• Journal of the Korean Society for Heat Treatment
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• v.30 no.6
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• pp.279-284
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• 2017

Mechanical properties of titanium alloy can be improved by controlling microstructure through heat treatment. In this study, Ti-3Al-8V-6Cr-4Mo-4Zr metastable beta titanium alloy, was controlled for excellent mechanical property and sound formability through various high temperature heat treatment and aging conditions and the optimum heat treatment conditions were determined. The specimens were heat-treated at $950^{\circ}C$, followed by various aging treatments from $430^{\circ}C$ to $500^{\circ}C$ for 1 to 24 h. As aging temperature and holding time increased, hardness increased by ${\beta}^{\prime}$ phase formation and precipitation of secondary ${\alpha}$ phase in ${\beta}$ matrix. However, the optimum aging temperature and holding time for mechanical properties were at $450{\sim}470^{\circ}C$ for 8~16 hr. Hardness values of the specimen aged at $450^{\circ}C$ for 8 h were found to be the highest. These results can be effectively applied to fabrication of spring with better formability and mechanical property.

• Korean Journal of Food Science and Technology
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• v.49 no.6
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• pp.714-716
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• 2017

Rose flower is widely used in the preparation of tea and contains a large variety of phytochemicals, including phenolics such as catechin, quercetin, and rutin. The effects of aging on rose (Rosa hybrida L.) flower extracts (RFE) were examined under conditions of varying temperature and relative humidity. The total phenolic content, antioxidative activity, and catechin levels were measured to evaluate the effects of temperature and relative humidity on the aging process. Performing the aging process at $30^{\circ}C$ under 60% or 90% relative humidity for 24 h significantly increased the total phenolic content and the antioxidant activities of RFE (p<0.05). Additionally, an aging process performed at $30^{\circ}C$ and 60% relative humidity for 24 h maximized the extraction rate of phenolics such as catechin and consequently led to increased antioxidative activity of RFE. In summary, this study indicates that the extraction rate of physiologically active phenolic compounds in rose flower can be increased by performing an aging process under optimized temperature and relative humidity conditions.

• Composites Research
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• v.19 no.4
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• pp.1-6
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• 2006

The effects of aging on fatigue of PSF/AS4 laminates tvas studied using the new energy release rate analysis. The analysis by the variational mechanics has been useful in providing fracture mechanics interpretation of matrix microcracking in cross-ply laminates. This paper describes the changes of the critical energy release rate ${\Delta}Gmc$(microcracking toughness) about the variation of the aging period during fatigue loading. The master plot by modified Pans-law gives a characterization of a material system's resistance to microcrack formation. PSF/AS4 $[0/902]_s$ laminates were aged at four different temperatures based on the glass transition temperature for 60 days. At all temperatures, the toughness decreased with aging time. The decrease of the toughness at higher temperature was faster than at lower temperature. To assess the effects of aging on fatigue, the unaged laminates were compared with the laminates which were aged for 60 days at $170^{\circ}C$ near $180^{\circ}C\;T_g$. The slope of dD/dN versus A 6u, of the aged laminates was lower than that of the unaged laminates. There was a significant shift of the aged data to formation of microcracks at the lower values of ${\Delta}G_m$.

• The Transactions of the Korean Institute of Electrical Engineers C
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• v.51 no.2
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• pp.62-67
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• 2002

This paper provides the results of accelerated aging test of 18kV ZnO lightning arresters to investigate the leakage current characteristics. It was impossible to establish the replacement criterion for field operating lightning arrester because conventional aging test was only focused on the aging of ZnO elements. In general, it is possible to replace the aged arresters before the failure in the field using the leakage current measurement because it must be increased by the aging. But we can not use the method because we don't know the characteristics of the installed lightning arresters. Therefore in this paper we applied operating voltage and accelerating cycle which consists of temperature and humidity to the arresters. Then we measured the variation of total and resistive leakage current and found out the characteristics of the acted lightning arresters.

• Korean Journal of Metals and Materials
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• v.49 no.6
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• pp.448-453
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• 2011

Pre-aging heat treatment after solution heat treatment (SHT) of Al-0.4 wt%Mg-1.2 wt%Si-0.1 wt%Mn alloy sheets for auto-bodies was carried out to investigate the effect of pre-aging and its conditions on the bake-hardening response. Mechanical properties were evaluated by a tensile and Vickers hardness test. Microstructural observation was also performed using a transmission electron microscope (TEM). It was revealed that pre-aging treatments play a great role in the bake-hardening response. In addition, it was found that the sphere-shaped nanosized clusters that can directly transit to the needle-shaped ${\beta}$" phase during the paint-bake process, not being dissolved into the matrix, are formed at 343 K. The result, reveals that the dominant factor of the bake-hardening response is the pre-aging temperature rather than the pre-aging time.

• Journal of the Korean Society for Heat Treatment
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• v.26 no.6
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• pp.293-299
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• 2013

A specimen of weld metal was prepared by GTA welding with weld wire of super duplex stainless steel. Aging treatment was conducted for the sample at the temperature range of 700 to $900^{\circ}C$ for 5 to 300 minutes. The effect of volume fraction of ${\sigma}$-phase to intergranular corrosion of weld metal has been investigated and the results were derived as follows. The volume fraction of ${\sigma}$ phase tends to increase with an increase of aging temperature and time and intergranular corrosion of weld metal was increased by an increase of ${\sigma}$ phase. Degree of sensitization representing intergranular corrosion was found to tend to increase with an increase of aging time at 700 to $800^{\circ}C$, while it decreased by an increase of aging time at $900^{\circ}C$.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.16 no.9
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• pp.842-850
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• 2003

The suspension insulators are subjected to harsh environments in service for a long time. The long-term reliability of tile insulators is required for both mechanical and electrical performances. This study describes some basic performance tests and accelerated aging test by cool-heat cycling methods and thermal mechanical performance test methods on alumina porcelain insulators (new and aged) used for transmission line in KOREA. There was no fail in electrical and mechanical performance tests such as a high voltage strength, a flashover voltage, and an impact strength in all samples. But in the case of accelerating aging tests which have above 9$0^{\circ}C$ temperature gradient, fracture phenomena was happened by a thermal shock in tile aged sample(sample A) with low alumina porcelain body. It was indicated that sample A was more severely aged than other samples. According to results of HRB test and microstructural analysis, it was reasoned that insulator bodies with the matrix reinforced with alumina crystalline phase have advantages over the suppression of crack advance. And cool-heat aging and mechanical thermal ageing tests shows that a temperature gradient is more effective to accelerating than a cycling number.

• Transactions of Materials Processing
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• v.30 no.5
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• pp.226-235
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• 2021

The strain aging behavior of a low carbon dual phase steel was examined in two conditions: representing room temperature strain aging (100 ℃ × 1 hr after 7.5 % prestrain) and bake hardening process (170 ℃ × 20 min after 2 % prestrain), basing on carbon effective diffusion and dislocation distribution. The first principle calculations revealed that (Mn or Cr)-vacancy-C complexes exhibit the strongest attractive interaction compared to other complexes, therefore, act as strong trapping sites for carbon. For room temperature strain aging condition, the carbon effective diffusion distance is smaller than the dislocation distance in the high dislocation density region near ferrite/martensite interfaces as well as ferrite interior considering the carbon trapping effect of the (Mn or Cr)-vacancy-C complexes, implying ineffective Cottrell atmosphere formation. Under bake hardening condition, the carbon effective diffusion distance is larger compared to the dislocation distance in both regions. Therefore, formation of the Cottrell atmosphere is relatively easy resulting in to a relatively large increase in yield strength under bake hardening condition.

• International Journal of Highway Engineering
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• v.15 no.1
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• pp.87-94
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• 2013

PURPOSES: To characterize the aging effect on asphalt binder, dynamic shear modulus mastercurve of two typical asphalt binders are developed. METHODS: To develop dynamic shear modulus mastercurve, dynamic shear modulus at high temperature and creep stiffness at low temperature are measured by temperature sweep test and bending beam rheometer test, respectively. RESULTS: It is observed that the aging effect on asphalt binder can be clearly observed from dynamic shear modulus mastercurve and the mastercurve can be utilized to predict behavior of asphalt binder at wide range of temperature. CONCLUSIONS: It is confirmed that SBS 5% modified binder has more desirable mechanical property at low and high temperature as a pavement material comparing to PG64-22 binder and the mastercurve is an effective tool to evaluate the property of asphalt binder.

• Proceedings of the KWS Conference
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• 2002.10a
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• pp.59-64
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• 2002

Effects of the aging treatments on the microstructure and strength of heat affected zone(HAZ) in the welds of a age-hardened Al-Mg-Si alloy, 5N01-T5, were investigated. The base metal aging treatments before MIG welding were conducted at 423K to 473K for 28.8ks Post weld heat treatment(PWHT) to recover the HAZ strength was performed at 448K for 28.8ks. Microstructure observations, hardness measurements and tensile tests were conducted to study properties of the MIG weld joints. The position of the softest region in HAZ where the hardness insufficiently recovered after natural aging and PWHT was at a distance of approximately 15mm from the center of the fusion zone. Hardness of the softest regions after natural aging and PWHT decreased with increase in the base metal aging temperature. TEM observation clarified that strengthening ${\beta}$"(Mg$_2$Si) precipitates and coarse ${\beta}$′ precipitates affected the hardnes of HAZ. Incomplete recover of hardness in HAZ after PWHT was caused by the precipitating of non-hardening ${\beta}$′ phase during the weld thermal cycle. In order to examine the effects of weldheat input and welding speed, the laser weld joints were also investigated and compared with the MIG weld ones. Laser welding had the narrower width of the softened regions in HAZ compared with MIG welding. The hardness of the softest regions of the laser welds after PWHT was higher than that of the MIG welds. Quantitative relations between hardness of the softest region and base metal aging temperature were obtained for both welding processes. Accordingly, the equations to estimate the strength of the weld joints after PWHT with varying base metal temperatures were proposed for MIG welding and laser welding.