• 대한금속재료학회지
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• 제47권3호
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• pp.155-168
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• 2009

In this study, microstructural investigation was conducted on the separation phenomenon occurring during Charpy impact tests of API X80 linepipe steels. Particular emphasis was placed on the role of microstructural phases present in the API X80 steels such as acicular ferrite, bainite, and hard secondary phases. Detailed microstructural analysis of fractured impact specimens showed that highly elongated bainite worked as prior initiation sites for separations, and that the number and length of separations increased with increasing volume fraction of bainite. In the steels having high work hardenability, tearing-shaped separations were found because the hammer-impacted region was seriously hardened during the impact test, which led to the reduction in the impact toughness. As the test temperature decreased, the tendency of separations increased, but separations were not observed when the cleavage fracture prevailed at very low temperatures. Thus, the minimization of the formation of bainite and secondary phases in the steels would be beneficial for preventing or minimizing separations because separations deteriorated low-temperature impact toughness.

• 소성∙가공
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• 제15권2호
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• pp.118-125
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• 2006

API steel is used for line-pipe to transport the oil and natural gas. As the recent trends in the development of API steel are towards the use of larger diameter and thicker plate, many researches have been studied to achieve higher strength, higher toughness and lower yield ratio in API steel. However, the strength of API steel after pipe forming is changed depending on the competition of the Bauschinger effect and work hardening which are affected by the strain history during pipe forming process. So, the purpose of this study is to investigate the influence of microstructure on the Bauschinger effect for API steel. To change the microstructure of API steel we have changed the hot rolling condition and the amounts of V and Cu addition. The compression-tensile test and the microstructure observation by OM and TEM were conducted to investigate the yield strength drop and the correlation between the Bauschinger effect and microstructure of API steel. The experimental results show that the increase of polygonal ferrites volume fraction increases the Baushcinger effect due to the back stress which comes from the increase of mobile dislocation density at polygonal ferrite interior during the compressive deformation. The hot rolling condition was more effective on the Bauschinger effect in API steel than the small amount of V and Cu addition.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2004년도 춘계학술대회
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• pp.216-221
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• 2004

Linepipe steels with a low carbon acicular ferrite microstructure have been recently developed to accommodate the current transportation condition of the gas and oil industry, and they are finally applied to West- East pipeline project in China. By adopting acicular microstructure, both better formability and better toughness could be obtained due to low yield ratio and fine grained microstructure. Mechanical properties of pipe are not greatly different from those of base plates or hot coils with a microstructure of acicular ferrite. Merits of introducing higher strength steels are well known, i.e., reducing the gauge of pipe and the material cost, increasing the welding speed and decreasing construction cost because of reducing the construction period. Threfore, gas and oil industry has required higher strength steel than APIX70 grade steel. Under this background, API-X80 steel has been developed and shall be applied to the several projects. In this paper, developing stage of API-X80 steel is also presented and discussed.

• 대한금속재료학회지
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• 제47권2호
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• pp.59-70
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• 2009

This study is concerned with the correlation between microstructure and mechanical properties in heat affected zones (HAZs) of API X80 pipeline steels containing complex oxides. Three kinds of specimens were fabricated by varying alloying elements of Ti, Al, and Mg to form complex oxides, and their microstructures, Vickers hardness, Charpy impact properties were investigated. The number of complex oxides increased as the excess amount of Ti, Al, and Mg was included in the steels. The simulated HAZs containing a number of oxides showed a high volume fraction of acicular ferrite region because oxides acted as nucleation sites for acicular ferrite. According to the correlation study between thermal input, volume fraction of acicular ferrite region, and Charpy impact properties, the ductile fracture occurred predominantly when the volume fraction of acicular ferrite region was 65% or higher, and the Charpy absorbed energy was excellent over 200 J. When the volume fraction of acicular ferrite region was 35% or lower, the Charpy absorbed energy was poor below 50 J as the brittle cleavage fracture occurred. These findings suggested that the active nucleation of acicular ferrite in the oxide-containing steel HAZs was associated with the great improvement of Charpy impact properties of the HAZs.

• 대한금속재료학회지
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• 제46권4호
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• pp.199-208
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• 2008

This study is concerned with effects of complex oxides on Charpy impact toughness of heat affected zone (HAZ) of API X80 linepipe steels. Three kinds of steels were fabricated by varying alloying elements such as Ti, Al, and Mg and hot-rolling conditions to form complex oxides, and their microstructures and Charpy impact properties were investigated. The number of complex oxides present in the steel containing excess Ti, Al, and Mg was twice larger than that in the conventional steels, while their size ranged from 1 to $3{\mu}m$ in the three steels. After the HAZ simulation test, the steel containing a number of oxides contained about 20 vol.% of acicular ferrite in the simulated HAZ, together with bainitic ferrite and martensite, whereas the HAZ microstructure of the conventional steels consisted of bainitic ferrite and martensite with a small amount of acicular ferrite. This formation of acicular ferrite in the oxide-containing steel was associated with the nucleation of acicular ferrite at complex oxides, thereby leading to the great (five times or more) improvement of Charpy impact toughness over the conventional steels.

• 대한금속재료학회지
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• 제46권12호
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• pp.788-799
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• 2008

This study is concerned with the effects of Mo, Cr, and V addition on tensile and Charpy impact properties of API X80 linepipe steels. Four kinds of steels were processed by varying Mo, Cr, and V additions, and their microstructures and tensile and Charpy impact properties were investigated. Since the addition of Mo and V promoted to form fine acicular ferrite and granular bainite, while prohibiting the coarsening of granular bainite, it increased the strength and upper shelf energy, and decreased the energy transition temperature. The Cr addition promoted the formation of coarse granular bainite and secondary phases such as martensite-austenite constituents, thereby leading to the increased effective grain size, energy transition temperature, and strength and to the decreased upper shelf energy. The steel containing 0.3wt.% Mo and 0.06wt.% V without Cr had the highest upper shelf energy and the lowest energy transition temperature because its microstructure was composed of fine acicular ferrite and granular bainite, together with a small amount of hard secondary phases, while its tensile properties maintained excellent.

• 대한금속재료학회지
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• 제47권9호
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• pp.523-532
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• 2009

In this study, four API X80 linepipe steel specimens were fabricated with varying cooling rates and finish cooling temperatures, and their microstructures and crystallographic orientations were analyzed to investigate the effects of cooling conditions on their tensile and Charpy impact properties. All the specimens consisted of acicular ferrite, granular bainite, and secondary phases such as martensite and martensiteaustenite constituent. The volume fraction of secondary phases increased with increasing cooling rate, and the higher finish cooling temperature resulted in the reduction in volume fraction and grain size of secondary phases. According to the crystallographic orientation analysis data, the effective grain size and unit crack path decreased as fine acicular ferrites having a large amount of high-angle grain boundaries were homogeneously formed, thereby leading to the improvement of Charpy impact properties. The specimen fabricated with the higher cooling rate and lower finish cooling temperature had the highest upper shelf energy and the lowest energy transition temperature because it contained a large amount of fine secondary phases homogeneously distributed inside fine acicular ferrites, while its tensile properties well maintained.

• 한국전산구조공학회:학술대회논문집
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• 한국전산구조공학회 2007년도 정기 학술대회 논문집
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• pp.211-216
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• 2007

The objective of this paper is to present the results of an experimental and a finite-element investigation into the behavior of X80 grade pipes subjected to bending. For the pipe specimens comprising the test series, different D/t is applied to be representative of those that can be expected in the field. Results from the numerical models are checked against the observations in the testing program and the ability of numerical solutions to predict pipe moment capacity. curvatures. and buckling modes is established. A finite-element model was developed using the finite-element simulator to predict the local buckling behavior of pipes. The comparison between the numerical and the experimental results demonstrates the ability of the analytical model to predict the local buckling behavior of pipes when deformed well into the post-yield range.

• 대한금속재료학회지
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• 제49권10호
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• pp.766-773
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• 2011

In this study, three kinds of linepipe steels were processed by changing the amount of Mo and Nb to investigate the effects on microstructures, tensile and Charpy impact properties. All the specimens consisted of acicular ferrite, granular bainite and secondary phases such as martensite and austenite constituents (MA). The increase in Mo raised the volume fractions of the granular bainite and MA, and raised the number of fine precipitates, which increased the yield and tensile strengths and decreased the upper self energy and energy transition temperatures. In the steel having less Mo and more Nb, the volume fractions of the granular bainite and MA decreased, and a finer microstructure was observed. This microstructure suppressed the formation of separation during Charpy impact testing and led to a higher upper shelf energy and lower energy transition temperature, while the yield and tensile strengths were lower than those of the steels with more Mo and less Nb.

• 대한금속재료학회지
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• 제48권8호
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• pp.705-716
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• 2010

Effects of specimen thickness and notch shape on fracture mode appearing in drop weight tear test (DWTT) specimens of API X70 and X80 linepipe steels were investigated. Detailed microstructural analysis of fractured DWTT specimens showed that the fractures were initiated in normal cleavage mode near the specimen notch, and that some separations were observed at the center of the fracture surfaces. The Chevron-notch (CN) DWTT specimens had broader normal cleavage surfaces than the pressed-notch (PN) DWTT specimens. Larger inverse fracture surfaces appeared in the PN DWTT specimens because of the higher fracture initiation energy at the notch and the higher strain hardening in the hammer-impacted region. The number and length of separations were larger in the CN DWTT specimens than in the PN DWTT specimens, and increased with increasing specimen thickness due to the plane strain condition effect. As the test temperature decreased, the tendency to separations increased, but separations were not found when the cleavage fracture prevailed at very low temperatures. The DWTT test results, such as upper shelf energy and energy transition temperature, were discussed in relation with microstructures and fracture modes including cleavage fracture, shear fracture, inverse fracture, and separations.