• Title/Summary/Keyword: 3MS

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Distribution Characteristics of Organic Matters and Nutrients in Surface Sediments of Yeongsan River Basin (영산강 수계 표층 퇴적물의 유기물 및 영양염류 분포 특성)

  • Bong, Kimoon;Kang, Taewoo;Yang, Haejong;Han, Jonghak;Yang, Wonjun;Jeong, Hyojin;Jung, Heejung;Hwang, Soonhong;Kim, Kyunghyun
    • Journal of the Korean Society of Urban Environment
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    • v.18 no.4
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    • pp.455-463
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    • 2018
  • This study was carried out to assess the distribution and pollution level of organic matters and nutrients in surface sediments of the Yeongsan River Basin. The surface sediments were collected from the mainstream (12) and tributaries sites (4) for two years from 2015 to 2016, and the particle sizes, organic matters (Ignition Loss, COD, TOC) and nutrients (TN, TP, SRP) were analyzed. The distribution of particle sizes was dominated by sand in the upstream sites (MS1-MS7) and by silt loam in the downstream sites (MS8-MS12), but MS3 and MS6, located slightly upstream of the two weirs, were found to be mostly loamy sand and silt loam, respectively. As a results of the correlation assessment, the organic matters (IL, COD, TOC) were strongly correlated with particle sizes, while the nutrients (TP, SRP) were weak except for TN. The concentrations of organic matter and nutrient were higher at the downstream and the sites nearby the two weirs (MS3, MS6). In particular, the TP concentration at the MS3 site sampled in the second half period of the years was higher than that in the first half periods. Comparing of sediments criteria, the organic matters and nutrients were evaluated to have almost no toxic effects at all sites.

FPGA implementation of high temperature feature points extraction algorithm for thermal image (열화상 이미지에 대한 고온 특징점 추출 알고리즘의 FPGA 구현)

  • Ko, Byoung-Hwan;Kim, Hi-Seok
    • Journal of IKEEE
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    • v.22 no.3
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    • pp.578-584
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    • 2018
  • Image segmentation has been presented in the various method in image interpretation and recognition, and the image is using separate the characteristics of the specific purpose. In this paper, we proposed an algorithm that separate image for feature points detected to high temperature in a Thermal infrared image. In order to improve the processing time, the proposed algorithm is implemented to FPGA Hardware Block using the Zynq-7000 Evaluation Board environment. The proposed High-Temperature Detection Algorithm and total FPGA blocks show a decrease of a processing time result from 16ms to 0.001ms, and from 50ms to 0.322ms respectively. It is also verified similar results of the PSNR to comparing software thermal testbench and hardware ones.

Analysis of Pesticides in Herbal Medicine by QuEChERS and GC-MS/MS (QuEChERS 전처리와 GC-MS/MS를 활용한 생약의 잔류농약 분석 가능성 연구)

  • Seo, Go Eun;Kim, A Young;Pyo, Byoung Sik;Lee, Kyoung in
    • Korean Journal of Pharmacognosy
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    • v.51 no.3
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    • pp.207-216
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    • 2020
  • The analysis method for qualitative analysis of the screening method that can be performed prior to the quantitative analysis of individual pesticide was reviewed in order to meet the safety standards that are being strengthened in the field of pesticide residue testing of herbal medicines. Among the residual pesticides presented in the Korean Pharmacopoeia, 56 pesticides, excluding 15 pesticides that need to be individually analyzed, were selected for analysis using QuEChERS preprocessing and GC-MS/MS, which are used in the existing agricultural products field. For each pesticide, the detection limit level of 0.001-0.005 mg/kg and the quantitative limit level of 0.002-0.017 mg/kg were confirmed. In the recovery test in which the standard was treated at a concentration of 0.02 mg/kg, it was confirmed that the proportion of pesticides satisfying the recovery of 70-120% was 85.7-96.4% for each herbal medicine, so it was confirmed that it was a level that could be reviewed by the screening method.

Voice/Data Integration and Performance Analysis using Mobile If on the VoIP Network for the service of CDMA-2000 (CDMA-2000 서비스를 위한 VoIP 기반 망에서 Mobile IP를 이용한 음성/데이타 통합 및 성능평가)

  • Eom, Ki-Bok;Yoe, Hyun;Lee, Yoon-Ju
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2001.10a
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    • pp.89-92
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    • 2001
  • In this paper, it is proposed that RSVP and WFQ must be a good way of a better service for the better quality for Mobile If Network. For the Performance Analysis of working it was composed of Mobile IP and VoIP Network model, and further more test of the postpone and QoS was implemented. The results of the test is as follows, Before the movement of mobile agent was 2ms, after that, 3ms, And before QoS was adapted the value was 30ms, after being adapted, analyzed as 10ms. This research that the problem of put off was improved by adaping QoS in the mobile IP Network.

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Electrical and Mechanical Properties of Epoxy/Heterogeneous Inorganic Composites Materials for the Application of Electric Power GIS Appliances (친환경 GIS용 전력기기의 적용을 위한 에폭시 이종무기물 복합재료의 전기적, 기계적 특성)

  • Park, Jae-Jun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.67 no.12
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    • pp.1633-1640
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    • 2018
  • Epoxy resin is a polar thermosetting polymer that is widely employed in different branches of industry and everyday life, due to their stable physical and chemical properties. Of all the polymer materials currently being used in the electrical insulation industry, epoxy resin is the most widely used kind, chosen as the base polymer material in the present study. Composites were prepared according to the mixing ratio (MS: MA, 1: 9, 3: 7, 5: 5, 7: 3, 9: 1)of mixture for Heterogeneous Minerals(Micro Silica:MS, Micro Alumina:MA) (MS+MA). We have investigated for AC electrical insulation breakdown characteristics and the dielectric properties (permittivity, dielectric loss, and conductivity) with frequency changes. The electrical AC insulation breakdown performance was improved with the increase of the mixing ratio of MS according to heterogeneous mineral material mixture(MS+MA). As Dielectric properties, the dielectric constant and dielectric loss increased with decreasing frequency and decreased with increasing MS content ratio of heterogeneous mineral mixture. Tensile strength and flexural strength according to the mixing ratio (MS + MA) of epoxy / heterogeneous mineral mixture were studied by mechanical properties. The performance of mechanical tensile and flexural strength was significantly improved as the fill contents ratio of MS increased.

Validation of simultaneous mycotoxin analysis method in pet food using LC-MS/MS (LC-MS/MS를 이용한 반려동물 사료에서 곰팡이독소 동시분석법 유효성 확인)

  • Choi, Yoon Hwa;Ahn, Woo Seok;Kim, Ji Eun;Kim, Doo Hwan
    • Korean Journal of Veterinary Service
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    • v.45 no.3
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    • pp.237-242
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    • 2022
  • The simultaneous analysis of mycotoxins using LC-MS/MS, a food official analysis method, was applied with compound feed for pets with high consumer preferences. In this study, the linearity of all calibration curves showed good linearity of 0.99 or more. and both the accuracy (recovery rate) and precision (repeatability) criteria of the concentration range for each mycotoxin in the National Agricultural Products Quality Management Service's Validation and Verification Guidelines were met. And as a result of analyzing FAPAS QCM in the same way, it was assesed that the z-scores of Aflatoxin B1, Ochratoxin A, Zearalenone, and Fumonisin B1, were within ±2 range. This study showed that the application of the food official analysis method to compound feed for pets is suitable.

Development of Simultaneous Analysis for Multiple Agricultural Pesticides in Raw Milk Products using GC-MS/MS (GC-MS/MS를 이용한 원유 원료 중 농약 동시분석법 확립)

  • Young Nae Choi;Yoon ho Shin;Hwangeui Cho;Jung Bok Kim
    • Journal of Food Hygiene and Safety
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    • v.38 no.6
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    • pp.420-429
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    • 2023
  • GC-MS/MS using liquid-liquid extraction (LLE) and C18 cartridges was used to identify and quantify levels of chlorpyrifos, chlorpyrifos-methyl, cypermethrin, deltamethrin and permethrin in bulk raw milk. A calibration curve spanning 10 ng/mL to 200 ng/mL was obtained with a satisfactory correlation coefficient of 0.99. The limits of detection (LOD) and limits of quantitation (LOQ) for chlorpyrifos, chlorpyrifos-methyl, cypermethrin, deltamethrin, and permethrin in the matrix ranged from 0.06 to 1.81 ng/mL and 0.19 to 6.04 ng/mL, respectively. The recoveries of 5 pesticides from spiked samples at 37.5-125 ng/mL ranged from 86.1 to 102.1%. The measurement of uncertainty of the GC-MS/MS method for these five pesticides was developed based on the analytical process and quantification. An analysis method that is easier and faster than the method specified in the Korean food standards codes for analyzing these five pesticides in raw material milk was developed. Moreover, the analytical method for chlorpyrifos, chlorpyrifos-methyl, cypermethrin, deltamethrin, and permethrin in bulk raw milk by GC-MS/MS was established.

The Study of Generation of Adduct and Fragment Ions by LC/TSP/MS (LC/TSP/MS에 의한 이온종들의 생성에 관한 연구)

  • Kim, Yunje
    • Analytical Science and Technology
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    • v.9 no.1
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    • pp.1-12
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    • 1996
  • The thermally labile compounds with hydroxyl group generate the [${MNH_4}^+$] ion, [$MH^+$] and [$MH^+-OH$] ion by ion-molecule reaction in LC/TSP/MS. But these ions create the trouble in the estimation of molecular weight of an unknown compound because the margin of [${MNH_4}^+$] ion and [$MH^+$] ion is same to that of [$MH^+$] ion and [$MH^+-OH$] ion. If it is compensated for the results by using of the $CF_3COOD+NH_4OH$ LC eluent, the molecular weight of analyte will be able to be confirmed. And this study was tried to recognize whether the fragment ions of thermally labile compound are generated by electron impact or by thermal degradation in ion source.

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A Fast and Sensitive Method for the Simultaneous Determination and Quantification of Six Anionic Surfactants in Surface Water using HILIC-ESI-MS Technique

  • Dash, Upendra N.;Paul, Saroj Kumar
    • Mass Spectrometry Letters
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    • v.3 no.3
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    • pp.78-81
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    • 2012
  • The hydrophobic hydrocarbon chain and the polar sulfate group confer surfactant properties and enable them to be used as anionic surfactants. Anionic surfactants (AS) are known for their adverse impact on environment, particularly on aquatic ecosystem. In the present study a fast, sensitive and selective method for the determination and subsequent quantification of six anionic surfactants was developed using hydrophilic interactive liquid chromatography (HILIC) coupled to a electrospray ionization (ESI) mass spectrometer (MS), in the concentration range 15-20 ${\mu}g/L$. The capability of the method was established using regression analysis and ANOVA. The method performance was evaluated by analyzing real time surface water spiked with 1-dodecyl hydrogen sulfate at 15 ${\mu}g/L$. Combined efficiency of solid phase extraction and MS detection established recovery of 89% in presence of natural matrix. These results point out that HILIC coupled to multistage MS procedures can be a powerful technique for environmental applications concerning the screening of polar contaminants.

A Design of Hierarchical Tile-based Rasterizer Using The Improved Tiling Algorithm (타일링 속도를 개선한 계층 구조 타일 기반 Rasterizer 설계)

  • Kim, Do-Hyun;Kyung, Gyu-Taek;Kwak, Jae-Chang;Lee, Kwang-yeob
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2014.10a
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    • pp.309-311
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    • 2014
  • The tile-based rendering technique which divides the screen area into tiles of a specific size and creates a 3D graphic model of one tile at a time is used to efficiently utilize limited resources in a 3D graphic pipeline. In this paper, the tiling speed of tile-based rendering was improved by reducing the count of calling lower-levels in the hierarchical tile-based rendering technique. The tiling speed of the proposed Rasterizer is 13.030ms which is 56% faster than 29.614ms of multi-sort tiling and 24% faster than 17.208ms of the conventional hierarchical tiling technique.

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