• The Journal of Advanced Prosthodontics
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• v.1 no.3
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• pp.113-117
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• 2009

STATEMENT OF PROBLEM. Recently Yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) has been introduced due to superior flexural strength and fracture toughness compared to other dental ceramic systems. Although zirconia has outstanding mechanical properties, the phenomenon of decrease in the life-time of zirconia resulted from degradation in flexural strength after low temperature aging has been reported. PURPOSE. The objective of this study was to investigate degradation of flexural strength of Y-TZP ceramics after various low temperature aging treatments and to evaluate the phase stability and micro-structural change after aging by using X-ray diffraction analysis and a scanning electron microscope (SEM). MATERIAL AND METHODS. Y-TZP blocks of Vita In-Ceram YZ (Vita Zahnfabrik, Bad $S\ddot{a}ckingen$, Germany) were prepared in 40 mm (length) $\times$ 4 mm (width) $\times$ 3 mm (height) samples. Specimens were artificially aged in distilled water by heat-treatment at a temperature of 75, 100, 125, 150, 175, 200, and $225^{\circ}C$ for 10 hours, in order to induce the phase transformation at the surface. To measure the mechanical property, the specimens were subjected to a four-point bending test using a universal testing machine (Instron model 3365; Instron, Canton, Mass, USA). In addition, X-ray diffraction analysis (DMAX 2500; Rigaku, Tokyo, Japan) and SEM (Hitachi s4700; Jeol Ltd, Tokyo, Japan) were performed to estimate the phase transformation. The statistical analysis was done using SAS 9.1.3 (SAS institute, USA). The flexural strength data of the experimental groups were analyzed by one-way analysis of variance and to detect statistically significant differences ($\alpha$= .05). RESULTS. The mean flexural strength of sintered Vita In-Ceram YZ without autoclaving was 798 MPa. When applied aging temperature at below $125^{\circ}C$ for 10 hours, the flexural strength of Vita In-Ceram YZ increased up to 1,161 MPa. However, at above $150^{\circ}C$, the flexural strength started to decrease. Although low temperature aging caused the tetragonal-to-monoclinic phase transformation related to temperature, the minimum flexural strength was above 700 MPa. CONCLUSION. The monoclinic phase started to appear after aging treatment above $100^{\circ}C$. With the higher aging temperature, the fraction of monoclinic phase increased. The ratio of monoclinic/tetragonal + monoclinic phase reached a plateau value, circa 75% above $175^{\circ}C$. The point of monoclinic concentration at which the flexural strength begins to decrease was between 12% and 54%.

• Journal of Technologic Dentistry
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• v.37 no.3
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• pp.107-113
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• 2015

Purpose: This study provided the basic data for selecting the zirconia blocks by comparing the mechanical properties of the all ceramic crown between the domestic, import, translucent and shade blocks that were used in clinically. Methods: Currently, the most commercial block of five types(one import and two domestic block which is the translucent and shade) were used. It were elucidated by means of three point bending test, hardness test, FE-SEM observations and EDX analysis. The results were analyzed using a one-way ANOVA and Scheffe post hoc test for significant findings. Results: For flexural strength, LT specimen was the highest as 733.1 MPa, followed by JT specimen(712.0 MPa), ZT specimen(646.0 MPa), LS specimen(553.1 MPa), JS specimen(429.0 MPa). One-way ANOVA showed statistically significant difference between groups for flexural strength(p<0.05). For hardness, ZT specimen was the highest as 1556.5 Hv, followed by JT specimen(1540.3 Hv), LT specimen(1512.3 Hv), JS specimen(1472.0 Hv), LS specimen(1353.3 Hv). One-way ANOVA showed statistically significant difference between groups for hardness(p<0.05). Conclusion: Domestic block was higher than import block for flexural strength, and translucent block was higher than shade block for flexural strength. However, all blocks showed clinically acceptable range. There was no significant difference in hardness between domestic and import blocks. And significant difference was observed in translucent and shade blocks.

• Journal of the Korean Ceramic Society
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• v.43 no.3 s.286
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• pp.193-197
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• 2006

Symmetric three-layer $Al_2O_3/ZrO_2$ composite has been prepared by freeze casting and pressureless sintering at $1400-1600^{\circ}C$ in air. The layered material sintered at $1600^{\circ}C$ showed the maximum fracture strength (410 MPa), measured by a four-point bending test. Contact damage strength was superior in three-layer composite compared with corresponding mono-layered material, possibly due to the development of relatively large compressive stress. The grain growth of $ZrO_2$ particles was mainly governed by coalescence mechanism.

• Computers and Concrete
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• v.19 no.4
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• pp.375-385
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• 2017

In the present paper experimental and numerical analysis of hook-ended steel fiber reinforced concrete is carried out. The experimental tests are performed on notched beams loaded in 3-point bending using fiber volume fractions up to 1.5%. The numerical analysis of fiber reinforced concrete beams is performed at meso scale. The concrete is discretized with 3D solid finite elements and microplane model is used as a constitutive law. The fibers are modelled by randomly generated 1D truss finite elements, which are connected with concrete matrix by discrete bond-slip relationship. It is demonstrated that the presented approach, which is based on the modelling of concrete matrix using microplane model, able to realistically replicate experimental results. In all investigated cases failure is due to the pull-out of fibers. It is shown that with increase of volume content of fibers the effective bond strength and slip capacity of fibers decreases.

• Transactions of the Korean Society of Automotive Engineers
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• v.18 no.6
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• pp.38-45
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• 2010

Welding structures are designed to endure its expected life. The most important factors are life. Especially on welded structure, fatigue strength is critical. So this study performed a research on Box and T shape weldment specimen to examine the influence of welding type. In this experiment, the results indicate Box shape was available in more than T shape. Fatigue tests were performed to evaluate the fatigue strength of the both as-welded and statically pre-loaded specimens by 3 point bending load. Fatigue life can be improved by using Ultrasonic Impact Treatment(UIT) effect. Ultrasonic Impact Treatment(UIT) is excellent for eliminating the tensile residual stresses and generating compressive residual stresses which elevate fatigue strength of welded structures. Also, this shows that welding part has better fatigue life and welding was performed well. In this study, to evaluate the Ultrasonic Impact Treatment(UIT) effect, for welding structure, the experiment was conducted at various levels of stress range between 100MPa and 500MPa. From the test results, it was indicated that fatigue performance was improving by Ultrasonic Impact Treatment(UIT)

• Journal of Industrial Technology
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• v.18
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• pp.363-370
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• 1998

This study focused on the development of an alternative stress estimation procedure to instantly calculate the critical stresses bonded concrete pavement. Closed form analysis is commonly used to analyze pavement structures. This type of analysis assumes linearelastic material properties and static loading conditions. The well-known ILLI-SLAB finite element program was used for the analysis. Bonded concrete overlay analyzed the stress distribution, behavior and load carrying capacity under track load is made evaluation standard of bonded concrete overlay. In the study, the following results were derived ; The properties of strength is that compress and 3-point bending strength of existing pavement is deteriorated with $184kg/cm^2$, $59kg/cm^2$ but compress and splitting tensile strength of overlay is satisfied with $465kg/cm^2$, $45kg/cm^2$. Load transfers is happen at adjacent slab by interlocking under track load. The stress distribution under interior, corner and edge load is described high loading position surrounding then loading position.

• Korean Journal of Metals and Materials
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• v.49 no.9
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• pp.726-731
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• 2011

The present work shows how the flexural displacement-induced fracture strength of silicon devices, whose back surfaces have wafer grinding-induced scratch marks, depends on the crystallographic orientation. Experimental results indicate that silicon devices with scratch marks parallel to their lateral direction (i.e. reference axis in this work) are very susceptible to flexural fracture, as compared to devices with marks which deviated from the direction. The 3-point bending test shows that the fracture strength of silicon devices having marks which are oriented away from the reference axis is 2.6 times higher than that of devices with marks parallel to the axis. It was particularly interesting to see that silicon devices with identical preferred marks even reveal different fracture strengths, depending on whether the marks are involved in specific crystal planes such as {111} or {011}, called cleavage planes. This work demonstrates that silicon devices with the reference axis-aligned scratch marks not existing on such cleavage planes can have higher fracture strength approximately 20% higher than those existing on the planes.

• The Journal of Advanced Prosthodontics
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• v.6 no.4
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• pp.266-271
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• 2014

PURPOSE. The purpose of this study was to compare the fracture strength of the metal and the bond strength in metal-ceramic restorations produced by selective laser sintering (SLS) and by conventional casting (CAST). MATERIALS AND METHODS. Non-precious alloy (StarLoy C, DeguDent, Hanau, Germany) was used in CAST group and metal powder (SP2, EOS GmbH, Munich, Germany) in SLS group. Metal specimens in the form of sheets ($25.0{\times}3.0{\times}0.5mm$) were produced in accordance with ISO 9693:1999 standards (n=30). To measure the bond strength, ceramic was fired on a metal specimen and then three-point bending test was performed. In addition, the metal fracture strength was measured by continuing the application of the load. The values were statistically analyzed by performing independent t-tests (${\alpha}=.05$). RESULTS. The mean bond strength of the SLS group (50.60 MPa) was higher than that of the CAST group (46.29 MPa), but there was no statistically significant difference. The metal fracture strength of the SLS group (1087.2 MPa) was lower than that of the CAST group (2399.1 MPa), and this difference was statistically significant. CONCLUSION. In conclusion the balling phenomenon and the gap formation of the SLS process may increase the metal-ceramic bond strength.

• Journal of Advanced Marine Engineering and Technology
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• v.12 no.3
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• pp.57-67
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• 1988

Although handicapped by the inability to bridge the size gap between small laboratory sample and large engineering component, the V charpy test sample method does possess certain advantages, such as each of preparation, simplicity of test method, speed, low cost in test machinery, and low cost per test. On the other hand, the COD test method does posses advantages, which reduce the size gap between the laboratory sample and actual engineering component. Consequently, the correlation between V charpy absorbed energy and the critical COD value is required for estimating critical COD value from the simple V charpy test results. In this paper, the high tensile strength steel AH36 plate specimens having a single edge cracked notch were investigated to find out the correlation between V charpy absorbed energy and critical COD value in the welded parts under such various welding methods as shielded metal arc welding, the submerged arc welding and the electro gas welding by means of V charpy impact test and static 3-point bending test. Main results obtained are as follow ; 1. The relationships between V charpy absorbed energy Wc' and critical COD value ($\delta_c$)show; $\delta_c$=0.0065 Wc'+0.1906. 2. Ductile- brittle transition behaviours can be estimated by means of fracture appearance and general yielding behaviours. 3. The V charpy absorbed energy of SMAW is higher than that of SAW, EGW and similar relationships are obtained in the COD tests.

• Advances in concrete construction
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• v.13 no.3
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• pp.233-242
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• 2022

An attempt is made to develop an eco-friendly concrete with ground granulated blast furnace slag (GGBS) and pond ash as partial replacement materials for cement and fine aggregate, respectively without compromising the strength and durability. Sixteen concrete mixes were developed by replacing cement and fine aggregate by GGBS and pond ash, respectively in stages of 10%. The maximum replacement levels of cement and fine aggregates were 50% and 30% respectively. Experimental results revealed that the optimum percentage of GGBS and pond ash replacement levels were 30% and 20% respectively. The optimized mix was used further to study the flexural behavior and durability properties. Reinforced Concrete (RC) beams were cast and tested under a four-point bending configuration. Also, the specimens prepared from the optimized mix were subjected to alternate wet and dry cycles of acid (3.5% HCl and H₂SO₄) and sulphate (10% MgSO₄) solutions. Results show that the optimized concrete mix with GGBS and pond ash had a negligible weight loss and strength reduction.