• Journal of the Korean Magnetics Society
• /
• v.9 no.1
• /
• pp.23-28
• /
• 1999

${\Alpha}-Fe_2O_3$ was accomplished by chemical method as low temperature as possible and the crystallographic and magnetic properties have been studied by Mossbauer spectroscopy and X-ray diffraction. The sample heated at 15$0^{\circ}C$ is found to have a Corundums symmetry with the hexagonal lattice constant a=8.26$\pm$0.05$\AA$, c=8.75$\pm$0.05$\AA$. The M$\"{o}$ssbauer spectra between the 4.2K and the room temperature show that the ${\Alpha}-Fe_2O_3$ crystallized with a single phase and fine sizes. The particle size distribution has the Gaussian distribution center at 98$\AA$ and the half width of 32$\AA$.TEX>.

• Journal of the Optical Society of Korea
• /
• v.14 no.3
• /
• pp.221-227
• /
• 2010

Aerosol size distribution provides good information for predicting weather changes and understanding cloud formation. Aerosol extinction coefficient and backscattering coefficient are measured by many scientists, but these parameters depend not only on aerosol size but on aerosol concentrations. An algorithm has been developed to measure aerosol parameters such as ${\AA}$ngstr$\ddot{o}$m exponent, color ratio, and LIDAR ratio without any assumptions by using two wavelength rotational Raman LIDAR signals. These parameters are good indicators for the aerosol size. And we can find ${\AA}$ngstr$\ddot{o}$m exponent, color ratio, and LIDAR ratio under various weather conditions. Finally, it can be seen that the ${\AA}$ngstr$\ddot{o}$m exponent has an inverse relationship to the particle size of the aerosol and the color ratio is linearly dependent on the aerosol size. An ${\AA}$ngstr$\ddot{o}$m exponent from 1.2 to 3.1, a color ratio from 0.28 to 1.04, and a LIDAR ratio 66.9 sr at 355 nm and 32.6 sr at 532 nm near the cloud were obtained.

• Journal of the Korean Magnetics Society
• /
• v.5 no.1
• /
• pp.42-47
• /
• 1995

FeN thin films for inductive recording heads were sputter deposited using RF diode sputtering mehtod from a pure iron target onto 7059 glass substrates, and their magnetic properties were measured. The magnetic properties were greatly affected by film thickness, gas pressure, sputter power and flow ratio of $N_{2}$ to Ar. Single layer FeN films with their thickness varied from $1,000\;{\AA}$ to $6,000\;{\AA}$ were doposited. 800 W sputter power, 3 mT gas pressure, $N_{2}$ to Ar flow ratio of 6.6 : 100 were the sputtering conditions. Up to 7 layers of FeN films having total thickness of $6,000\;{\AA}$ were deposited using $SiO_{2}$ of $30\;{\AA}$ thickness as intermediate layers and their coercivity and saturation magnetization were measured. The sputtering conditions were the same as those in the single layer films. Easy axis coercivity of the single layer FeN films gradually decreased as their thickness was increased, but for the films with their thicknesses above $3,000\;{\AA}$, the coercivity changed very little. As the number of the FeN layers were increased, the coercivity decreased We estimated the grain size of FeN films from the FWHM (Full Width at Half Maximum) of X-ray diffraction peaks. The grain size steadily decreased from about $200\;{\AA}$ to $120\;{\AA}$ as the number of layers were increased. Minimum hard axis coercivity of 0.4 Oe was obtained when the number of layers was four. Maximum relative permeability was 2,900 when the number of layers was three. The cut off frequeocy of the multilayer films were above 100 MHz.

• Journal of the Korean institute of surface engineering
• /
• v.54 no.4
• /
• pp.200-208
• /
• 2021

This paper investigated generation behavior of micro-arcs and growth behavior of PEO films on the AA7050 disc specimen in 0.1 M NaAlO₂ solution under the application of 1200 Hz anodic pulse current. Morphologies, thickness and surface roughness of PEO films were examined at the edge part and central part separately. Micro-arcs were generated first at the edge part and then moved towards the central part with PEO treatment time, indicating lateral growth of PEO films. The lateral growth resulted in uniform PEO thickness of about 5 ㎛ and surface roughness of about 0.5 ㎛. Moving of the arcs from the edge towards the central part appeared only one time and large size arcs were generated at the edge before completing the central part with small size micro-arcs. This suggests that vertical growth starts before completing the lateral growth. Large size arcs generated at the edge resulted in the formation of relatively large size pores within the PEO films on the AA7050 disc specimen.

• Communications for Statistical Applications and Methods
• /
• v.10 no.1
• /
• pp.115-123
• /
• 2003

In this paper, we discuss the usefulness of AB/BA/AA/BB crossover design sense of sample size. The result is that the AB/BA/AA/BB crossover design is more economical than AB/BA one if large carryover effect exists and so is it in the comparison with completely randomized design within-subject correlation is large.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2007.10a
• /
• pp.326-327
• /
• 2007

A study on the texture and the formability after asymmetric rolled and subsequent heat-treated AA 1050 aluminum alloy sheets have been carried out. The specimens after the asymmetric rolling showed a very fine grain size, a decrease of <100>//ND, and an increase of <111>//ND textures. The change of plastic strain ratios has been investigated and it was found that they were higher than those of the initial Al sheet.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2007.10a
• /
• pp.328-329
• /
• 2007

A study on the texture and the formability after frictional rolled and subsequent heat-treated AA 1050 aluminum alloy sheets have been carried out. The specimens after the frictional rolling showed a very fine grain size, a decrease of <100>//ND, and an increase of <111>//ND textures. The change of plastic strain ratios has been investigated and it was found that they were higher than those of the initial Al sheet.

• Korean Journal of Materials Research
• /
• v.32 no.2
• /
• pp.72-79
• /
• 2022

A cold roll-bonding process using AA1050, AA5052 and AA6061 alloy sheets is performed without lubrication. The roll-bonded specimen is a multi-layer complex aluminum alloy sheet in which the AA1050, AA5052 and AA6061 sheets are alternately stacked. The microstructural evolution with the increase of annealing temperature for the roll-bonded aluminum sheet is investigated in detail. The roll-bonded aluminum sheet shows a typical deformation structure in which the grains are elongated in the rolling direction over all regions. However, microstructural evolution of the annealed specimen is different depending on the type of material, resulting in a heterogeneous microstructure in the thickness direction of the layered aluminum sheet. Complete recrystallization occurs at 250 ℃ in the AA5052 region, which is lower by 100K than that of the AA1050 region. Variation of the misorientation angle distribution and texture development with increase of annealing temperature also differ depending on the type of material. Differences of microstructural evolution between aluminum alloys with increase of annealing temperature can be mainly explained in terms of amounts of impurities and initial grain size.

• Electrical & Electronic Materials
• /
• v.10 no.8
• /
• pp.794-799
• /
• 1997

Poly-Si films have been prepared by solid phase crystallization of LPCVD(low-pressure CVD) amorphous silicon. The crystallinity of poly-Si films has been derived from UV reflectance spectrum and lies in the range between 70% and 80% . From XRD measurement the peak at 28.2$^{\circ}$from (111) plane is dominantly detected in the SPC poly-Si films, The average grain size of poly-Si film is determined by the image of SEM and varies from 4000 $\AA$ to 8000$\AA$. The electrical conductivity of as-deposited amorphous silicon film is about 2.5$\times$10$^{-7}$ ($\Omega$.cm)$^{-1}$ , and 3~4$\times$10$^{-6}$ ($\Omega$.cm)$^{-1}$ of room temperature conductivity is the SPC poly-Si films. The conductivity activation energies are 0.5~0.6 eV or the 500$\AA$-thick poly-Si films.

• Applied Chemistry for Engineering
• /
• v.3 no.4
• /
• pp.701-709
• /
• 1992

Silver particles were impregnated on carbon black with colloidal method and used as catalyst for oxygen electrode in alkaline fuel cell. With the addition of sodium dodecylbenzenesulfonate in $AgNO_3$ and $NaBH_4$solution, colloidal solution was made and confirmed with electrophoresis test. Effects of particle size on electrode performance were studied and $200{\AA}$ of silver particle size shown the highest value of mass activity. The aggromeration of silver particle was Influenced with surfactant amount, stirring time and heat treatment. Considering the increase of particle size caused of operating temperature, recommendable particle size of silver catalyst for manufacturing the electrode was $100{\AA}$. Dispersity of carbon black was investigated and reagglomeration was appeared after homogenizing 30 sec.