• 제목/요약/키워드: Agitation method and time

검색결과 51건 처리시간 0.03초

전기화학적 방법의 TRC(Total residual chlorine) 측정 연구(II: Pt전극 이용) (The Determination of TRC using an Electrochemical Method (II: Pt electrode))

  • 이준철;박대원
    • 한국물환경학회지
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    • 제30권3호
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    • pp.304-310
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    • 2014
  • The conventional methods for total residual chlorine such as iodometry and DPD colorimetric can cause secondary pollution due to additional agents, also have a wide error range. As for alternative, electrochemical method can measure TRC(Total residual chlorine), and is not required as additional agents, also very suitable for using the fields of ballast water because test time is relatively fast. Therefore, this study was investigated for changing charge by agitation, salt concentration, and temperature change. Charge showed differences based on changes of reduction peak with or without agitation. In contrast, TRC and charge were well correlated in constant agitation speed. As TRC and charge were analyzed with high correlations in constant salinity and temperature of ocean, thereby conductivity was firstly measured, and charge had high correlation for TRC in spite of changing salinity and temperature Pt electrode revealed high reliability ($r^2=0.960$) because it was rarely effected by TRC, On the other hand, Au electrode appeared inadequate ($r^2=0.767$) to use sensor in less than 1.0 ppm of TRC. For high accuracy and detection of TRC, Pt and Au electrodes for test time were, respectively, 14 and 22 seconds. As a result, Pt electrode was more valuable than Au electrode in terms of response time.

Dissolution Characteristics of ph-Dependent Antacid Granules Agglomerated in High Speed Agitation Type Speed Agitation Type Granulator

  • Choi, Woo-Sik;Lee, Jung-Sun
    • Archives of Pharmacal Research
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    • 제18권5호
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    • pp.314-319
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    • 1995
  • Antacid granules were prepared by agglomeration and powder method in high speed agitation type granulator. The copmositions of the test antacids were sodium bicarbonate nad magnesium carbonate nad a coating material was powder of polyvinylacetal diethyl-aminocacetate (AEA) and an additive material was talc powder. The dissolution characteristics of base from the antacid granules were investigated to evaluate neutralization capacity of hydrochloric profile of base and neutralization behavior, the following results were obtained : The prepared granules showed a pH-dependent dissolution pattern of a base. The dissolution profile of a base was varied with addition of talc powder as well as coating amount of AEA. The relationship between the ratio of dissolution retarded time for 20% and 10% AEA. The relationship between the ratio of dissolution retarded time for 20% AEA coated granules $\theta_{20}/\theta_{10}$ and the diameter reduction of the granules was explained by the rate process of neutralization of hydrochloric acid.

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pH, duty cycle, 교반, 첨가제가 Ni-TiO2 전기도금 복합체의 TiO2 공석특성과 열적안정성에 미치는 영향 연구 (A Study of pH, Duty Cycle, Agitation on the Property of Co-deposited TiO2 and Thermal Stability in the Electrodeposited Ni-TiO2 Composite)

  • 김명진;김정수;김동진;김홍표;황성식
    • 한국표면공학회지
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    • 제45권3호
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    • pp.97-105
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    • 2012
  • The effects of pH, types of applied current, agitation method and time, additive on the amount of co-deposited $TiO_2$ particles in the matrix were investigated. The deposition rates increased with increasing pH values, while the volume fraction of $TiO_2$ particles and the size of agglomerated $TiO_2$ particles in the composite decreased. The volume fraction of $TiO_2$ particles in the composite decreased when pulsed current of 50% duty cycle was used. And the size of agglomerated $TiO_2$ particles in the nickel matrix of pulsed current was smaller than that of DC current specimen. The volume fraction of $TiO_2$ particles in the matrix decreased with longer time by air agitation, but in case of using magnetic bar, volume fraction in the same range of time was relatively constant. The volume fraction of the electrodeposited Ni-$TiO_2$ composite in the solution containing 0.01 M Dimethylamine borane (DMAB) increased slightly with increasing agitation time regardless of agitation methods. Thermal stability of the electrodeposited Ni-$TiO_2$ composite increased with lower pH at the temperature range of $200{\sim}800^{\circ}C$, and the results showed that the amount of co-deposited $TiO_2$ relies more on the deposition rate than zetapotential of $TiO_2$ particles.

Laundering Factors in Soil Removal

  • Kadolph, Sara J.;Schofield-Tomschin, Sherryl A.;Kwon, Young-Ah
    • 한국의류산업학회지
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    • 제3권5호
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    • pp.455-465
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    • 2001
  • Assessing soil removal is of interest to the washing machine industry because of government-mandated energy savings and changes in detergent formulation and consumer laundry practices. We designed this study to examine the laundry process from a holistic perspective by integrating factors perceived to be of importance. Our purpose was to assess the impact of selected variables (fabric and soil type, wash temperature and time. detergent amount, and degree of agitation) on soil removal using accelerated laundry conditions. We used the Taguchi method to develop the research design and ANOVA to analyze the data. Although soil removal was affected by fabric type, soil type, type and amount of detergent, degree of agitation, wash time and temperature, and water hardness and volume, wash temperature was the most significant variable.

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Microencapsulation을 이용한 미립자 사료개발 (The Development of Microparticle Feed Using Microencapsulation)

  • 이은주;김성구
    • 생명과학회지
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    • 제6권2호
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    • pp.129-134
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    • 1996
  • The development of fish feed is essential to aquaculture. Recently, yeast, dhlorella and plankton have been studied and development as the feed of the fry fishes, But, these biological feeds cause the nutritional unbalance to fry fishes, rotifer or artemia. Therefore, to solve these problems, microcapsules with micron sizes were prepared for enhancing the nutritional values of artemia and rotifer which are used as the feed of fry fishes. Microparticle oil capsules were prepared by the complex coacervation technique. The method to make the optimal size of microcapsule which the artemia and rotifer can be easily taken was wvaluated. The size of oil microcapsule in the range of 5-70$\mu$m was obtained by the agitation conditions during coacervation. Capsule size and size distribution were dependent on the agitation speed and agitation time, respectively.

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새로운 도선감는 방법을 사용한 전기장을 이용한 스케일 제거 (Prevention of Particulate Scale with a new winding method in the Electronic Descaling Technology)

  • 김건우;안희섭;손창현
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2000년도 춘계학술대회논문집B
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    • pp.180-186
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    • 2000
  • This paper presents a new winding method in the electronic descaling(ED) technology. The ED technology Produces an oscillating electric field via the Faraday's law to Provide necessary molecular agitation to dissolved mineral ions. But present method gives another agitation force to mineral ions, which is Lorentz's force. Experiments were peformed at various Renolds number. A series of tests was conducted, measuring pressure drop across test section and the overall heat transfer coefficient as a function of time. In order to accelerate the rate of fouling, artificial hard water of 1000ppm $CaCO_3$ was used throughout the tests. The results show that the new method accelerates collision of mineral ions and improvs efficiency of system.

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Alginate Nanohydrogels Prepared by Emulsification-Diffusion Method

  • Lee, So-Min;Yoo, Eun-Soo;Ghim, Han-Do;Lee, Su-Jeong
    • Macromolecular Research
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    • 제17권3호
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    • pp.168-173
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    • 2009
  • This study reports the preparation and characterization of nanohydrogels by using sodium alginate as a model material. Alginate nanohydrogels (ANH) were prepared by emulsification-diffusion method in a w/o system with 1,2-diacyl-sn-glycero- 3-phosphocholin as the lipophilic surfactant. The effects of the alginate to surfactant ratio and the remaining water contents on the mean particle size and swellability of ANHs were investigated in terms of the concentration, agitation speed, and agitation time. The feasibility of using nanohydrogels and their controllability were proved by the water the absorbency of ANHs during a 7-day evaluation by dynamic light scattering. In this work, the mean particle sizes of ANHs could be controlled from 49.2 nm (measured in ethanol phase) to $1.9{\mu}m$ (measured in water phase, after 7 days of water absorption).

Response Surface Method를 이용한 폐식용유로부터 바이오디젤 생산의 최적화 (Optimization of Biodiesel Production from Waste Frying Oil using Response Surface Method)

  • 이세진;김의용
    • KSBB Journal
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    • 제17권4호
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    • pp.396-402
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    • 2002
  • 바이오디젤(지방산 메틸 에스테르)은 생분해성, 무독성, 그리고 재생연료로서 지난 10여년간 많은 관심을 끌고 있다. 바이오디젤을 생산하기 위해 다양한 방법들이 개발되었는데, 그 중 알칼리 촉매를 이용한 에스테르화 반응이 짧은 시간동안 높은 수율을 얻을 수 있다. 따라서 본 연구에서는 알칼리 촉매하에 에스테르화 반응의 최적조건을 찾기 위하여 response surface method를 사용하였다. 결과적으로 바이오디젤 생산 공정에 영향을 주는 7개의 변수 중 반응온도, 반응시간, 그리고 교반속도가 중요했는데 이들의 최적 값은 각각 67$^{\circ}C$, 68분, 94 rpm이었다. 이와같은 최적인 조건하에서 실험한 결과 바이오디젤로의 전화율은 99.7%이었다.

화학응집제를 이용한 미세조류의 응집 특성 (Flocculation Characteristics of Microalgae Using Chemical Flocculants)

  • 권도연;정창규;박광범;이철균;이진원
    • KSBB Journal
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    • 제26권2호
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    • pp.143-150
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    • 2011
  • The aim of the study was to optimize harvesting method for concentrating microalgae from microalgae mass culture. It is well known that the mass density of microalgae is usually very low and these are small size (5-20 ${\mu}m$) in the culture medium. It is essential that microalgae is harvested and concentrated economically for economical biodiesel production from microalgae. In this study, to determine optimized conditions for microalgae harvesting by chemical flocculation. Flocculation of three algae, Chlorella ellipsoidea, Dunaliella bardawil, and Dunaliella tertiolecta, was performed using various chemical flocculants, such as inorganic flocculants (aluminium sulfate, aluminium potassium sulfate, ferrous sulfate, ferric sulfate, ferric chloride, calcium hydroxide, sodium carbonate, sodium nitrite, and sodium aluminate), organic flocculant (polyacrylamide), and biopolymer flocculants (chitosan and starch). The results indicated that aluminium based inorganic flocculants is suitable for microalgae harvesting such as Chlorella ellipsoidea, Dunaliella bardawil, and Dunaliella tertiolecta. The results also recommended that flocculant doses, agitation speed, agitation time, sedimentation time for economical microalgae harvesting method using chemical flocculants.

새 도선 감는 방법을 적용한 전기장 이용 스케일 제거 (Prevention of Particulate Scale with a New winding Method in the Electronic Descaling Technology)

  • 손창현;구상모;김창수;김건우
    • 대한기계학회논문집B
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    • 제26권5호
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    • pp.658-665
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    • 2002
  • This paper presents a new winding method in electronic descaling (ED) technology. Conventional ED technology Produces an oscillating electric field via Faraday's law to provide the necessary molecular agitation to dissolve mineral ions. However, the proposed method produces an additional agitation force for mineral ions, called Lorentz's force. Experiments were performed using various Renolds numbers. A series of tests was conducted to measure the pressure drop across the test section and the overall heat transfer coefficient as a function of time. In order to accelerate the rate of fouling, artificial hard water, 1000ppm CaCO$_3$, was used throughout the tests. The results show that the new winding method accelerates the collision of the mineral ions, thereby improving the system efficiency. The present study can develope more effective fouling-removing equipment with change of estabishment method of coil.