• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.27 no.8
• /
• pp.1398-1408
• /
• 2003

Tensile and LCF(low cycle fatigue) tests were carried out in air at wide temperature range 20$^{\circ}C$-750$^{\circ}C$ and strain rates of 1${\times}$10$\^$-4//s-1${\times}$10$\^$-2/ to ascertain the influence of strain rate on tensile and LCF properties of prior cold worked 316L stainless steel, especially focused on the DSA(dynamic strain aging) regime. Dynamic strain aging induced the change of tensile properties such as strength and ductility in the temperature region 250$^{\circ}C$-600$^{\circ}C$ and this temperature region well coincided with the negative strain rate sensitivity regime. Cyclic stress response at all test conditions was characterized by the initial hardening during a few cycles, followed by gradual softening until final failure. Temperature and strain rate dependence on cyclic softening behavior appears to result from the change of the cyclic plastic deformation mechanism and DSA effect. The DSA regimes between tensile and LCF loading conditions in terms of the negative strain rate sensitivity were well consistent with each other. The drastic reduction in fatigue resistance at elevated temperature was observed, and it was attributed to the effects of oxidation, creep and dynamic strain aging or interactions among them. Especially, in the DSA regime, dynamic strain aging accelerated the reduction of fatigue resistance by enhancing crack initiation and propagation.

• Journal of Korea Foundry Society
• /
• v.38 no.4
• /
• pp.75-81
• /
• 2018

This study examined the effect of the CaMgSn ternary phase on the aging response of the Mg-Sn-Zn alloy. The results revealed that the CaMgSn ternary phase formed in rod-like or needle-like shapes in Mg-3Zn-0.3Ca-xSn (x=1.5, 3, and 5 wt%) alloys and its size decreased as the Sn content increased from 1.5 wt% to 5 wt%. The Mg-3Zn-0.3Ca-5Sn alloy with a relatively fine CaMgSn phase was subjected to solution heat treatment and an aging process. Both the Mg-5Sn-3Zn-0.3Ca and Mg-5Sn-3Zn (base alloy) alloys had similar peak hardness values throughout all aging temperatures but the time-to-peak hardness in the Mg-5Sn-3Zn-0.3Ca alloy was 24-36 hours-earlier than that in the base alloy. Precipitates in the Mg-5Sn-3Zn-0.3Ca alloy were more refined than those in the Mg-5Sn-3Zn alloy and were mostly formed on basal planes. The $Mg_2Sn$ phase formed in either plate-like or rod-like shapes in the Mg-5Sn-3Zn alloy, whereas block-shaped $Mg_2Sn$ particles also formed in the Mg-5Sn-3Zn-0.3Ca alloy.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.24 no.9 s.180
• /
• pp.2183-2190
• /
• 2000

A thermal aging is observed in a primary reactor cooling system(RCS) made of a casting stainless steel when the RCS is exposed for long period at the reactor operating temperature, 290~3300C An investigation of effects of thermal aging on a low cycle fatigue characteristics included a stress variations caused by a reactor operation and trip, is required. The purpose of the present investigation is to find an effect of a thermal aging of the CF8M on a low cycle fatigue life. The specimen of CF8M are prepared by an artificially accelerated aging technique holding 300 and 1800hr at 4300C respectively. The low cycle fatigue tests for the virgin and two aged specimens are performed at the room temperature for various strain amplitudes($\varepsilon$ta), 0.3, 0.5, 0.8, 1.0, 1.2 and 1.5% strain. Through the experiment, it is found that the fatigue life is rapidly reduced with an creasing of the aging time. The experimental fatigue life estimation formulas between the virgin and two aged specimen are obtained and are proposed to a analysis purpose.

• Korean Journal of Materials Research
• /
• v.9 no.7
• /
• pp.695-700
• /
• 1999

Effects of two-step aging treatment on the stress corrosion cracking(SCC) resistance of 7050 Al alloy were investigated by transmission electron microscopy, electrical conductivity measurement and stress corrosion facter(SCF) evaluation. It was found that η', principal hardening phase, transformed to η during over aging above maximum hardness, and SCC resistance was improved by increasing of the size and interspacing of η particles in matrix and grain boundary. The electrical conductivity increased with aging time, but SCF decreased due to the decrease of yield strength. This results mean increase of SCC resistance The optimum two-step aging condition in forged 7050 Al alloy was to be first aged at $120^{\circ}C$ for 6h and then finally aged at $175^{\circ}C$ for 12h.

• Korean Journal of Metals and Materials
• /
• v.48 no.10
• /
• pp.957-963
• /
• 2010

The aging behavior of aluminum borate whisker ($Al_{18}B_4O_{33}$) reinforced AS52+Sr magnesium matrix composites was investigated with Vickers hardness measurements, bending tests, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Experimental results showed that aging is accelerated in the $AS52+Sr/Al_{18}B_4O_{33}$ composite compared with an unreinforced AS52+Sr alloy. The hardness of the alloy and composite increases monotonically as a function of the aging time before reaching its peak hardness and then gradually decreases. The composite reaches its peak hardness in 10 h, whereas the matrix alloy requires 30h, indicating accelerated age-hardening in the $AS52+Sr/Al_{18}B_4O_{33}$ composite compared with the unreinforced AS52+Sr alloy at $170^{\circ}C$. The interfacial reaction of $AS52+Sr/Al_{18}B_4O_{33}$ magnesium matrix composite is considered to play a dominant role in the strengthening mechanism, ultimately affecting the mechanical properties of the composite.

• Journal of the Korean Geosynthetics Society
• /
• v.20 no.2
• /
• pp.1-11
• /
• 2021

In this study, a study related to laboratory and pilot test were performed to use an environmental soil stabilizer developed to induce a hardening reaction similar to that of Ordinary Portland Cement (OPC) by using industrial by-products of blast furnace slag and the combustion ash of a circulating fluidized bed boiler as the main material. For this, specimens were prepared using liquid A of sodium silicate and silica sol, and liquid B of an environmental soil stabilizer (or OPC), and laboratory tests were performed to analyze the strength and environmental characteristics. And pilot test was performed on the aging reservoir, field permeability test and electrical resistivity survey were performed in the field to analyze the applicability. As a result of the laboratory test, the homo-gel compressive strength of the chemical injection material using the environmental soil stabilizer as liquid B was about 2.88 to 3.23 times greater than that of OPC. In addition, the elution amount of most heavy metals was lower than that of OPC, and the survival rate in the fish, acute toxicity test was 100%. Therefore, when judged based on the results of the laboratory test, it was analyzed to be superior to OPC in terms of strength and environment. In the results of the pilot test in the aging reservoir, when the environmental soil stabilizer was reinforced with liquid B of the chemical injection material, the coefficient of permeability in the aging reservoir decreased to 1/50 level. In addition, as a result of the electrical resistivity survey, it was analyzed that the electrical resistivity inside the aging reservoir increased as time passed, the saturation zone disappeared, and the overall reinforcement.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 2000.06a
• /
• pp.48-53
• /
• 2000

The effects of added elements, such as Co or Nb, on wear properties of high speed steel by powder metallurgy(PM-HSS) had been evaluated in previous paper. The wear properties of materials, in fact, have been a]so influenced by heat-treating conditions. In this paper, the effects of heat-treating conditions on wear properties of PM-HSS have been evaluated. The wear tests have been performed as same conditions as previous paper using PM-HSS(5%Co-1%Nb) heat-treated under different quenching and tempering temperature. The result of this paper shows that wear resistance of PM-HSS is improved with relatively high quenching temperature. However tempering temperature is not sensitve to the wear resistance in range of high quenching temperature. It may be deduced by the fact that the shear strength of matrix by strengthening mechanisms of quenching aging in addition to dispersion-hardening is improved.

• Korean Journal of Animal Reproduction
• /
• v.17 no.2
• /
• pp.93-101
• /
• 1993

These experiments were carried out to investigate whether zona hardening affect the efficiency of in vitro fertilization in mouse oocytes. The soluble properties for zona pellucida of oocytes matured in vivo, aged oocytes, and ovarian oocytes matured in vitro have been analyzed with proteolytic enzyme, 3mg/ml of $\alpha$-chymotrypsin. The mean solubility(t50) for the zona of unfertilized oocytes, oocytes not fertilized at the first inseminati and in vitro produced zygotes were 10.1, 20.3 and 32.3min., respectively. The t50 for zona lysis of fertilized oocytes was significantly difference than those observed for unfertilized oocytes and oocytes not fertilized at the first insemination(P<0.01). In addition, the t50 of zona in ovulated oocytes with and without cumulus cells incubated for 0, 3, 6, 9 and 12 hr in vitro, t50 were 13.9, 11.1, 20.7 and 28.0min., and 22.3, 21.0, 30.0 and 33.5min., respectively. In these experiments, the zona pellucida showed a gradual increase in resistance to dissolution by $\alpha$-chyjotrypsin with in vitro aging for more than 6 hrs. This effect was greater in cumulus-free as compared to cumulus-intact oocytes. Finally, in cumulus-intact and cumulus-free ovarian oocytes matured for 0, 5, 10 and 15 hr in vitro the t50 of zona pellucida were 3.0, 10.6, 18.4 and 24.5 min., and 3.0, 14.0, 26.2 and 32.0 min., respectively. Clear differences in solubility between the zona pellucida of oocytes matured in vivo and in vitro. This data were found suggest that under in vitro conditions there is a gradual change in the soluble properties of the zona pellucida, particularly in the absence of the cumulus cells.

• Korean Journal of Materials Research
• /
• v.17 no.11
• /
• pp.587-592
• /
• 2007

Al-42wt%Nb powder was prepared by high-energy mechanical milling(HEMM). The particle size, phase transformation and microstructure of the as-milled powder were investigated by particle size distribution (PSD) analyzer, scanning electron microscopy (SEM), X-ray diffractometery (XRD), transmission electron microscopy (TEM)and differential thermal analysis (DTA). The milled powders were heated to a sintering temperature at 1000C with under vaccum with vaccum tube furnace. Microstructural examination of sintered Ti-42wt%Nb alloy using 4h-milled powder showed Ti-rich phases (${\alpha}$-Ti) which are fine and homogeneously distributed in the matrix (Nb-rich phase: ${\beta}$-Ti). The sintered Ti-42wt%Nb alloy with milled powder showed higher hardness. The microstructure of the as quenched specimens fabricated by sintering using mixed and milled powder almost are same, but the hardness of as quenched specimen fabricated by using mixed powder increased due to solution hardening of Nb in Ti matrix. The aging effect of these specimens on microstructural change and hardening is not prominent.

• Korean Journal of Materials Research
• /
• v.14 no.10
• /
• pp.713-718
• /
• 2004

To study the dynamic strain aging behavior of Zr-0.4Sn-1.5Nb-0.2Fe sample tube for nuclear fuel cladding in the range of pressurized water reactor (PWR) operation temperature, the tensile tests of the tube specimens, which had been finally heat-treated at $470^{\circ}C\;and\;510^{\circ}C$, had been carried out with the strain rate $1.67{\times}10^{-2}/s\;and\;8.33{\times}10^{-5}/s$ at the various temperatures from room temperature to $500^{\circ}C$. It was observed that the elongation of the specimens got shortened as the temperature increased from $200^{\circ}C\;to\;340^{\circ}C$. The specimens that were finally heat-treated at $470^{\circ}C$ showed a plateau more remarkably on the plot of yield strength-temperature than those heat-treated at $510^{\circ}C$. In the range of $310\sim400^{\circ}C$, the strain rate sensitivity of the specimens finally heat-treated at $510^{\circ}C$ was $30.4\%\sim33.7\%$ lower but the work hardening exponent index of the specimens was a little higher than that without dynamic strain aging effect.