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$Si/In/CeO_2/Si$ 박막의 Indium 분포와 photoluminescence

  • 문병식;양지훈;김종걸;박종윤
    • Proceedings of the Korean Vacuum Society Conference
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    • 1999.07a
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    • pp.104-104
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    • 1999
  • Cerium dioxide 박막의 포토루미네슨에 관해서는 Cerium 4f band에서 oxygen 2p band로의 transition에 의한 발광(400nm) 현상이 보고되었다. 또한 Indium Oxide 박막의 발광(637nm0 현상이 보고되었다. 본 연구에서는 3족인 Indium을 Si/In/CeO2/Si 구조와 CeO2/Si 구조에 도핑하여 포토루미네슨스 현상을 관찰하였다. E-beam evaporator를 사용하여 Silicon(111) 기판에 Cerium dioxcide 박막을 성장시킨 경우의 두가지 시료를 분석하였다. 포토루미네슨스 관찰을 위해서 Ge-Cd laser (325nm)가 사용되었으며 Indium의 도핑양과 분포 상태를 알기 위해 SIMS와 ADP를 이용하여 분석하였다. Indium양에 대한 포토루미네슨스 변화와 열처리 후의 indium의 분포의 변화에 의한 포토루미네슨스 변화를 관찰하였다. 상온에서 In/CeO2/Si 시료와 Si/In/CeO2/Si 시료에 대한 포토루미네슨스 현상을 관찰한 결과 Si/In/CeO2/Si 시료에서만 500nm(2.5eV)에서 발광 현상이 관찰되었다. 도핑된 indium은 ADP에서는 검출되지 않고 SIMS에서만 검출되어 ADP의 detection range(1-0.1%) 이하의 양이 도핑된 것으로 추측된다. 도핑된 Indium의 양이 증가할수록 포토루미네슨스의 Intensity가 증가하였다. 또한 열처리(110$0^{\circ}C$, 1min) 후 포토루미네슨스의 peak위치가 390nm(3.18eV)로 변화하였다. Si/In/CeO2/Si에서 포토루미네슨스 현상이 관측되고 Intensity가 indium의 양에 의존하므로 완전하지 못한 Cerium dioxide의 CeOx 구조와 indium과의 결합이 포토루미네슨스의 원인으로 추측된다. 열처리 후 SIMS의 분석결과 indium의 분포가 변화하였으며 이는 포토루미네슨스의 변화의 원인으로 판단된다.

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Performance Test of High-Power Pulsed Klystron-Load (대출력 펄스 클라이스트론 부하의 성능시험)

  • Jang, S.D.;Son, Y.G.;Oh, J.S.
    • Proceedings of the KIEE Conference
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    • 2003.07c
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    • pp.1756-1758
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    • 2003
  • 포항 방사광 가속기의 선형가속기는 2.5GeV 전자빔 용 마이크로웨이브의 발생을 위하여 80MW 급 클라이스트론(klystron) 11대와 입사부 용 65MW 급 클라이스트론 1대를 사용한다. 80-MW 급 클라이스트론 부하를 구동하기 위하여 최대 펄스 정격출력 200 MW(400kv, 500A, 평탄도 4.4 ${\mu}s$)인 대출력 펄스 전원공급 장치(modulator)가 요구된다. 모듈레이터 시스템 용 PFN(pulse forming network) 커패시터의 충전용 입력전원으로써 최대 출력전압 50 kV, ${\pm}$ 0.5% 이내의 전압제어가 가능한 고전압 인버터 전원장치를 적용하여 클라이스트론 부하의 성능시험을 수행하였다. 클라이스트론의 RF 전력과 입력 빔의 특성을 정확히 측정하기 위하여 응답특성이 양호한 측정 장치와 정밀한 측정이 요구된다. 인버터 시스템의 적용에 따른 모듈레이터의 충전 특성을 파악하였으며, 방향성 결합기와 검파기를 설치하여 클라이스트론의 RF 출력을 측정하였다. 본 논문에서는 포항 방사광 가속기의 대출력 펄스 고주파원으로 사용되는 클라이스트론 부하의 성능시험 과정에서 수행하였던 시험장치 개선 및 특성 분석, 고전압(빔전압 320 kV) 및 RF 길들이기의 시험 결과에 관하여 고찰하고자 한다.

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Experimental Analysis on Temperature Compensation of Capacitive Voltage Divider for a Pulsed High Voltage Measurement (고전압 펄스신호 측정용 분압기의 온도보상에 관한 실험)

  • Jang, S.D.;Son, Y.G.;Kwon, S.J.;Oh, J.S.;Cho, M.H.
    • Proceedings of the KIEE Conference
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    • 2005.07b
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    • pp.1530-1533
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    • 2005
  • Total 12 units of high power klystron-modulator systems as microwave source is under operation for 2.5-GeV electron linear accelerator in Pohang Light Source(PLS) linac. RF power and beam power of klystron are precisely measured for the effective control of electron beam. A precise measurement and measurement equipment with good response characteristics are required for this. Input power of klystron is calculated from the applied voltage and the current on its cathode. Tiny measurement error severely effects RF output power value of klystron. Therefore, special care is needed to measure precise beam voltage. Capacitive voltage divider(CVD) unit is intended for the measurement of beam voltage of 400 kV generated from the pulsed klystron-modulator system. Main parameter to determine the standard capacitance in the high arm of CVD is dielectric constant of insulation oil. Therefore CVD should be designed to have a minimum capacitance variation due to voltage, frequency and temperature in the measurement range. This paper will discuss the analysis of capacitive voltage divider for a pulsed high-voltage measurement, and the empirical relations between capacitance and oil temperature variation.

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Neutron Capture Resonance Energy Identification of Indium by Time-of-Flight Method (중성자 비행시간법을 이용한 인듐의 공명에너지 동정에 관한 연구)

  • Lee, Sam-Yol
    • Journal of the Korean Society of Radiology
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    • v.6 no.5
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    • pp.403-408
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    • 2012
  • Prompt gamma ray from the natural Indium sample was measured by using an assembly of BGO($Bi_4Ge_3O_{12}$) scintillation detectors in the neutron energy region from 1 to 300 eV. The assembly was composed of pieces of BGO. The spectrometer was composed geometrically as total energy absorption detector. 46-MeV electron linear accelerator which is located at Research Reactor Institute, Kyoto University used for neutron sources from photonuclear reaction. The measurement of the neutron capture resonances was performed to below neutron energy 1 keV, because of strong X-ray effect from photonuclear reaction in Ta target and short distance from the target to an assembly of detector. The distance of neutron flight path is $12.7{\pm}0.02m$. The large neutron capture resonances were measured from 1 to 400 eV. The energy in the capture resonance was compared with the evaluated values. The large resonances were seen in the present measurement. General agreement can be seen between the present measurement and the previous evaluated data in relevant energy region. In the present study, we measured the continues resonance structure above 1 keV neutron energy region. 91.49 eV new neutron capture resonance was found in present measurement.

Crystal Structure and Piezoelectric Properties of Four Component Langasite A3B Ga3Si2O14 (A = Ca or Sr, B = Ta or Nb)

  • Ohsato, Hitoshi;Iwataki, Tsuyoshi;Morikoshi, Hiroki
    • Transactions on Electrical and Electronic Materials
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    • v.13 no.4
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    • pp.171-176
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    • 2012
  • As langasite $A_3BC_3D_2O_{14}$ compounds with piezoelectric properties exhibit no phase transition up to the melting point of 1,400-$1,500^{\circ}C$, many high temperature applications are expected for the SAW filter, temperature sensor, pressure sensor, and so on, based on the digital transformation of wider bandwidth and higher-bit rates. It has a larger electromechanical coupling factor compared to quartz and also nearly the same temperature stability as quartz. The $La_3Ga_5SiO_{14}$ (LGS) crystal with the $Ca_3Ga_2Ge_4O_{14}$-type crystal structure was synthesized and the crystal structure was analyzed by Mill et al. It is also an important feature that the growth of the single crystal is easy. In the case of three-element compounds such as $[R_3]_A[Ga]_B[Ga_3]_C[GaSi]_DO_{14}$ (R=La, Pr and Nd), the piezoelectric constant increases with the ionic radius of R. In this study, crystal structures of four-element compounds such as $[A_3]_A[B]_B[Ga_3]_C[Si_2]_DO_{14}$ (A = Ca or Sr, B = Ta or Nb) are analyzed by a single crystal X-ray diffraction, and the mechanism and properties of the piezoelectricity depending on the species of cation was clarified based on the crystal structure.

A Trade-Off Study of the Number of Engines for Fighter Characteristics (엔진 수에 따른 전투기 특성 비교분석연구)

  • Kim, Sung-Lae;Reu, Tae-Kyu
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.31 no.6
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    • pp.102-109
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    • 2003
  • The number of engines for fighters has been decided by thrust required and available engines at the time since the beginning of the jet age. However, many factors such as combat effectiveness, survivability, performance, and cost were considered as engine technology has been progressed. From the vietnam war and desert storm, a twin engine fighter was shown slight superiority to a single engine one in an vulnerability,but single engine fighters were a little predominant in susceptibility This paper includes the trade-off study results on the number of engines for the supersonic light attack aircraft with single and twin engines. Twin engine configuration is 8%, 26%, and 13% higher than single engine one in MTOGW, Flyaway Cost, and LCC respectively. Little difference has been found in RM&S, Maneuver and field performance. According to the factors above, single engine fighter is profitable for low class and twin engine one for medium and higher class.

Practical countermeasures for the aerodynamic performance of long-span cable-stayed bridges with open decks

  • Zhou, Rui;Yang, Yongxin;Ge, Yaojun;Mendis, Priyan;Mohotti, Damith
    • Wind and Structures
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    • v.21 no.2
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    • pp.223-239
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    • 2015
  • Open decks are a widely used deck configuration in long-span cable-stayed bridges; however, incorporating aerodynamic countermeasures are advisable to achieve better aerodynamic performance than a bluff body deck alone. A sectional model of an open deck cable-stayed bridge with a main span of 400 m was selected to conduct a series of wind tunnel tests. The influences of five practical aerodynamic countermeasures on flutter and vortex-induced vibration (VIV) performance were investigated and are presented in this paper. The results show that an aerodynamic shape selection procedure can be used to evaluate the flutter stability of decks with respect to different terrain types and structural parameters. In addition, the VIV performance of $\prod$-shaped girders for driving comfortableness and safety requirements were evaluated. Among these aerodynamic countermeasures, apron boards and wind fairings can improve the aerodynamic performance to some extent, while horizontal guide plates with 5% of the total deck width show a significant influence on the flutter stability and VIV. A wind fairing with an angle of $55^{\circ}C$ showed the best overall control effect but led to more lock-in regions of VIV. The combination of vertical stabilisers and airflow-depressing boards was found to be superior to other countermeasures and effectively boosted aerodynamic performance; specifically, vertical stabilisers significantly contribute to improving flutter stability and suppressing vertical VIV, while airflow-depressing boards are helpful in reducing torsional VIV.

Development of Design and Field Quality Control Techniques of Shallow Foundation Resting on Intermediate Geomaterials (중간토에 지지된 직접기초의 설계 및 현장품질관리기법 개발)

  • Byun, Young-Gi;Park, Young-Ho;Jeong, Hoon-Jun;Lee, Woo-Jin
    • Proceedings of the Korean Geotechical Society Conference
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    • 2010.03a
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    • pp.1148-1155
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    • 2010
  • To suggest a modified shallow foundation design method which can be considered the scale effect of foundation on IGM(intermediate geomaterial) soil layer, the weathered soil layer that is uniformly formed up to 8m(2B) with over 50 N-value is selected and 3 times field loading tests are performed on several sized square-shaped shallow foundations with 30, 75, 150, 240 and 400cm in width respectively. Because the soil modulus of elasticity(Es) calculated by soil investigation and 1st field test(PBT) results showed an underestimated tendency, a modified correlation is required for the reasonable estimation of Es on the weathered soil. Also, the N-value was increased with an increasing in depth. However, the N-values around the test foundations showed the different values even though the foundations on the same level because the test site was arranged by excavation. Therefore, the more detail soil investigations are required for the each test foundations respectively. Since Es based on elasticity theory is determined by the stress distribution shape of the foundation and elasticity modulus of the soil, the scale effect considered pressure-settlement curve can be clearly derived from the correlation on stress distribution shape and the variation of soil elasticity modulus with depth. Therefore, the modified correlation will be suggested to estimate a reasonable Es on the weathered soil, and the scale effect considered shallow foundation design method is also developed based on the elastic theory and field tests in this research.

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Low-Temperature Selective Catalytic Reduction of No with NH3 over Mn-V2O5/TiO2 (Mn-V2O5/TiO2 촉매의 NH3에 의한 NO의 저온 선택적 촉매환원)

  • Choi, Sang-Ki;Choi, Sung-Woo
    • Journal of Environmental Science International
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    • v.15 no.4
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    • pp.333-340
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    • 2006
  • A (5 wt.%)Mn-(1 wt.%)$V_{2}O_{5}/TiO_{2}$ catalyst were prepared by co-precipitation method and used for low-temperature selective catalytic reduction (SCR) of $NO_x$ with ammonia in the presence of oxygen. The properties of the catalysts were studied by X-ray diffraction (XRD), temperature programmed reduction (TPR) and scanning electron microscope-energy dispersive X-ray spectroscopy (SEM-EDS). The experimental results showed that (5 wt.%)Mn-(1 wt.%)$V_{2}O_{5}/TiO_{2}$ catalyst yielded 81% NO conversion at temperature as low as $150^{\circ}C$ and a space velocity of $2,400\;h^{-1}$. Crystalline phase of $Mn_{2}O_3$ was present at ${\ge}\;15%$ Mn on $V_{2}O_{5}/TiO_{2}$. XRD confirmed the presence of manganese oxide ($Mn_{2}O_{3}$) at $2{\theta}=32.978^{\circ}(222)$. The XRD patterns presented of (5 wt.%)Mn-(1 wt.%)$V_{2}O_{5}/TiO_{2}$ did not show intense or sharp peaks for manganese oxides and vanadia oxides. The TPR profiles of (5 wt.%)Mn-(1 wt.%)$V_{2}O_{5}/TiO_{2}$ catalyst showed main reduction peat of a maximum at $595^{\circ}C$.

Capacitive Voltage Divide for a Pulsed High-Voltage Measurement (펄스형 고전압 측정용 용량성 분압기)

  • Jang Sung-Duck;Son Yoon-Kyoo;Kwon Sei-Jin;Oh Jong-Seok;Cho Moo-Hyun
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.54 no.2
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    • pp.63-68
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    • 2005
  • Total 12 units of high power klystron-modulator systems as microwave source are under operation for 2.5 GeV electron linear accelerator in Pohang Light Source (PLS) linac. The klystron-modulator system has an important role for the stable operation to improve an availability statistics of overall system performance of klystron-modulator system. RF power and beam power of klystron are precisely measured for the effective control of electron beam. A precise measurement and measurement equipment with good response characteristics are demanded for this. Input power of klystron is calculated from the applied voltage and the current on its cathode. Tiny measurement error severely effects RF output power value of klystron. Therefore, special care is needed to measure precise beam voltage. Capacitive voltage divider (CVD), which divides input voltage as capacitance ratio, is intended for the measurement of a beam voltage of 400 kV generated from the klystron-modulator system. Main parameter to determine standard capacitance in the high arm of CVD is dielectric constant of insulation oil. Therefore CVD should be designed to have a minimum capacitance variation due to voltage, frequency and temperature in the measurement range. This paper will be present and discuss the design concept and analysis of capacitive voltage divider for a pulsed high-voltage measurement, and the empirical relations between capacitance effects and oil temperature variation.