• Title/Summary/Keyword: Additional curing

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EFFECT OF AN INTERMEDIATE BONDING RESIN AND FLOWABLE RESIN ON THE COMPATIBILITY OF TWO-STEP TOTAL ETCHING ADHESIVES WITH A SELF-CURING COMPOSITE RESIN (자가 중합 복합 레진과 두 단계 산 부식 접착제의 친화성에 대한 중간 접착제와 흐름성 레진의 효과)

  • Choi, Sook-Kyung;Yum, Ji-Wan;Kim, Hyeon-Cheol;Hur, Bock;Park, Jeong-Kil
    • Restorative Dentistry and Endodontics
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    • v.34 no.5
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    • pp.397-405
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    • 2009
  • This study compared the effect of an activator, intermediate bonding resin and low-viscosity flowable resin on the microtensile bond strength of a self-curing composite resin used with two-step total etching adhesives. Twenty extracted permanent molars were used. The teeth were assigned randomly to nine groups (n=10) according to the adhesive system and application of additional methods (activator, intermediate adhesive, flowable resin). The bonding agents and additional applications of each group were applied to the dentin surfaces. Self-curing composite resin buildups were made for each tooth to form a core, 5mm in height. The restored teeth were then stored in distilled water at room temperature for 24h before sectioning. The microtensile bond strength of all specimens was examined. The data was analyzed statistically by one-way ANOVA and a Scheffe's test. The application of an intermediate bonding resin (Optibond FL adhesive) and low-viscosity flowable resin (Tetric N-flow) produced higher bond strength than that with the activator in all groups. Regardless of the method selected, Optibond solo plus produced the lowest ${\mu}TBS$ to dentin. The failure modes of the tested dentin bonding agents were mostly adhesive failure but there were some cases showed cohesive failure in the resin.

Research of Early-age Strength Development Technology for Remove the Steel Form of Large-wide Tunnel Lining Concrete (대단면 터널 라이닝 거푸집의 조기 제거를 위한 초기 강도 발현 기법 연구)

  • Kim, Kwang-Don;Lee, Deuk-Bok
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.18 no.5
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    • pp.116-127
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    • 2014
  • The studies were carried out to process one cycle for a day to the large section tunnel lining concrete. Climatic characteristics of the tunnel inside are changed, when the temperature of the concrete placement is low, the mold remove time is increased that the heat of hydration speed be delayed because affects the strength development, to compensate for this, after installing the curing sheet on both sides of the steel form and installation of tunnel entrance, when it comes to providing the additional heat source of $28{\pm}2^{\circ}C$ therein, it was to be achieved early strength development control standards (4.5MPa) presented as a crack control scheme or more, thus, It was able to remove after age of 14hr from mold. On the other hand, under the conditions of $10{\pm}1^{\circ}C$ that a natural curing temperature in the tunnel, it was analyzed must ensure the curing time of 36hr or more after concrete placement. Throughout this study, the concrete strength development and the temperature in the early-age concrete, it can find that reverify the curing temperature is greatly affected, even concrete fly ash is mixed 10%, if it is possible to raise the surface temperature for a predetermined time, is not a problem in the early strength development.

A Study on Adhesion of Mechanical Properties of Rubber by MgCl2 (투명 차폐 필름 구현을 위한 전도성 복합 바인더의 입자구조에 따른 성능 평가)

  • Park, Ji-won;Back, Jong-Ho;Lee, Tae-Hyung;Kim, Hyun-Joong
    • Journal of Adhesion and Interface
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    • v.18 no.2
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    • pp.59-67
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    • 2017
  • Recently, integration of parts is accelerating according to the growth of the smart mobile industry. The integration of these parts causes problems of interference phenomena between the parts, and the importance of electromagnetic wave shielding technology to solve this problem is highlighted. Electromagnetic wave shielding technology is implemented so as to reflect or absorb electromagnetic waves, and generally conductive materials are utilized for electromagnetic wave shielding. Transparent shielding technology is required according to recent industrial changes. In this research, we propose transparent the shielding film using imprint technology with conductive composite binder. Utilizing UV polymerized acrylic binder to produce a conductive composite binder. Spherical, plate and stacked silver particles were used for conductivity. The changes of the curing characteristics, conductivity and adhesion were observed according to the structural characteristics of the silver particles. The use of spherical particles was the most efficient in the curing process, and an additional curing system was required to complement the UV-shadowing structure. In the conductivity evaluation, the stacked structure showed excellent characteristics. The adhesion of spherical system was the best. It is evaluated as a result of irregularities on the surface. Ultimately, the patterned film using this showed excellent transparency characteristics.

Flexual strength of resins for provisional fixed prostheses (임시 고정성 보철물 제작용 레진의 굽힘강도)

  • Choi, Myoung-Ah;Ahn, Seung-Geun;Cho, Kuk-Hyeon
    • Journal of Dental Rehabilitation and Applied Science
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    • v.16 no.3
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    • pp.221-227
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    • 2000
  • Provisional fixed partial dentures(FPDs) are an important part of many prosthodontic treatment procedures. These provisional fixed prostheses must fulfill biologic, mechanical, and esthetic requirements to be considered successful. Consideration of all these factors and requirements are important because provisional resin restorations may be worn over a long period to assess the results of periodontal and endodontics therapies, and also during the restorative phase of implant reconstructive procedures. This in vitro study examined flexual strength of four resins commonly used for fixed provisional prostheses. The effects of polymerization conditions were also evaluated. The four resins tested were : Caulk Temporary bridge resin(L.D. Caulk Co. Dentsply International Millford), Jet(Lang Dental Mfg. Co. Chicago. ILL. U.S.A), Alike (Coe Laboratories. Inc. Chicago. ILL. U.S.A) and Tokuso Curefast (Coe Laboratories. Inc. Chicago. ILL. U.S.A) The test specimens were 65mm long, 14mm wide, and 3.5mm thickness. 10 specimens of four resins were cured for 15 minutes at atmospheric pressure and 10 specimens of four resins were cured at an additional pressure of approximately 20 psi. A total of 80 specimens were prepared. The flexual strength was determined by three-point bending test. Data were analysed with the Paired samples T-test and Tukey student-range test Within the limitations imposed in this study, the following conclusions can be drawn : 1. Under the condition of bench curing, Caulk Temporary bridge resin showed the highest flexual strength. In decreasing order, the flexual strength of the other materials was as follows : Jet, Tokuso Curefast, Alike, and Caulk Temporary bridge resin demonstrated significantly higher strength than other resins. 2. Under the condition of pressure curing, Jet showed the highest flexual strength. In decreasing order, the flexual strength of the other materials was as follows : Caulk Temporary bridge resin, Tokuso Curefast, and Alike. There were all statistically significant differences among four resins 3. There was a statistically significant difference between bench- and pressure-cured specimens in all four materials.

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Study on effect of ultrasonic inspection criteria to soundness evaluation of honeycomb core sandwich and laminate structure used for commercial aircrafts (초음파검사 판정 기준이 항공기용 복합구조재의 건전성 평가에 미치는 영향에 관한 고찰)

  • 진양준;한중원;김국진;송기경
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.10a
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    • pp.202-207
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    • 2002
  • The soundness of honeycomb core sandwich and laminate structure used for commercial aircrafts is generally evaluated with ultrasonic inspection because the inspection is most sensitive to planar surfaces which are perpendicular to sound propagation pass and reflects sound almost 100% to equipment. And most defects inherent in composite material curing process has good reflective surfaces. With all this advantage, unexpected obstruction to product and additional cost could be occurred when inappropriate accept/reject criteria is given. In this study the importance of inspection criteria will be discussed to show how inappropriate criteria cause unexpected results leading to high production cost and how much time must be spent to correct those improper criteria with an actual case occurred in Aerospace Division, Korean Air.

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Nonformaldehyde Anti-crease Finish of Ramie with Glyoxal (Part I) (글리옥살을 이용한 마직물의 무포름알데히드 방추가공(제 1보)-촉매의 영향)

  • 오경화;홍경화
    • Journal of the Korean Society of Clothing and Textiles
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    • v.22 no.8
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    • pp.1060-1068
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    • 1998
  • The effects of various catalysts and softners on the anti-crease finish of ramie with glyoxal were investigated. A number of metal salts commonly used as Lewis acid catalysts in DP finishing of cotton with formaldehyde and N-methylol agents were screened for glyoxal treatment of ramie fabric. Various organic and inorganic acids were mixed with Lewis acid catalyst as co-catalysts to improve catalytic activity. As a result, the combination of aluminum sulfate and citric acid was proven highly effective in catalyzing the crosslinking of ramie cellulose by glyoxal under lower curing temperature. With a mixed catalyst, performance properties, such as whiteness and tearing strength as well as wrinkle recovery of treated ramie fabric were improved as compared with that treated with aluminum sulfate alone. Additional improvement of tearing strength and wrinkle recovery was achieved by applying silicons softner in the treatment bath.

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A Study on the Tendency to Research of Scalp Acupunture (두침요법의 연구동향에 대한 고찰)

  • Kim, Min-Ki;Oh, Min-Seok
    • Journal of Haehwa Medicine
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    • v.17 no.1
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    • pp.113-127
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    • 2008
  • Method : We consider some books on scalp acupuncture and reports of scalp acupuncture published in korea, and survey motor cortex stimulation. The results are as follows. Result : Scalp acupuncture was based on theory of meridian pathway and functional cerebral cortex. Scalp acupunctur was used especially for CVA(Cerebral Vascular Accident) out of cerebral diseases many time. and this acupuncture shows better effect when used with different treatments than when used singly. Motor cortex stimulation is brothers to scalp acupuncture, and give medical treatment on neuropathic pain. Conclusion : The possibility of curing illness through scalp acupuncture have been shown factually and clinically. Based upon such facts, it is regarded that further scientific research along with additional clinical approaches involving scalp acupuncture should be performed.

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Process Conditions for the Fabrication of Hydrophobic Surfaces with Different Photo-curable Resins (광경화성 레진의 성분 변화에 대한 소수성 표면 제작을 위한 공정 조건)

  • Hong, Sung-Ho;Woo, Heung-Sik
    • Tribology and Lubricants
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    • v.36 no.5
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    • pp.267-273
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    • 2020
  • This study experimentally investigates hydrophobic surfaces fabricated via additive manufacturing. Additive manufacturing, commonly known as 3D printing, is the process of joining materials to fabricate parts from 3D model data, usually in a layer-upon-layer manner. Digital light processing is used to fabricate hydrophobic surfaces in this study. This method uses photo-curable resins and ultraviolet (UV) sources. Moreover, this technique generally has faster shaping speeds and is advantageous for the fabrication of small components because it enables the fabrication of one layer at a time. Two photo-curable resins with different compositions are used to fabricate micro-patterns of hydrophobic surfaces. The resins are composed of a photo-initiator, monomer, and oligomer. Experiments are conducted to determine suitable process conditions for the fabrication of hydrophobic surfaces depending on the type of resin. The most important factors affecting the process conditions are the UV exposure time and slice thickness. The fabrication capability according to the process conditions is evaluated using the side and top views of the micro-patterns observed using a microscope. The micro-patterns are collapsed and intertwined when the exposure time is short because sufficient light (heat) is not applied to cure the photo-curable resin with a given slice thickness. On the other hand, the micro-patterns are attached to each other when the exposure time is prolonged because the over-curing time can cure the periphery of a given shape. When the slice is thicker, the additional curing area is enlarged in each slice owing to the straightness of UV light, and the slice surface becomes rough.

A Study on the Isotropic Nd$_2$Fe$_{14}$B/Epoxy Bonded Magnets with High Characteristics (고특성 등방성 Nd$_2$Fe$_{14}$B/에폭시 본드자석의 연구)

  • 조태식;정원용
    • Polymer(Korea)
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    • v.26 no.1
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    • pp.98-104
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    • 2002
  • This study was investigated to fabricate the isotropic $Nd_2Fe_{14}B$/epoxy bonded magnets with high characteristics paroduced by compression molding. The magnetic characteristics of the bonded magnets were directly proportional to the density of the magnets and were enhanced by using raw $Nd_2Fe_{14}B$ magnetic powders, having the mean particle size of $200{\mu} m$.without additional milling process. The high characteristics of the bonded magnets were achieved at the following conditions: epoxy resin of 2.0 wt%, silane coupling agent of 0.8 wt%, curing agent of 0.7 wt% on the base of magnetic powders, and curing condition of $150^{\circ}C$/3 hrs. The bonded magnets at the optimum conditions indicated the high characteristics such as the density of 6.1 g/㎤, the remanent flux density of 7.1 kG, the maximum energy product of 9.7 MGOe, and the compressive strength of 17 kg/$mm^2$.

Properties of CLC using Silica to Suppress Cracking due to Drying Shrinkage (건조수축에 따른 균열 억제를 위한 규사 혼입 CLC의 특성)

  • Lee, Chang-Woo;Lee, Sang-Soo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2021.11a
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    • pp.125-126
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    • 2021
  • In order to improve the housing culture, construction changes for the utilization of diverse and multifunctional spaces are appearing in response to the increasing diverse needs of consumers. Cellular Light-weight Concrete (CLC) is being developed for use in fire-resistant heat-insulating walls and non-bearing walls. However, manufacturing non-uniformity has become a problem as a drawback due to the use of foamed bubbles and normal temperature curing, and additional research is required. Therefore, in order to suppress cracks due to drying shrinkage, silica sand is mixed with CLC to try to understand its characteristics. In the experiment, the compressive strength from 7 to 28 days of age was measured via a constant temperature and humidity chamber, and the drying shrinkage was analyzed according to each condition using a strain gauge. The compressive strength of matrix tends to decrease as the substitution rate of silica sand increases. This is judged by the result derived from the fact that the specific surface area of silica sand is smaller than that of slag. Based on KS F 2701 (ALC block), the compressive strength of 0.6 products is 4.9 MPa or more as a guide, so the maximum replacement rate of silica sand that satisfies this can be seen at 60%. Looking at the change in drying shrinkage for just 7 days, the shrinkage due to temperature change and drying is 0.7 mm, and the possibility of cracking due to shrinkage can be seen, and it seems that continuous improvement and supplementation are needed in the future.

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