• Transactions of Materials Processing
• /
• v.16 no.2 s.92
• /
• pp.101-106
• /
• 2007

Uniaxial displacement controlled tests were performed on annealed Type 304 stainless steel at room temperature. A servo-controlled testing machine and strain measurement on the gage length were employed to measure the response to a given input. The test results exhibit that the flow stress increases nonlinearly with the strain rate and the relaxed stress at the end of the relaxation periods depends strongly on the strain rate preceding the relaxation test. The rate-dependent inelastic deformation behavior is simulated using a new unified viscoplasticity model that has the rate-dependent format of nonlinear kinematic hardening rule, which plays a key role in modeling the rate dependence of relaxation behavior. The model does not employ yield or loading/unloading criteria and consists of a flow law and the evolution laws of two tensor and one scalar-valued state variables.

• Journal of the Korea Institute of Military Science and Technology
• /
• v.10 no.3
• /
• pp.5-15
• /
• 2007

A welding structures is generally composed of dissimilar steel materials in order to reduce weight cost, and has a gap to fill the welding agent. Also, heat flow analysis should be fulfilled for structure existing of gap to figure out residual stress which is generated after welding. Since mechanical properties of welding structure composed of dissimilar steel is more fragile than mechanical properties of welding structure consisted of same material, heat flow analysis verifying this should be fulfilled as well. Therefore, on this research, heat flow analysis about dissimilar steel weldment consisted of gap existing AISI304 and AISI630 is practiced so that it could be a basic data of research about mechanical properties of gap existing dissimilar steel welding part which is going to be studied later on. During heat flow analysis, heat input model which based on Gaussian profile and using volume heat flux was newly consisted and applied. In addition, for verifying of analysis on this research, gap existing dissimilar steel weldment which had gap of 0.25mm and was welded using Nd-YAG. The welding profile and temperature distribution for weldment during welding was compared to the result which was gotten through heat flow analysis. Both of those results corresponded each other.

• Journal of Welding and Joining
• /
• v.11 no.1
• /
• pp.21-32
• /
• 1993

A cracking failure of a austenitic stainless steel elbow in a naphtha cracking line in a petrochenmical plant occurred, resulting in leakage of organic compound flowing inside the elbow. Due to the failure, emergency shutdown of the plant was enforced to repair the troubled part of the line. The repair cost as well as production loss during the unscheduled plant shutdown has cost the company a great amount of financial loss. In this studies, a failure analysis of the cracked elbow was performed using NDT, chemical analysis, microstructural analysis including optical microscopy as well as scanning electron microscopy with EPMA, mechanical testings such as tensile testing, hardness testing and Charphy impact test fractography. The results indicated that several problems such as a welding defect and presence of a detrimental phase which was found to be relate to improper postforming heat treatment process was identified and the failure was concluded to be due to a low temperature embrittlement of the defect-containing elbows.

• Korean Journal of Metals and Materials
• /
• v.47 no.10
• /
• pp.629-634
• /
• 2009

The effects of processing parameters on the surface properties of the hardened layers processed by the low temperature plasma nitrocarburizing and the low temperature two-step plama treatment (carburizing+nitriding) were investigated. The nitrogen-enriched expanded austenite structure (${\gamma}_N$) or S phase was formed on all of the treated surface. The surface hardness reached up to 1200 $HV_{0.025}$, which is about 5 times higher than that of untreated sample (250 $HV_{0.1}$). The thickness of hardened layer of the low temperature plasma nitrocarburized layer treated at $400^{\circ}C$ for 40 hour was only $15{\mu}m$, while the layer thicknesss in the two-step plama treatment for the 30 hour treatment increased up to about $30{\mu}m$. The surface thickness and hardness increased with increasing treatment temperature and time. In addition, the corrosion resistance was enhanced than untreated samples due to a high concentration of N on the surface. However, higher treatment temperature and longer treatment time resulted in the formation of $Cr_2N$ precipitates, which causes the degradation of corrosion resistance.

• Structural Engineering and Mechanics
• /
• v.7 no.5
• /
• pp.457-471
• /
• 1999

In this paper, different curvature-rates are controlled to highlight the characteristic of viscoplastic response in cyclic bending tests. The curvature-ovalization apparatus, which was designed by Pan et al. (1998), is used for conducting the curvature-controlled experiments on thin-walled tubular specimens for AISI 304 stainless steel under cyclic bending. The results reveals that the faster the curvature-rate implies, the fast degree of hardening of the metal tube. However, the ovalization of the tube cross-section increases when the curvature-rate increases.

• Nuclear Engineering and Technology
• /
• v.47 no.4
• /
• pp.454-460
• /
• 2015

Acoustic emission (AE) is one of the promising methods for detecting the formation of stress corrosion cracks (SCCs) in laboratory tests. This method has the advantage of online inspection. Some studies have been conducted to investigate the characteristics of AE parameters during SCC propagation. However, it is difficult to classify the distinct features of SCC behavior. Because the previous studies were performed on slow strain rate test or compact tension specimens, it is difficult to make certain correlations between AE signals and actual SCC behavior in real tube-type specimens. In this study, the specimen was a AISI 304 stainless steel tube widely applied in the nuclear industry, and an accelerated test was conducted at high temperature and pressure with a corrosive environmental condition. The study result indicated that intense AE signals were mainly detected in the elastic deformation region, and a good correlation was observed between AE activity and crack growth. By contrast, the behavior of accumulated counts was divided into four regions. According to the waveform analysis, a specific waveform pattern was observed during SCC development. It is suggested that AE can be used to detect and monitor SCC initiation and propagation in actual tubes.

• Journal of the Korean Society for Nondestructive Testing
• /
• v.26 no.1
• /
• pp.7-11
• /
• 2006

Since ceramic layers coated on machinery components inevitably experience the changes in their properties it is necessary to evaluate the characteristics of ceramic coating layers nondestructively for a reliable use of coated components and 4heir remaining life prediction. To address such a need, in the present study, an ultrasonic backward radiation technique is applied to investigate the characteristics of leaky Rayleigh surface waves propagating through the very thin TiN ceramic layers coated on AISI 1045 steel or austenitic 304 steel substrate with three different conditions of surface roughness, coating layer thickness and wear condition. In the experiments performed in the present work, the peak angle and the peak amplitude of ultrasonic backward radiation profile varied sensitively according to three specimen preparation renditions. in fact, this result demonstrates a high possibility of the ultrasonic backward radiation as an effective tool for the nondestructive characterization of the resting layers even in such a thin regime.

• Korean Journal of Metals and Materials
• /
• v.46 no.3
• /
• pp.125-130
• /
• 2008

Conventional plasma carburizing or nitriding for austenitic stainless steels results in a degradation of corrosion resistance. However, a low temperature plasma surface treatment can improve surface hardness without deteriorating the corrosion resistance. The 2-step low temperature plasma processes (the combined carburizing and post nitriding) offers the increase of both surface hardness and thickness of hardened layer and corrosion resistance than the individually processed low temperature nitriding and low temperature carburizing techniques. In the present paper, attempts have been made to investigate the influence of the introduction of Ar gas (0~20%) in nitriding atmosphere during low temperature plasma nitriding at $370^{\circ}C$ after low temperature plasma carburizing at $470^{\circ}C$. All treated specimens exhibited the increase of the surface hardness with increasing Ar level in the atmosphere and the surface hardness value reached up to 1050 HV0.1, greater than 750 $HV_{0.1}$ in the carburized state. The expanded austenite phase (${\gamma}_N$) was observed on the most of the treated surfaces. The thickness of the ${\gamma}_N$ layer reached about $7{\mu}m$ for the specimen treated in the nitriding atmosphere containing 20% Ar. In case of 10% Ar containing atmosphere, the corrosion resistance was significantly enhanced than untreated austenitic stainless steels, whilst 20% Ar level in the atmosphere caused to form CrN in the N-enriched layer (${\gamma}_N$), which led to the degradation of corrosion resistance compared with untreated austenitic stainless steels.

• Journal of the Korean Ceramic Society
• /
• v.32 no.1
• /
• pp.95-105
• /
• 1995

Ceria(CeO2) stabilized zirconia(CeSZ) sol was synthesized with zirconium n-butoxide Zr(OC4H9)4 and cerium nitrate hexahydrate Ce(NO3)3.6H2O as precursors and ethylacetoacetate(EAcAc) as a chelating agent under atmosphere. CeSZ films were deposited on AISI 304 stainless steel using the prepared polymeric sol by dipcoating and the coating characteristics were investigated by XRD, ellipsometry, scratch test and SEM. The CeSZ film began to crystallize from amorphous to tetragonal phase at 40$0^{\circ}C$ and it was not converted into monoclinic phase up to 100$0^{\circ}C$ by the addition of 16mol% CeO2 as a stabilizer which could suppress phase transformation of zirconia. The CeSZ films were prepared by varying the EAcAc contents and the cncentration of CeSZ sol and measured the thickness and refractive index. From these results, it was found that the EAcAc contents and concentration of CeSZ coating sol evidently affect the densification of CeSZ film. The CeSZ film coated with 0.4M CeSZ sol and heat-treated at $600^{\circ}C$ for 10min had thickness of 50nm and 17% porosity. The CeSZ film on 304 stainless steel effectively acted as a protective layer against oxidation up to 80$0^{\circ}C$ and had superior corrosion resistance in 25% H2SO4 solution for 4.5 hrs.

• Proceedings of the KWS Conference
• /
• 2002.10a
• /
• pp.260-265
• /
• 2002

Microbiologically influenced Corrosion (MIC) is one of the most deleterious effects of metal microbe interactions. When a fresh metal surface comes in contact with a non-sterile fluid, biofilm formation is ensued. This might result in the initiation of corrosion. The sites and materials where MIC is implicated are versatile. Industries such as shipping, power generation, chemical etc are reported to be affected. The rapid and unexpected failure of AISI type 304 stainless steel was investigated in the laboratory by simulation studies for a period of 4 months. Slime and water samples from the failure site were screened for corrosion causing bacteria. Both aerobic and anaerobic nora were enumerated and identified using PCR techniques. Pseudomonas sp. and Bacillus sp. were the most common aerobic bacteria isolated from the water and slime samples, whilst sulfate reducing bacteria (SRB) were the major anaerobic bacteria. The aerobic bacteria were used for the corrosion experiments in the laboratory. Coupon exposure studies were conducted using a very dilute (0.1%V/V) nutrient broth medium. The coupons after retrieval were observed under a Scanning Electron Microscope (SEM) for the presence of MIC pits. Compared to sterile controls, metal coupons exposed to Pseudomonas sp and Bacillus sp. showed the initiation of severe pitting corrosion. However, amongst these two strains, Psudomonas sp. caused pits in a very short span of 14 days. Towards the end of the experiment, severe pitting was observed in both the cases. The detailed observation of pits showed they vary both in number and shapes. Whilst the coupons exposed to Bacillus sp. showed widely spread scales like pits, those exposed to Pseudomonas sp. showed smaller and circular pits, which had grown in number and size by the end of the experiment. From these results it is inferred that the rapid and unexpected failure of 304 SS might be due to MIC. Pseudonwnas sp. could be considered as the major responsible bacteria that could initiate pits in the metallic structures. As the appearance of pits was different in both the tested strains, it was thought that the mechanisms of pit formation are different. Experiments on these lines are being continued.