• Title/Summary/Keyword: Adhesive interface

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Enhanced Adhesion of Cu Film on the Aluminum Oxide by Applying an Ion-beam-mixd Al Seed Layar

  • Kim, Hyeong-Jin;Park, Jae-Won
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.229-229
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    • 2012
  • Adhesion of Copper film on the aluminum oxide layer formed by anodizing an aluminum plate was enhanced by applying ion beam mixing method. Forming an conductive metal layer on the insulating oxide surface without using adhesive epoxy bonds provide metal-PCB(Printed Circuit Board) better thermal conductivities, which are crucial for high power electric device working condition. IBM (Ion beam mixing) process consists of 3 steps; a preliminary deposition of an film, ion beam bombardment, and additional deposition of film with a proper thickness for the application. For the deposition of the films, e-beam evaporation method was used and 70 KeV N-ions were applied for the ion beam bombardment in this work. Adhesions of the interfaces measured by the adhesive tape test and the pull-off test showed an enhancement with the aid of IBM and the adhesion of the ion-beam-mixed films were commercially acceptable. The mixing feature of the atoms near the interface was studied by scanning electron microscopy, Auger electron spectroscopy, and X-ray photoelectron spectroscopy.

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COMPARISON OF SHEAR BOND STRENGTHS OF FOUR DENTINAL ADHESIVES (네가지 상아질 접착제의 전단 결합 강도 비교)

  • Cho, Kyeong-Mee;Hur, Bock;Lee, Hee-Joo
    • Restorative Dentistry and Endodontics
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    • v.21 no.1
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    • pp.280-288
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    • 1996
  • The purpose of this study was to assess comparatively the shear bond strength on dentin of four dentin bonding agents used in conjunction with light-curing composite resins. Clearfil New Bond, Scotchbond Multipurpose Dentin Adhesive, All-Bond 2 and X-R Bond were applicated on labial dentin surfaces just below dentin - enamel juction of bovine incisor teeth. After shear bond strength testing with the universal testing machine, the bonding interface of the specimens were observed under light stereomicroscope. Following results were obtained. 1. The shear bond strength was high in the order of B,C,D,A and group B Scotchbond Multipurpose Dentine Adhesive revealed greater bond strength than Clearfil New Bond and X-R Bond. (p<.001) 2. When using ANOVA and Duncan's multiple range test, there were statistical differences among the four groups, except between group Band C,group D and A. 3. There was no relationship between mode of failure and shear bond strength.

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Experimental Study on Bonding Properties of Reinforced Concrete with Water-Cement Ratio and Blending of Mineral Admixture (물-시멘트비 및 혼화재 혼입에 따른 철근콘크리트의 부착 특성에 관한 연구)

  • Choi, Yoon-Suk;Kim, Myung-Yu;Yang, Eun-Ik;Yi, Seong-Tae
    • Proceedings of the Korea Concrete Institute Conference
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    • 2006.05b
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    • pp.225-228
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    • 2006
  • To clarify the one body behavior of reinforcing bar and concrete, it is important to investigate bond characteristics between two materials. Bond strength is decided by applied force and interface area between reinforcing bar and concrete. And, the resultant force of chemical adhesive force, frictional force, and mechanical interaction are to be main factors. Property of concrete influences on chemical adhesive force and frictional force; bond strength is decreased by corrosion of reinforcing bar, as the result, durability is also decreased. In this study, to confirm bond characteristics with property of concrete, w/c ratio and blending of mineral admixture were selected as the main test parameters. The results obtained from this study will be used as the basic data for bond characteristics with corrosion.

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INTERFACIAL MORPHOLOGY BETWEEN DENTIN AND ADHESIVES (상아질과 접착제 간의 계면양상)

  • Kang, Ji-Young;Hur, Bock
    • Restorative Dentistry and Endodontics
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    • v.20 no.1
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    • pp.183-192
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    • 1995
  • The purpose of this study was to evaluate the effect of smear layer management on the interfacial morphology between dentin bonding system and dentin. Clearfil New Bond, Scotchbond Multipurpose, Prisma Universal Bond 3 and X-R Bond were used on the cervical dentinal surfaces of bovine incisor teeth. All of the dentin bonding systems were labeled with fluorescene in primer and rhodamine B in adhesive. Specimens of 2~3mm thichness were prepared by longitudinal and labiolingual sectioning. The interface between dentin bonding system and dentin was observed by flouresence imaging with a confocal laser scanning microscope. Following results were obtained. 1. In the specimen of Clearfil New Bond, dentinal tubules were widened by destruction of peritubular dentin in the course of treatment with phosphoric acid of high concentration. 2. Hybrid layer was observed in the specimen of Scotchbond Multipurpose and X-R Bond. 3. In the specimen of Prisma Universal Bond 3, the penetraton of adhesive was not observed clearly.

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Joints Strength Evaluation of light Structure material (경량 구조재료의 접합강도평가)

  • Jang C. S.;Yi W.;Oh S. K.
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2005.05a
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    • pp.234-238
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    • 2005
  • One approach to testing the suitability of a adhesive joint for a particular application is to build and test to destruction of a representative sample of the joint. The nondestructive test will not measure strength directly but will measure a parameter which can be correlated to the strength. It is therefore, essential that a suitable nondestructive test is chosen and its results are correctly interpreted. In this paper, typical ultrasonic signal analysis in adhesive joints are evaluated together with interface stress from the result of finite element analysis.

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Shear bond strength of orthodontic bracket with hydrophilic primer (친수성 프라이머를 이용한 교정용 브라켓 접착시의 전단결합강도에 관한 연구)

  • Park, Chul-Wan;Cha, Kyung-Suk;Lee, Jin-Woo
    • The korean journal of orthodontics
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    • v.32 no.4 s.93
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    • pp.293-300
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    • 2002
  • The purpose of this study was to evaluate the clinical effectiveness of hydrophilic primer, which claim to retain adequate bond strength on moistened enamel resulting from moisture or saliva contamination, by comparing the shear bond strength and adhesive failure patterns of brackets bonded using hydrophilic primer and conventional hydrophobic primer. Brackets were bonded to human premolars embedded in metal cylinders utilizing light cured adhesive, primed with either a hydrophilic primer(Transbond fm primer) or a conventional hydrophobic primer(Transbond XT primer). Each sample was exposed to varying degrees of artificial saliva contamination during the priming process. The shear bond strength was measured using a universal testing machine, and the adhesive failure patterns after debonding were visually examined by strereomicroscope and assessed using the adhesive remnant index(ARI). The results were as follows 1. In dry conditions, no significant differences in shear bond strength between Transbond W and Transbond XT primers were found. 2. Transbond MIP primer exhibited a significantly higher shear bond strength than Transbond XT primer in saliva-contaminated conditions, regardless of the degree of contamination. 3. When contaminated with one coat of saliva, Transbond MIP primer did not exhibit significant differences in shear bond strength compared to the dry condition. When contaminated with two coats of saliva, Transbond MIP primer exhibited a singnificantly lower shear bond strength compared to the dry condition. 4. The adhesive remnant index of the adhesive failure pattern had a tendency to decrease, as the degree of saliva contamination increased. Bracket-adhesive interface failure was observed in more than half of the saliva contaminated samples utilizing Transbond MIP primer, whereas the bond failure sites of the Transbond XT primer samples occurred almost exclusively at the adhesive-enamel interface in saliva-contaminated conditions. The results of this study suggest that in cases where moisture control is difficult, Transbond MIP primer is an effective alternative to conventional hydrophobic primers.

Shear bond strength and adhesive failure pattern in bracket bonding with plasma arc light (Plasma arc light를 이용한 bracket 부착시의 전단결합강도와 파절양상의 유형)

  • Yoo, Hyung-Seok;Oh, Young-Geun;Lee, Seung-Yeon;Park, Young-Chel
    • The korean journal of orthodontics
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    • v.31 no.2 s.85
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    • pp.261-270
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    • 2001
  • The purpose of this study was to evaluate the clinical usefulness of plasma arc light which can reduce the curing time dramatically compared by shear bond strengths and failure patterns of the brackets bonded with visible light in direct bracket bonding. Some kinds of brackets were bonded with the Transbond$^{\circledR}$ to the human premolars which were embedded in the resin blocks according to the various conditions. After bonding, the shear bond strength was tested by Instron universal testing machine and in addition , the amount of residual adhesive remaining on the tooth after debonding was measured by the stereoscope and assessed with adhesive remnant index(ARI). The results were as follows : 1. When plasma arc light was used for bonding the brackets, the shear bond strength was clinically sufficient in both metal and ceramic brackets, but resin brackets showed significantly lower bond strength but which was clinically useful. 2. When metal brackets were bonded using visible light, there was no significant difference in shear bond strength due to the light-curing time and the bond strength was clinically sufficient. 3. When the adhesive failure patterns of brackets bonded with plasma arc light were observed by using the adhesive remnant index, the bond failure of the metal and resin bracket occurred more frequently at bracket-adhesive interface but the failure of the ceramic bracket occurred more frequently at enamel-adhesive interface. 4. There was no statistically significant difference of the shear bond strength and adhesive failure pattern between metal bracket bonded for 2 seconds by curing with plasma arc light and 10 seconds by curing with visible light. 6. When metal brackets were bonded using plasma arc light, the shear bond strength decreased as the distance from the light source increased. The above results suggest that plasma arc light can be clinically useful for bonding the brackets without fear of the decrease of the shear bond strength.

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A Study of Interface Layer on CdZnTe Radiation Sensor for Potable Isotope Identifier (이동형 핵종 분석 장치용 CZT 반도체 검출기의 완충전극에 대한 연구)

  • Cho, Yun Ho;Park, Se-Hwan;Kim, Yong Kyun;Ha, Jang Ho
    • Journal of Radiation Industry
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    • v.5 no.1
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    • pp.95-99
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    • 2011
  • The electrical and mechanical properties of electrode for radiation detection are very important. In general, Au electrode and CZT crystal are combined to form ohmic contacts, and the best energy resolution is shown at the Au electrode. The metal contacts are fabricated by electroless deposition method, sputtering deposition method and thermal evaporation method. The electrode fabrication is easy with use of the thermal evaporation method, while an adhesive strength is weak. Thus interface materials such as Ag, Al and Ni were investigated to overcome defects generated by the this method. The thickness of the interface material between the Au electrode and the CZT crystal was 100 Angstroms, the Au electrode with thickness of 400 Angstroms was deposited. The Al+Au electrode is shown that the results of current-voltage and radiation response are similar to results of Au electrode.

Conservation of Golden Decorative(Jikgeumdan) Jeogori and Chima of Costumes Excavated from Hangju Gi' Tomb of Angang, Kyungsangbukdo Province - Re-adhesion of Gold Leaves in Gilt Paper Strips - (경상북도 안강 행주 기씨 묘 출토 직금단 치마와 저고리 보존처리 - 직금단 편금사의 금박 재접착을 중심으로 -)

  • Oh, Joon-Suk;Noh, Soo-Jung
    • Journal of the Korean Society of Costume
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    • v.57 no.9
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    • pp.67-75
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    • 2007
  • The purpose of this research is to conserve of golden decoration(Jikgeumdan) of Chima(skirt) and Jeogori(Korean jacket) of the costumes excavated from Hangju Gi' tomb(17th Century) of Joseon dynasty$(1392{\sim}1910)$ and to focus on the development of conservation skill to prevent flakings of gold leaves in gilt paper strips. Up to the present, in case of golden decorations of costumes excavated from tombs of Joseon dynasty, some of gold leaves in gilt paper strips of costumes were flaked away by deterioration of adhesives in tombs. However, most of gold leaves were flaked away and totally lost by wet cleaning for eliminating contaminants after excavation. In order to prevent flaking, preliminary experiments for re-adhesion of gold leaves have been carried out. Firstly, simulation was performed using gold leaf which was available in the market. Adhesives used in this research were water-soluble adhesives(hide glue(cow, rabbit), glue made from air bladders of sciaenoid fish and Primal AC-3444 of acrylic emulsion) and solvent-soluble adhesives(acrylic adhesive Paraloid B-67 and B-72). Because of difficulty in wetting and spreading of adhesive solutions into the interface between gold leaf and Korean paper, water-soluble adhesives were not proper for adhesion of gold leaf and Korean paper. Solvent-soluble adhesives were easily infiltrated into interface between gold leaf and Korean paper and the adhesive force was also satisfied. From this result, the researchers chose more flexible Paraloid B-72$(Tg\;40^{\circ}C)$ 1% solution than Paraloid B-67$(Tg\;50^{\circ}C)$ for adhesion of gold leaf and Korean paper. Secondly, using Paraloid B-72 1% solution, the estimations of re-adhesions of gold leaves in gilt paper strips of Jeogori were carried out. When Paraloid B-72 1% solution was injected three times into the interface between gold leaf and Korean paper, the re-adhesion was most effective. On the basis of the results in these preliminary experiments, re-adhesions of gold leaves in gilt paper strips of Chima and Jeogori were carried out on condition of three times injections of Paraloid B-72 1% solution before wet cleaning. After wet cleaning, the most of the gold leaves were survived, which was confirmed by both the examination with the naked eye and the microscopic examination.

Comparison of Mechanical and Interfacial Properties on Chemical Structures of Acrylic and Epoxy Adhesives (아크릴 및 에폭시 접착제의 화학적 구조에 따른 유리섬유 복합재료의 기계적 및 계면 물성 변화 평가)

  • Shin, Pyeong-Su;Kim, Jong-Hyun;Choi, Jin-Yeong;Kwon, Dong-Jun;Lee, Sang-Il;Park, Joung-Man
    • Composites Research
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    • v.29 no.2
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    • pp.79-84
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    • 2016
  • An adhesive can be used to connect two different materials in structures. In comparing with other connecting methods, such as bolt, rivet, and hot melting, the adhesive does not need to use them. It leads to reduce the weight and decrease the stress concentration along the connecting line. This work studied the comparison of mechanical and interfacial properties of commonly-used two adhesives, acrylic type and bisphenol-A epoxy type. Tensile and flexural strength of neat adhesives were also compared. Lap shear test of two adhesives was deduced from the measurement of tensile and fatigue tests. After testing, the failure patterns of adhesive surfaces were observed by a microscope. Tensile strength and mechanical fatigue resistance at using bisphenol-A epoxy adhesive were better than acrylic adhesive. Also adding CNT reinforcement in epoxy adhesive can anticipate mechanical improvement.