• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 추계학술대회 논문집
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• pp.818-823
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• 2005

Creep damage is one of the mosl important characteristics for the stability of high temperature structures such as huge energy converting facilities. Creep failure of Type 316LN stainless steel is highly correlated to generation and growth of the voids. In this paper, in order to investigate the correlation of creep rupture time and ultrasonic parameters (group velocity, angular velocity), creep-damaged Type 316LN specimens and measurements for the ultrasonic parameters were made. However, bi-directional measurements were applied along the load direction and the perpendicular direction to the load line by means of the contact type probe of which the central frequencies are 10MHz, 15MHz and 20MHz. Analyzing the angular velocities of the ultrasonic signals obtained from the load direction, it was confirmed that the angular velocities were declined as the creep time passed when 15MHz and 20MHz probes were used. Also, the group velocities were declined for all three frequencies as the creep time increased. Thus, positive feasibility for the creep damage evaluation by means of the angular and group velocities was confirmed. Moreover, result of analysis for the ultrasonic signal which was obtained from the perpendicular direction upon the angular and group velocities indicated little variation for both of the angular and group velocities. Therefore, the creep damage is likely to represent anisotropic itself.

• Nuclear Engineering and Technology
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• 제53권2호
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• pp.647-656
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• 2021

Knowing a material's true stress-strain curve is essential for performing a nonlinear finite element analysis to solve an elastoplastic problem. This study presents a simple methodology to determine the true stress-strain curve of type 304 and 316 austenitic stainless steels in the full range of strain from a typical tensile test. Before necking, the true stress and strain values are directly converted from engineering stress and strain data, respectively. After necking, a true stress-strain equation is determined by iteratively conducting finite element analysis using three pieces of information at the necking and the fracture points. The Hockett-Sherby equation is proposed as an optimal stress-strain model in a non-uniform deformation region. The application to the stainless steel under different temperatures and loading conditions verifies that the strain hardening behavior of the material is adequately described by the determined equation, and the estimated engineering stress-strain curves are in good agreement with those of experiments. The presented method is intrinsically simple to use and reduces iterations because it does not require much experimental effort and adopts the approach of determining the stress-strain equation instead of correcting the individual stress at each strain point.

• 한국세라믹학회지
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• 제45권3호
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• pp.161-166
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• 2008

The multi-films of a metallic film and a transparent conducting oxide (TCO, indium-tin oxide, ITO) film were formed on the stainless steel 316 and 304 plates by a sputtering method and an E-beam method and then the external metallic region of the stainless steel bipolar plates was converted into the metal nitride films through an annealing process. The multi-film formed on the stainless steel bipolar plates showed the XRD patterns of the typical indium-tin oxide, the metallic phase and the metal substrate and the external nitride film. The XRD pattern of the thin film on the bipolar plates modified showed two metal nitride phases of CrN and $Cr_2N$ compound. Surface microstructural morphology of the multi-film deposited bipolar plates was observed by AFM and FE-SEM. The metal nitride film formed on the stainless steel bipolar plates represented a microstructural morphology of fine columnar grains with 10 nm diameter and 60nm length in FE-SEM images. The electrical resistivity of the stainless steel bipolar plates modified was evaluated.

• Corrosion Science and Technology
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• 제20권2호
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• pp.52-61
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• 2021

This study using experimental design and linear regression technique was implemented in order to predict the pitting potential of stainless steel in marine environments, with the target materials being AL-6XN and STS 316L. The various variables (inputs) which affect stainless steel's pitting potential included the pitting resistance equivalent number (PRNE), temperature, pH, Cl^- concentration, sulfate levels, and nitrate levels. Among them, significant factors affecting pitting potential were chosen through an experimental design method (screening design, full factor design, analysis of variance). The potentiodynamic polarization test was performed based on the experimental design, including significant factor levels. From these testing methods, a total 32 polarization curves were obtained, which were used as training data for the linear regression model. As a result of the model's validation, it showed an acceptable prediction performance, which was statistically significant within the 95% confidence level. The linear regression model based on the full factorial design and ANOVA also showed a high confidence level in the prediction of pitting potential. This study confirmed the possibility to predict the pitting potential of stainless steel according to various variables used with experimental linear regression design.

• 대한금속재료학회지
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• 제49권2호
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• pp.153-160
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• 2011

The AISI 216L stainless steel with a composition of Fe-16Cr-6Ni-6Mn-1.7Mo (wt.%) was oxidized at $700{\sim}900^{\circ}C$ in air for 100 h. At $700^{\circ}C$, a thin $Mn_{1.5}Cr_{1.5}O_4$ oxide layer with a thickness of $0.4{\mu}m$ formed. At $800^{\circ}C$, an outer thin $Fe_2O_3$ oxide layer and a thick inner $FeCr_2O_4$ oxide layer with a total thickness of $30{\mu}m$ formed. The non-adherent scale formed at $800^{\circ}C$ was susceptible to cracking. At $900^{\circ}C$, an outer thin $Fe_2O_3$ oxide layer and a thick inner $Mn_{1.5}Cr_{1.5}O_4$ oxide layer formed, whose total thickness was $10{\sim}15{\mu}m$. The scales formed at $900^{\circ}C$ were non-adherent and susceptible to cracking. 216 L stainless steel oxidized faster than 316 L stainless steel, owing to the increment of the Mn content and the decrement of Ni content.

• Corrosion Science and Technology
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• 제20권3호
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• pp.152-157
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• 2021

Stainless steel is a metal that does not generate rust. Due to its excellent workability, economic feasibility, and corrosion resistance, it is used in various industrial fields such as ships, piping, nuclear power, and machinery. However, stainless steel is vulnerable to corrosion in harsh environments. To solve this problem, its corrosion resistance could be improved by electrochemically forming an anodized film on its surface. In this study, 316L stainless steel was anodized at room temperature with ethylene glycol-based 0.1 M NH₄F and 0.1M H₂O electrolyte to adjust the thickness of the oxide film using different anodic oxidation voltages (30 V, 50 V, and 70 V) with time control. The anodic oxidation experiment was performed by increasing the time from 1 hour to 7 hours at 2-hour intervals. Corrosion resistance according to the thickness of the anodic oxide film was observed. Electrochemical corrosion behavior of oxide films was investigated through polarization experiments.

• 한국재료학회지
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• 제13권9호
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• pp.587-592
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• 2003

The thin films of 316L stainless steel were made on glass and S45C substrate by Ion beam assisted deposition with reactive atmosphere of argon and nitrogen. The films were deposited at the various conditions of ion beam power and the ratios of Ar/$N_2$gas. Properties of these films were analyzed by glancing x-ray diffraction method(GXRD), AES, potentiodynamic test, and salt spray test. The results of GXRD showed that austenite phase could be appeared by $N_2$ion beam treatment and the amount of austenite phase increased with the amount of nitrogen gas. The films without plasma ion source treatment had the weak diffraction peak of ferrite phase. But under the Ar plasma ion beam treatment, the strong diffraction peaks of ferrite phase were appeared and the grain size was increased from 12 to 16 nm. Potentiodynamic polarization test and salt spray test indicated that the corrosion properties of the STS 316L films with nitrogen ion source treatment were better than bulk STS 316L steel and STS 316L films with Ar ion source treatment.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2009년도 춘계학술대회 논문집
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• pp.244-245
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• 2009

Sol-gel coatings of $TiO_2$ have been prepared from $TiO_2$ sol and deposited by dip-coating technique on 316L stainless steel sheets in order to study the electrochemical behaviorin corrosive solutions. The influence of the coatings on the chemical corrosion of the substrate has been evaluated by potentiodynamic polarization curves in different aqueous NaCl solution at $25^{\circ}C$.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.64-65
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• 2006

Anisotropic constitutive equations for sintering of metal powder compacts have been formulated from a linear viscous transversely-isotropic model in which an anisotropic sintering stress has been introduced to describe free sintering densification kinetics. The identification of material parameters defined in the model, has been achieved from thermomechanical experiments performed on 316L stainless steel warm-compacted powder in a dilatometer allowing controlled compressive loading.

• 한국해양공학회지
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• 제20권1호
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• pp.1-6
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• 2006

The effects of microstructure on the damping capacity and tensile properties of 316L stainless steel were investigated. Increasing the degree of cold working, the volume fraction of $\varepsilon-martensite$ decreased after rising to maximum value at specific level of cold working, the volume fraction of d-martensite slowly increased and then dramatically increased from the point of decreasing $\varepsilon-martensite$ volume fraction. Increasing the degree of cold working, the behnvior of damping capacity is similar to that of the $\varepsilon-martensite$. After the damping capacity showing the maximum value at about $20\%$ of cold rolling, damping capacity was decreased with the volume fraction of $\varepsilon-martensite$. Tensile strength was proportional to the volume fraction of d-martensite, and elongation steeply decreased in the range low volume fraction of a'-martensite, then slowly decreased in range the above $10\%$ volume fraction of d-martensite. The damping capacity and elongation is strongly controlled by the volume fraction of $\varepsilon$ martensite with liner relationship. However, the effect of the volume fraction of d-martensite and austenite phase on the damping capacity was not observed. Tensile strength was governed by the volume fraction of d-martensite.