰한 결과, 분무주조 빌렛의 미세조직은 표면부 10mm 가량을 제외하고는 매우 균일한 미세조직을 보여주었다. 이에 본 연구에서는 분무주조 빌렛의 표면부와 중심부, 그리고 over-sprayed 분말조직으로 구분하여 각각에서 관찰되는 2차상을 관찰하였으며, 이를 바탕으로 분무주조 빌렛내에 형성된 2차상의 형성기구를 규명하고자 하였다. Over-sprayed 분말의 미세조직은 기지조직내에 균일하게 분포된 침상의 $\delta$-AlFeSi 상과 각형의 Si 입자로 구성되어 있었다. 반면, 분무주조 빌렛의 경우, 그 중심부에서는 기자조직내에 균일하게 분포된 막대형의 $\beta$-AlFeSi과 부정형의 조대한 Si입자가 관찰되었으며, 표면부에서는 부정형의 Si 입자와 함께 막대형의 $\beta$-AlFeSi/$\delta$-AlFeSi 복합상이 관찰되었다. 특히, 빌렛 표면부의 $\beta$-AlFeSi 상과 $\delta$-AlFeSi 상간에는 일정한 방위관계가 존재하였으며, 이러한 결과는 분무주조 빌렛내에 분포된 $\beta$-AlFeSi상들이 분무액적내에 형성된 준안정 $\delta$-AlFeSi 상으로부터 상분해되어 형성되었음을 제시한다. 이상의 분무주조 조직과 over-sprayed 분말의 미세조직으로부터 분무주조 빌렛의 최종 주조조직은 반응고상태의 분무액적 조직에 의해 지배됨을 알 수 있다.r plate)의 단면 미세조직 사진으로써 모재부와 오버레이충을 함께 보여주고 있다. 모재와 오버레이 충간의 경계면은 모재 일부가 용융된 후 웅고하면서 형성됨으로 인해서 도금이나 용사층과는 달리 매우 견고하게 결합되어 있다. 따라서 계면부의 탈락이라는 문 제점은 거의 없어 심한 응력을 받는 기계구조물 및 부품에도 본 기술은 널리 적용되고 있다. 그리고 사진 1에서 알 수 있는 바와 같이 모재와는 전혀 상이한 재료를 자유로이 선택하여 표면 유효층 일부만 오버레이시키며I 주조 및 단조가 불가능한 재료까지도 표면부에 오버레이 시킴으로 서 부품 및 설비의 제조에 있어 재료비의 절감과 제품의 수명이 획기적으로 개선될 수 있다. 그리고 최근에는 도금 빛 용사 둥과 같은 표면처리를 할 경우임의 소재 표면에 도금 및 용 사에 용이한 재료를 오버레이용접시킨 후 표면처리를 함으로써 보다 고품질의 표면층을 얻기위한 시도가 이루어지고 있다. 따라서 국내, 외의 오버레이 용접기술의 적용현황 및 대표적인 적용사례, 오버레이 용접기술 및 용접재료의 개발현황 둥을 중심으로 살펴봄으로서 아직 국내에서는 널리 알려지지 않은 본 기 술의 활용을 넓이고자 한다. within minimum time from beginning of the shutdown.및 12.36%, $101{\sim}200$일의 경우 12.78% 및 12.44%, 201일 이상의 경우 13.17% 및 11.30%로 201일 이상의 유기의 경우에만 대조구와 삭제 구간에 유의적인(p<0.05) 차이를 나타내었다.는 담수(淡水)에서 10%o의 해수(海水)로 이주된지 14일(日) 이후에 신장(腎臟)에서 수축된 것으로 나타났다. 30%o의 해수(海水)에 적응(適應)된 틸라피아의 평균 신사구체(腎絲球體)의 면적은 담수(淡水)에 적응된 개체의 면적보다 유의성있게 나타났다. 해수(海水)에 적응(適應)된 틸라피아의 신단위(腎單位)의 사

• 한국재료학회지
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• 제8권12호
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• pp.1127-1132
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• 1998

본 연구에서는 Al-10wt%Ti-4wt%Fe 복합재료를 in-situ공정으로 제조할 수 있는 가능성 및 2 원계 Al-10wt%Ti 복합재료의 낮은 기계적 성질(탄성계수, 상온 고온강도, 내마모특성 등)을 PM SiC/2124 복합재료 수준 흑은 그 이상으로 향상시킬 수 있는 가능성을 조사하였다. 제조된 Al-10wt%Ti-4wt%Fe 합금은 불연속 SiC 강화상으로 보강된 Al-기지 복합재료($SiC{w}$/2124)와 유사한 미세구조를 보여주었으며, 탄성계수 및 인장강도, 내마모성질 등의 기계적 특성이 2원계 Al-10%Ti 합금각 비교해 현저하게 향상되었음이 관찰되었다. 위의 결과는 초정 $Al_3Ti$상 외에도 Fe 원소의 첨가를 통한 추가적인 $Al_{x}Fe$의 분산강화 효과에 기인한 것으로 해석된다.

• 한국분말재료학회지
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• 제12권2호
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• pp.131-135
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• 2005

7xxx series Al alloy has the most attractive properties including its excellent high specific strength, stress corrosion cracking and corrosion-resistance. However, in case of the Al-Zn system, the liquid phase has a transient aspect because of the high solid solubility of Zn in Al. Therefore, transient liquid phase sintering behavior was observed during the sintering process. And the amount of liquid and its duration were influenced by the process variables including heating rate and final sintering temperature. At high heating rates($100^{\circ}C/min$), the liquid fraction increased during sintering because diffusion was minimized and therefore local saturation could easily occur. The sintered density increased with increasing heating rate.

• 한국세라믹학회지
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• 제47권4호
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• pp.283-289
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• 2010

Physical properties of Plasma electrolytic oxidized 8 different kinds of Al alloys, A-1100, A-2024, A-5052, A-6061, A-6063, A-7075, ACD-7B and ACD-12 were investigated. The electrolyte for PEO was $Na_2SiO_3$ and NaOH and some alkali earthen metal salts system solution. $\eta$-alumina, as well as $\gamma$-alumina, was main crystal phase, which were ever reported. Also, $Al_{4.95}Si_{1.05}O_{9.52}$ was found only in this research. So we can conclude that the process conditions of PEO apparatus and composition and concentration of its electrolyte affects crystal structure and physical properties of PEO layers much more than the compositions of Al alloy.

• 대한금속재료학회지
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• 제50권12호
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• pp.907-911
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• 2012

High purity silicon can be obtained from Al-Si alloys by a combination of solvent refining and centrifugation. Silicon purification by crystallization of silicon from an Al-Si alloy melt was carried out using 2N and 4N purity aluminum and 2N purity silicon as raw materials. The effect of the purity of raw materials on the final silicon ingot purity by centrifugation was investigated for an Al-50 wt% Si alloy. Alloys were melted using an electrical resistance furnace, and then poured into a centrifuging apparatus. A silicon lump like foam was obtained after centrifugation and was leached by an acid in order to get pure silicon flakes. Then silicon flakes were melted to make a silicon ingot using an induction furnace. The purities of the silicon flakes and silicon ingot were enhanced significantly compared to those of the raw materials of silicon and aluminum. The silicon ingot made of 4N aluminum and 2N silicon showed the lowest impurities.

• 대한금속재료학회지
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• 제56권11호
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• pp.805-812
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• 2018

High pressure die casting is one of the precision casting methods. It is highly productivity and suitable for manufacturing components with complex shapes and accurate dimensions. Recently, there has been increasing demand for efficient heat dissipation components, to control the heat generated by devices, which directly affects the efficiency and life of the product. Die cast aluminum alloys with high thermal conductivity are especially needed for this application. In this study, the influence of elements added to the die cast aluminum alloy on its thermal conductivity was evaluated. The results showed that Mn remarkably deteriorated the thermal conductivity of the aluminum alloy. When Cu content was increased, the tensile strength of cast aluminum alloy increased, showing 1 wt% of Cu ensured the minimum mechanical properties of the cast aluminum. As Si content increased, the flow length of the alloy proportionally increased. The flow length of aluminum alloy containing 2 wt% Si was about 85% of that of the ALDC12 alloy. A heat dissipation component was successfully fabricated using an optimized composition of Al-1 wt%Cu-0.6 wt%Fe-2 wt%Si die casting alloy without surface cracks, which were turned out as intergranular cracking originated from the solidification contraction of the alloy with Si composition lower than 2 wt%.

• 한국세라믹학회지
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• 제47권3호
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• pp.256-261
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• 2010

Physical properties of Plasma electrolytic oxidized 8 different types of Al alloys, A-1100, A-2024, A-5052, A-6061, A-6063, A-7075, ACD-7B and ACD-12 were investigated. The electrolyte for PEO was $Na_2SiO_3$ solutions with NaOH and some alkali earthen metal salts. Porous layer near the surface of PEO coating was not found, and surface roughness Ra50 was below 2.5 ${\mu}m$. Surface roughness was affected by growth rate of plasma electrolytic oxidized layer, not by Si content in Al alloy.