• 제목/요약/키워드: 2212

검색결과 296건 처리시간 0.026초

Phase Stability of Bi2212 and Bi2223 Thin Films Fabricated by ion Beam Sputtering

  • Lee, Hee-Kab;Park, Yong-Pil;Kim, Jeong-Ho
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 추계학술대회 논문집
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    • pp.108-111
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    • 2000
  • Bi2212 and Bi2223 thin films are fabricated by ion beam sputtering method. Three phases of Bi2201, Bi2212 and Bi2223 appear as stable ones in spite of the condition for thin film fabrication of Bi2212 and bi2223 compositions, depending on substrate temperature(T$\sub$sub/) and ozone pressure (PO$_3$). It is found out that these phases show similar T$\sub$sub/ and PO$_3$ dependence, and that the stable regions of these phases are limited within very narrow temperature.

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기판온도와 산화가스압에 따른 Bi-2212 초전도 박막의 단상막 형성에 관한 연구 (A Study on Formation of Single-phase Film in the Bi-2212 Superconducting Thin Films Substrate Temperature and Oxide Gas Pressures)

  • 양승호;이희갑;박용필
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.484-485
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    • 2007
  • BiSrCaCuO superconducting thin films have been fabricated by co-deposition using the faraday cup. Despite setting the composition of thin film Bi2212, Bi(2201, 2212, 2223) phase were appeared. It was confirmed the obtained field of stabilizing phase was represented in the diagonal direction of the right below end in the Arrhenius plot of temperature of the substrate and $PO_3$, and it was distributed in the rezone.

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열처리조건에 따른 Bi-2212 라운드형 선재의 특성 (Characteristics of Bi2212 Round-wire Depending on Heat Treatment Condition)

  • 이남일;장건익;오상수;하동우;김상철
    • 한국초전도ㆍ저온공학회논문지
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    • 제8권3호
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    • pp.1-4
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    • 2006
  • The characteristics of Bi2212 round wire was systematically studied depending on different heat treatment conditions. Initial wire was drawn after routine PIT (Powder In Tube) process. The wire was divided into 3 pieces with 10 cm in length and 2.5 mm in diameter. 3 wires were pre-heat treated separately by different heat treatment schedules, heated in air and nitrogen atmosphere and centrifugally melted. Pre-heated wires were annealed at $845^{\circ}C$ for 40 hours in oxygen atmosphere. SEM results indicate that all pre-heated wires showed highly oriented microstructure. However the wire by centrifugally melted process showed higher density and better electric properties as compared with 2 other wires pre-heated in air and nitrogen atmosphere. The critical current of a centrifugally melted wire was about 18 A in 77 K.

단상막 형성을 위해 기판온도와 산화 가스압에 따른 Bi-2223 초전도 박막의 생성 영역에 관한 연구 (A Study on Produced Region of Bi-2223 Superconducting Thin Films versus substrate temperature and oxide gas pressures for formation of single-phase Film)

  • 양승호;박용필
    • 한국정보통신학회:학술대회논문집
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    • 한국해양정보통신학회 2007년도 춘계종합학술대회
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    • pp.536-539
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    • 2007
  • BSCCO 박막은 다양한 기판온도와 산화 가스압에 변화에서 증발법에 의해 제작되었다. 박막조성을 Bi2212 또는 Bi2223으로 설정했음에도 불구하고, 어느 경우나 Bi2201, Bi2212 및 Bi2223상이 생성되었다. 이들 안정상의 생성 영역은 기판 온도-산화 가스압의 Arrhenius 플롯에서 우측 하단 방향으로 경사진 직선으로 표시되며 매우 좁은 영역에 분포되어 있다. 생성막의 XRD 피크는 기판 온도에 따라 연속적으로 변화했다. 이는 Bi2201, Bi2212, Bi2223의 각상이 결정 구조 내에 혼합되어 있는 혼합 결정계의 존재를 나타내고 있으며, 각 상의 단상막은 매우 좁은 온도, 가스압 범위에서만 생성되었다.

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BSCCO-2212/$SrSO_4$ 벌크 초전도체의 제작 및 특성평가 (Fabrication and characterizations of the BSCCO-2212/$SrSO_4$ bulk superconductors)

  • 김규태;장석헌;박의철;황수민;주진호;홍계원;김찬중;김혜림;현옥배
    • Progress in Superconductivity
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    • 제8권1호
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    • pp.108-112
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    • 2006
  • We fabricated Bi-2212/$SrSO_4$ bulk superconductors by the casting process and evaluated the effects of the powder mixing method and annealing temperature on the texture, microstructure, and critical current. In the process, the Bi-2212 powders were mixed with $SrSO_4$ by hand-mixing(HM) and planetary ball milling(PBM) method and then the powder mixtures were melted at $1100^{\circ}C{\sim}1200^{\circ}C$, solidified, and annealed. We observed that the rod made by the PBM had a more homogeneous microstructure and smaller $SrSO_4$ and second phases than that of the rod made by the HM, resulting in increased $I_c$. The $I_c$ of the rod also depended on the annealing temperature and the highest $I_c$ was obtained to be 200 A when prepared by HM at $1200^{\circ}C$ and annealed at $810^{\circ}C$ which is probably due to the moderate density and 2212 texture and the smaller and less second phase compared to that at higher temperature. The possible causes of the variations of $I_c$ with the powder mixing method and annealing temperature were related to the microstructural evolution based on the SEM, EPMA, and DTA analyses.

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배전급 초전도 한류기 개발을 위한 Bi-2212 초전도 한류소자의 사고전류 제한 특성 (Fault current limitation characteristics of the Bi-2212 bulk coil for distribution-class superconducting fault current limiters)

  • 심정욱;김혜림;임성우;현옥배;이해근;박권배;김호민;이방욱;오일성
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2006년도 제37회 하계학술대회 논문집 B
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    • pp.639-640
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    • 2006
  • We investigated fault current limitation characteristics of the resistive superconducting fault current limiter(SFCL) which consisted of a Bi-2212 bulk coil and a shunt coil. The Bi-2212 bulk coil and the shunt coil were connected in parallel. The Bi-2212 bulk coil was placed inside the shunt coil to induce field-assisted quench. The fault test was conducted at an input voltage of 200 $V_{rms}$ and fault current of 12 $kA_{rms}$ and 25 $kA_{rms}$. The fault conditions were asymmetric and symmetric, and the fault period was 5 cycles. The test results show that the SFCL successfully limited the fault current of 12 $kA_{rms}$ and 25 $kA_{rms}$ to below $5.5{\sim}6.9kA_{peak}$ within $0.64{\sim}2.17$ msec after the fault occurred. Limitation was faster under symmetric fault test condition due to the larger change rate of current. We concluded that the speed of fault current limitation was determined by the speed of current rise rather than the amplitude of a short circuit current. These results show that the Bi-2212 bulk coil is suitable for distribution-class SFCLs.

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원심 용융 성형공정으로 제조된 BSCCO 튜브의 전기적 특성 (Electronical Property of BSCCO Tube Fabricated by Centrifugal Melting Process)

  • 최정숙;오성룡;전병혁;김혜림;현옥배;김형섭;김찬중
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
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    • pp.267-267
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    • 2006
  • 전력에 큰 손실을 초래하는 고장전류를 차단하기 위한 한류기(FCL) 소재로서 고온 초전도체인 BSCCO 2212가 사용된다. 고온에서 용융된 BSCCO 2212 분말은 원심성형법에 의해 한류기용 튜브로 제조되었다. BSCCO 튜브의 기계적 특성을 높이고 용융온도를 낮추기 위해 $SrSO_4$(10wt-%)를 첨가하였다. 용탕은 $1200^{\circ}C$에서 완전히 용융되어 금속 몰드로 주입되었고 원심성형에 사용되는 금속 몰드는 $550^{\circ}C$ 온도로 2시간 예열 후 1020 ~ 2520 RPM으로 회전시켰다. 원심력에 의해 성형된 BSCCO 튜브는 약 48시간 동안 로에서 서냉 후 금속 몰드로부터 분리하였다. 튜브의 용이한 분리를 위해 이형제로서 BSCCO 2212 powder를 사용하였고 임계전류측정을 고려하여 Ag tape 단자를 튜브 끝단에 부착하였다. BSCCO 제조 공정에 있어서 몰드의 예열온도, 용융온도, 몰드 회전속도 등의 변수를 조절하여 최적의 조건을 확립하였다. 제조한 BSCCO 튜브의 임계전류($I_c$)와 임계전류밀도($J_c$)는 77K에서 536A와 $205A/cm^2$ 이었다. 본 연구에서는 BSCCO 2212 튜브를 제조하는 공정조건 변화와 각 조건에서 제조된 BSCCO 2212 튜브의 전기적 특성 및 그에 따른 분석에 대해 기술하였다.

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플라즈마 용사 BSCCO(Bismuth Strontium Calcium Copper Oxide) 초전도 피막의 접합 특성 (Joining Characteristics of Plasma Sprayed BSCCO Superconducting Coatings)

  • 박정식;조창은;고영봉;박광순;박경채
    • 한국표면공학회지
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    • 제46권5호
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    • pp.181-186
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    • 2013
  • We performed plasma spraying for 2001 (Bi:Cu = 2:1), 0212 (Sr:Ca:Cu = 2:1:2) oxide powders. $Bi_2Sr_2CaCu_2Ox$ (2212) superconductor has been prepared by PMP-AT (partial melting process-annealing treatment). The 2212 phase is synthesized between Sr-Ca-Cu oxide coating layer (0212) and Bi-Cu oxide coating layer (2001) by movement of partial melted Bi on 2001 layer and the diffusion reaction (Cu, Sr, Ca) after PMP-AT. There are two different coating layers on joining process. The one is ABAB coating layers and the other is BAAB coating layers by arrangement of 2001 (A), 0212 (B) layers. We performed heat treatment these two different coating layers processes under same PMP-AT conditions. We obtained Bi-2212 superconducting layers at each experimental condition, and the result of MPMS, the critical temperature was showed about 78 K. But the microstructure images and result of EDS as each experimental variable were showed about the qualitatively different Bi-2212 superconducting phases. We also deduced the generation mechanism of Bi-2212 superconducting layer as a result of these experimental data, microstruc ture images, EDS data and phase diagram.