• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2015년도 추계 학술논문 발표대회
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• pp.137-138
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• 2015

The use of the cement and increased with the recent development of the construction industry. If the cement is the environmental problems caused by generating a large quantity of CO₂ and the production process. Accordingly, this study is the test to determine the sulfuric acid and hydrochloric acid resistance properties of the Light weight matrix product of blast furnace slag-based light. A result, the compression strength of the sulfuric acid and hydrochloric acid immersion showed alower strength than the Plain.

• The Journal of Advanced Prosthodontics
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• 제8권5호
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• pp.339-344
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• 2016

PURPOSE. Pre-surface treatments of coping materials have been recommended to enhance the bonding to the veneering ceramic. Little is known on the effect on shear bond strength, particularly with new coping material. The aim of this study was to investigate the shear bond strength of veneering ceramic to three coping materials: i) metal alloy (MA), ii) zirconia oxide (ZO), and iii) lithium disilicate (LD) after various pre-surface treatments. MATERIALS AND METHODS. Thirty-two (n = 32) discs were prepared for each coping material. Four pre-surface treatments were prepared for each sub-group (n = 8); a) no treatment or control (C), b) sandblast (SB), c) acid etch (AE), and d) sandblast and acid etch (SBAE). Veneering ceramics were applied to all discs. Shear bond strength was measured with a universal testing machine. Data were analyzed with two-way ANOVA and Tukey's multiple comparisons tests. RESULTS. Mean shear bond strengths were obtained for MA ($19.00{\pm}6.39MPa$), ZO ($24.45{\pm}5.14MPa$) and LD ($13.62{\pm}5.12MPa$). There were statistically significant differences in types of coping material and various pre-surface treatments (P<.05). There was a significant correlation between coping materials and pre-surface treatment to the shear bond strength (P<.05). CONCLUSION. Shear bond strength of veneering ceramic to zirconia oxide was higher than metal alloy and lithium disilicate. The highest shear bond strengths were obtained in sandblast and acid etch treatment for zirconia oxide and lithium disilicate groups, and in acid etch treatment for metal alloy group.

• The Journal of Advanced Prosthodontics
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• 제4권4호
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• pp.187-191
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• 2012

PURPOSE. The aim of the present study was to assess the effect of ascorbic acid, ethanol and acetone on microtensile bond strength between fiber posts pre-treated with hydrogen peroxide and composite resin cores. MATERIALS AND METHODS. Twenty four fiber posts were pre-treated with 24% hydrogen peroxide and divided into 4 groups as follows: G1: no treatment, as control group; G2: treatment with10% ascorbic acid solution for 5 minutes; G3: treatment with 70% ethanol solution for 5 minutes; and G4: treatment with 70% acetone solution for 5 minutes. Each fiber post was surrounded by a cylinder-shaped polyglass matrix which was subsequently filled with composite resin. Two sections from each sample were selected for microtensile test at a crosshead with speed of 0.5 mm/min. Statistical analyses were performed using one-way ANOVA and a post hoc Tukey HSD test. Fractured surfaces were observed under a stereomicroscope at ${\times}20$ magnification. The fractured surfaces of the specimens were observed and evaluated under a SEM. RESULTS. Means of microtensile bond strength values (MPa) and standard deviations in the groups were as follows: G1: $9.70{\pm}0.81$; G2: $12.62{\pm}1.80$; G3: $16.60{\pm}1.93$; and G4: $21.24{\pm}1.95$. G4 and G1 had the highest and the lowest bond strength values, respectively. A greater bond strength value was seen in G3 compared to G2. There were significant differences between all the groups (P<.001). All the failures were of the adhesive mode. CONCLUSION. Application of antioxidant agents may increase microtensile bond strength between fiber posts treated with hydrogen peroxide and composite cores. Acetone increased bond strength more than ascorbic acid and ethanol.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1990년도 가을 학술발표회 논문집
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• pp.101-106
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• 1990

To estimate the concrete strength at fresh state is very important problem in quality control. So, this study is designed for analyzing the quality control application of practical use Re-Mi-Con with the early estimation method of concrete strength using the test of solution heat of hydrochloric acid.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1998년도 가을 학술발표회 논문집(I)
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• pp.76-81
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• 1998

The physical properties of cement sludge treated with hydrofluosilicic acid were investigated. The compressive strength of cement mortar substituted cement sludge was decreased than that of OPC(ordinary portland cement) mortar. Cement sludge, for improving its physical properties, was treated with hydrofluosilicic acid. And compressive strength of cement mortar substituted TCS was greatly improved than that of OPC mortar. Particularly, cement mortar substituted TCS had the higher value in water-proofness than of OPC.

• 대한화학회지
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• 제41권8호
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• pp.427-436
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• 1997

A simple relation exists between electronegativities of cations and their oxidation states and ionic radii. An empirical law is proposed: X = 0.274 z-0.15 z r - 0.01 r+1+${\alpha}$, z being oxidation number, r ionic radius in $\AA$ and ${\alpha}$ a term related to the atomic number. this relation permits to calculate an electronegativity scale covering a large set of electronic and crystallographic situations. An application to the calculation of acid strengths of cations is presented.

• 대한치과교정학회지
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• 제43권3호
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• pp.141-146
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• 2013

Objective: Bonding forces of brackets to enamel surfaces may be affected by the procedures used for bleaching and enamel etching. The aim of this study was to investigate the bonding strength of orthodontic brackets to laser-etched surfaces of bleached teeth. Methods: In a nonbleached control group, acid etching (group A) or Er:YAG laser application (group B) was performed prior to bracket bonding (n = 13 in each group). Similar surface treatments were performed at 1 day (groups C and D; n = 13 in each subgroup) or at 3 weeks (groups E and F; n = 13 in each subgroup) after 38% hydrogen peroxide bleaching in another set of teeth. The specimens were debonded after thermocycling. Results: Laser etching of bleached teeth resulted in clinically unacceptable low bonding strength. In the case of acid-etched teeth, waiting for 3 weeks before attachment of brackets to the bleached surfaces resulted in similar, but not identical, bond strength values as those obtained with nonbleached surfaces. However, in the laser-etched groups, the bonding strength after 3 weeks was the same as that for the nonbleached group. Conclusions: When teeth bleached with 38% hydrogen peroxide are meant to be bonded immediately, acid etching is preferable.

• Restorative Dentistry and Endodontics
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• 제18권2호
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• pp.423-430
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• 1993

The purpose of this study was to investigate the effect of ferric and ferric ions contained in phosphoric acid solution as a pretreatment solution on bonding of MMA/TBBO resin to dentin. Each of 1 % and 3 % ferric chloride. cupric chloride. cupric sulfate. and cupric nitrate was mixed into 10% phosphoric acid solution and pretreated dentin surface of bovine anterior teeth for 30 seconds followed- by water rinse and dry. Tensile bond strength was determined after bonding of pretreated dentin with MMA/TBBO resin by use of brush-on ;technique and storing for 24 hours in 3it distilled water. The amount of cupric ions adsorbed on pretreated dentin surface was detected by Wave-Dispersion X-ray microanalyzer for different groups of each pretreatment solution containing cupric salts. The pretreatment with cupric ions contained in 10% phosphoric acid solution was effective to increase bonding strength of MMA/TBBO resin to dentin but not in case of ferric ions. The pretreatment with 3 % cupric chloride and cupric nitrate both enhanced significant increase in bonding strength compared to the control group of 10% phosphoric acid solution(p<0.05). Cupric ions measured in pretreated dentin surface was higher in 3 % cupric chloride group than in 1% cupric chloride group, but couldn't find distinct relationship from the results of this experiment between the amount of adsorbed cupric ions according to the kind of cupric salts and the bonding strength value.

• 대한치과교정학회지
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• 제28권5호
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• pp.689-698
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• 1998

법랑질의 표면처리에 따른 광중합형 글래스아이오노머 시멘트의 전단결합강도를 알아보고자 사람 소구치 80개를 선택하여 8개군으로 나누어 전단 결합 강도를 측정하고, 접착 파절의 양상을 평가하여 다음과 같은 결과를 얻었다. $1.37\%$ 인산용액으로 부식한 후 건조상태에서 글래스아이오노머 시멘트, 광중합형 레진, 화학중합형 레진으로 각각 부착한 실험군에서 글래스아이오노머 시멘트 실험군의 전단결합강도는 두 군과 유의한 차가 없었으나 화학중합형 레진군의 그것은 광중합형 레진군에 비해 유의성있게 낮았다 (p<0.05). $2.37\%$ 인산 실험군, $10\%$ 폴리 아크릴산 실험군, $1.23\%$ APF 실험군, 산처리하지 않은 실험군의 습한 상태에서 부착한 글래스아이오노머 시멘트의 전단결합강도에서 산처리하지않은 실험군의 그것이 유의성 있게 낮았으며, 그 외 군간에는 유의성 있는 차이가 없었다 (p<0.05). 3. 글래스아이오노머 실험군에서 습기의 존재가 전단결합강도에 유의성 있는 영향을 미치지 않았다 (p<0.05). 4. 산부식처리를 하지않은 군의 접착제 잔류지수가 가장 낮았으며 $37\%$인산용액으로 처리한 군의 접착제 잔류지수가 가장 높았다.

• Restorative Dentistry and Endodontics
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• 제12권2호
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• pp.45-53
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• 1987

The purpose of this study was to evaluate the tensile bond strength between composite resin and the human enamel. Three composite resin systems, two chemical (Clearfil Posterior, and Clearfil Posterior-3) and one light cure (Photo Clearfil-A), used with and without an intermediate resin (clearfil bonding agent), were evaluated under different amounts of load (10g, 200g and 200g for a moment) for in vitro tensile bond strength to acid-eched human enamel. Clinically intact buccal or lingual surfaces of 144 freshly extracted human permanent molars, embedded in acrylic were flattened with No #600 carborundum discs. Samples were randomly assigned to the different materials and treatments using a table of random numbers. Eight samples were thus prepared for each group(Table 2) these surfaces were etched with an acid etchant (Kurarey Co. Japan) in a mode of etching for 30 seconds, washing for 15 seconds, and drying for 30-seconds. During the polymerization of composite resin on the acid-etched enamel surfaces with and without bonding agent 10-gram, 200 gram and temporary 200 gram of load were applied. The specimens were stored in 50% relation humidity at $37^{\circ}C$ for 24 hours before testing. An universal Testing machine (Intesco model No. 2010, Tokyo, Japan) was used to apply tensile loads in the vertical directed (fig 5), and the force required for separation was recorded with a cross head speed of 0.25 mm/min and 20 kg in full scale. The results were as follow: 1. The tensile bond strength was much greater in applying a bonding agent than in not doing that. 2. The tensile bond strength of chemical cure composite resin was higher than that of light cure composite resin with applying on bonding agent on the acid-etched enamel. 3. In case of not applying a bonding agents on the acid-etching enamel, the highest tensile bond strength under 200 gram of load was measured in light cure composite resin. 4. The tensile bond strength under 200-gram of load has no relation with applying the bonding agent. 5. Under the load of 10-gram, There was significant difference in tensile bond strength as applying the bonding agent.