• Title/Summary/Keyword: Adhesive failure

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Effects of a relined fiberglass post with conventional and self-adhesive resin cement

  • Wilton Lima dos Santos Junior;Marina Rodrigues Santi;Rodrigo Barros Esteves Lins;Luis Roberto Marcondes Martins
    • Restorative Dentistry and Endodontics
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    • v.49 no.2
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    • pp.18.1-18.13
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    • 2024
  • Objectives: This study was conducted to evaluate the mechanical properties of relined and non-relined fiberglass posts when cemented to root canal dentin using a conventional dual-cure resin cement or a self-adhesive resin cement. Materials and Methods: Two types of resin cements were utilized: conventional and self-adhesive. Additionally, 2 cementation protocols were employed, involving relined and non-relined fiberglass posts. In total, 72 bovine incisors were cemented and subjected to push-out bond strength testing (n = 10) followed by failure mode analysis. The cross-sectional microhardness (n = 5) was assessed along the root canal, and interface analyses (n = 3) were conducted using scanning electron microscopy (SEM). Data from the push-out bond strength and cross-sectional microhardness tests were analyzed via 3-way analysis of variance and the Bonferroni post-hoc test (α= 0.05). Results: For non-relined fiberglass posts, conventional resin cement exhibited higher pushout bond strength than self-adhesive cement. Relined fiberglass posts yielded comparable results between the resin cements. Type II failure was the most common failure mode for both resin cements, regardless of cementation protocol. The use of relined fiberglass posts improved the cross-sectional microhardness values for both cements. SEM images revealed voids and bubbles in the incisors with non-relined fiberglass posts. Conclusions: Mechanical properties were impacted by the cementation protocol. Relined fiberglass posts presented the highest push-out bond strength and cross-sectional microhardness values, regardless of the resin cement used (conventional dual-cure or self-adhesive). Conversely, for non-relined fiberglass posts, the conventional dual-cure resin cement yielded superior results to the self-adhesive resin cement.

THE EFFECT OF ADHESIVE PROPERTY ON MICROTENSILE BOND STRENGTH TO HUMAN DENTIN (상아질 접착제의 성상이 미세인장결합강도에 미치는 영향)

  • Kim, Hyoun-Jin;Hur, Bock;Kim, Hyun-Cheol
    • Restorative Dentistry and Endodontics
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    • v.29 no.3
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    • pp.281-287
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    • 2004
  • The purposes of this study were to evaluate the effect of adhesive property on microtensile bond strength and to determine the failure mode. Flat occlusal dentin surfaces were prepared using low-speed diamond saw. The dentin was etched with 37% phosphoric acid. The following adhesives were applied to the etched dentin to manufacturer's directions: Scotchbond Multi-Purpose in group SM, Prime&Bond NT in group NT, Scotchbond Multi-Purpose followed by Tetric-flow in group TR. After adhesive application, a cylinder of resin-based composite was built up on the occlusal surface. Each tooth was sectioned vertically to obtain the $1{\;}{\times}{\;}1\textrm{mm}^2$ "sticks". Microtensile bond strength were determined. Each specimen was observed under stereomicroscope and scanning electron microscope (SEM) to examine the failure mode. Data were analyzed using one way ANOVA. The results of this study were as follows:1. The microtensile bond strength value were:group SM ($18.98{\pm}3.01MPa$). group NT ($16.01{\pm}4.82MPa$) and group TR ($17.56{\pm}3.22MPa$). No significant statistical differences were observed among the groups (P>0.05). 2. Most of specimens showed mixed failure. In group TR, there was a higher number of specimens showing areas of cohesive failure in resin.

Influence of interfacial adhesive on the failure mechanisms of truss core sandwich panels under in-plane compression

  • Zarei, Mohammad J.;Hatami, Shahabeddin;Gholami, Mohammad
    • Steel and Composite Structures
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    • v.44 no.4
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    • pp.519-529
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    • 2022
  • Sandwich structures with the superior mechanical properties such as high stiffness and strength-to-weight ratio, good thermal insulation, and high energy absorption capacity are used today in aerospace, automotive, marine, and civil engineering industries. These structures are composed of moderately stiff, thin face sheets that withstand the majority of transverse and in-plane loads, separated by a thick, lightweight core that resists shear forces. In this research, the finite element technique is used to simulate a sandwich panel with a truss core under axial compressive stress using ABAQUS software. A review of past experimental studies shows that the bondline between the core and face sheets plays a vital role in the critical failure load. Therefore, this modeling analyzes the damage initiation modes and debonding between face sheet and core by cohesive surface contact with traction-separation model. According to the results obtained from the modeling, it can be observed that the adhesive stiffness has a significant influence on the critical failure load of the specimens. To achieve the full strength of the structure as a continuum, a lower limit is obtained for the adhesive stiffness. By providing this limit stiffness between the core and the panel face sheets, sudden failure of the structure can be prevented.

Design Study of Adhesively Bonded Structures

  • Chung, Jae-Ung
    • Korean Journal of Computational Design and Engineering
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    • v.14 no.2
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    • pp.122-128
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    • 2009
  • The failure responses of adhesively bonded, hat stiffened structures are studied through numerical analysis using the finite element method. The responses are evaluated numerically for the bonded hat section/substrate structures containing different combinations of materials. It is studied what kind of material combinations causes the easier crack initiation in the structure. This study is conducted under plane strain conditions and J-integral via a commercial code ABAQUS as a total critical energy release criterion was used for observation on crack initiation. Also, the influence of adhesive on the structure is studied.

Evaluation of Failure Mode and Strength on Baking Time of Adhesive for Hybrid Joining (접착제 경화시점에 따른 하이브리드 접합 파단모드 및 접합강도 평가)

  • Choi, Chul-Young;Saha, Dulal Chandra;Choi, Won-Ho;Kim, Jun-Ki;Kim, Jong-Hoon;Park, Yeong-Do
    • Journal of Welding and Joining
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    • v.29 no.6
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    • pp.49-55
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    • 2011
  • With the development of pre-painted steel sheets for automotive body application, a new joining method is required such as hybrid joining with combination of adhesive bonding and mechanical joining. The objective of this study is to investigate the effect of pre- and post-baking of adhesive bonding on failure mode and strength of hybrid joining of automotive steel sheets. Experiments show that the hybrid joining exhibits better bonding strength and displacement than conventional adhesive joining and mechanical fastening each. Comparison of pre- and post-baked hybrid joining results suggested that baking at $160^{\circ}C$ after mechanical joining was found to have higher joining properties than pre-baking condition. The prebaking condition changed its fracture mode from interfacial to button fracture. The changes in fracture mode with post-baking of hybrid joining was attributed to variation in neck thickness and undercut of joint.

A comparative study on bond strength and adhesive failure pattern in bracket bonding with self-etching primer (Self-etching Primer를 이용한 교정용 브라켓 부착시 전단결합강도와 파절양상에 관한 비교연구)

  • Kim, You-Kyoung;Lee, Jin-Woo;Cha, Kyung-Suk
    • The korean journal of orthodontics
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    • v.34 no.4 s.105
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    • pp.325-332
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    • 2004
  • A self-etching primer that combines the etchant and primer in one chemical compound saves time and should be mote cost-effective to the clinician and patient. The purpose of this study was to evaluate the clinical effectiveness of a self-etching primer by measuring shear bond strengths according to various conditions and observing adhesive failure patterns. For this Investigation, 120 upper and lower premolars extracted for orthodontic purposes were used and randomly divided into six groups of twenty teeth each. Human premolars were embedded in a metal cylinder with orthodontic resin. Metal brackets and ceramic brackets were bonded with XT primer and self-etching primer by means of XT adhesive. Upon curing, plasma arc light and visible light were used. After bonding, the shear bond strength was tested by Instron universal testing machine, and the amount of residual adhesive that remained on the tooth after debonding was measured by stereoscope and assessed with an adhesive remnant index. The results were as fellows: 1. When brackets were bonded, if other conditions remained the same, there was no significant difference in shear bond strength due to the type of primer - either self-etching primer or XT primer. 2. When metal brackets were bonded, there was no significant difference in shear bond strength according to the source of light - plasma arc light or visible light - and type of primer. 3. There was a very significant difference in shear bond strength according to the type of brackets - metal or ceramic brackets. The shear bond strength of ceramic brackets was stronger than metal brackets. 4. When the adhesive failure patterns of metal brackets bonded with self-etching primer were observed by using the adhesive remnant index, the bond failure of the metal bracket occurred more frequently at the bracket-adhesive. The failure of the ceramic bracket, however, occurred more frequently at the enamel-adhesive interface. The adhesive failure patterns of metal brackets bonded with XT primer observed the same patterns. The above results suggest that self-etching primer can be clinically useful for bonding the brackets without fear of a decrease in shear bond strength.

Analysis of the adhesive damage between composite and metallic adherends: Application to the repair of aircraft structures

  • Ibrahim, Nour Chafak;Bouanani, Morad Fari;Bouiadjra, Bel Abbes Bachir;Serier, Boualem
    • Advances in materials Research
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    • v.5 no.1
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    • pp.11-20
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    • 2016
  • In bonded composite repair of aircraft structures, the damage of the adhesive can thus reduce significantly the efficiency and the durability of the bonded composite repair. The adhesive damage models using critical zone have proven their effectiveness due to simplicity and ap-plicability of the damage criteria in these models. The scope of this study is to analyze the effects of the patch thickness and the adhesive thickness on the damage damage in bonded composite repair of aircraft structures by using modified damage zone theory. The obtained results show that, when the thickness of adhesive increases the damage zone increases and the adhesive loses its rigidity, inversely when the patch is reduced the adhesive damage be-comes more significant.

Progressive Failure Analysis of Adhesive Joints of Filament-Wound Composite Pressure Vessel (필라멘트 와인딩 복합재 압력용기의 접착 체결부에 대한 점진적 파손 해석)

  • Kim, Junhwan;Shin, Kwangbok;Hwang, Taekyung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.38 no.11
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    • pp.1265-1272
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    • 2014
  • This study performed the progressive failure analysis of adhesive joints of a composite pressure vessel with a separated dome by using a cohesive zone model. In order to determine the input parameters of a cohesive element for numerical analysis, the interlaminar fracture toughness values in modes I and II and in the mixed mode for the adhesive joints of the composite pressure vessel were obtained by a material test. All specimens were manufactured by the filament winding method. A mechanical test was performed on adhesively bonded double-lap joints to determine the shear strength of the adhesive joints and verify the reliability of the cohesive zone model for progressive failure analysis. The test results showed that the shear strength of the adhesive joints was 32MPa; the experiment and analysis results had an error of about 4.4%, indicating their relatively good agreement. The progressive failure analysis of a composite pressure vessel with an adhesively bonded dome performed using the cohesive zone model showed that only 5.8% of the total adhesive length was debonded and this debonded length did not affect the structural integrity of the vessel.

Fracture Characteristics Unidirectional Composite Single-Lap Bonded Joints (일방향 복합재료 single-lap 접합 조인트의 파괴 특성)

  • Kim Kwang-Soo;Yoo Jae-Seok;Jang Young-Soo;Yi Yeong-Moo
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.04a
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    • pp.232-236
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    • 2004
  • The fracture characteristics of unidirectional composite single-lap bonded joints were investigated experimentally and numerically. The effects of bonding method, surface roughness, bondline thickness and the existence of fillet on the failure characteristics and strength of bonded single-lap joints were evaluated experimentally. The failure process, failure mode and the behavior of load-displacement curve was apparently different according to bonding method. The failure load of the specimen co-cured without adhesive was definitely superior to other types of specimens but the specimens co-cured with adhesive film had a less strength than secondary bonded specimens. In the secondary bonded specimens, the lower value of surface roughness and existence of fillet improved the strength of specimens. The strain energy release rates calculated by geometric nonlinear finite element analyses and Virtual Crack Closure Technique for the secondary bonded specimens considering the three types of initial cracks - comer crack, edge crack and delamination crack - were consistent with the test results.

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Correction Coeffecient for Tensile Adhesive Strength of the Bridge Decks Waterproofing Systems with Different Temperature Conditions (온도조건에 따른 교면방수재의 인장접착강도 보정계수에 관한 실험적 연구)

  • Lee, Byung-Duck;Yun, Byung-Sung
    • Proceedings of the Korea Concrete Institute Conference
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    • 2004.05a
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    • pp.794-797
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    • 2004
  • In this study, tensile adhesive strength(TAS) test was carreid out for evaluated the effects of temperature conditions (-20, -10, 0, 5, 10, 20, 30, $40^{\circ}C$) on the tensile adhesive characteristics about 4 type waterproofing membranes which were commercially used in bridge decks. And, failure appeariences of waterproofing systems in each temperature after TAS test were observed the sawing surfaces of waterproofing systems for whether or not damaged of waterproofing membranes. Also, correction coefficient of TAS with temperature were calculated using 4 type waterproofing membrane. It could be shown that the higher TAS and shear adhesive strength, the lower temperature, regardless of the type of waterproofing membrane. Temperature sensibility of TAS was especially remarkable in epoxy membrane. Failure type was occurred the ductile failure in $30^{\circ}C\;and\;40^{\circ}C$. From these results, it was shown that if ambient temperature above $30^{\circ}C$ maintains for a long time, waterproofing membrane will be deformed by softening. Otherwise, waterproofing membrane in temperature below $20^{\circ}C$ shown that occurred the brittle failure. From the results of visual observation of cutting surface for specimen, the thin waterproofing membranes shown indented by hot aggregate of the asphalt mixtures. Therefore, it could be known that the specification of waterproofing membrane thickness is necessary by waterproofing membrane type. As temperature change varied with pavement depth, the interface temperature was more important than ambient temperature in TAS test. Now, TAS test results were limited only in $-10^{\circ}C\;and\;20^{\circ}C$ temperature, but correction coefficient of TAS by ambient temperature could be used as a solution to deal with this problem.

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