• Proceedings of the KSME Conference
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• 2001.11a
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• pp.222-227
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• 2001

Nonlinear acoustic effect has been considered as an effective tool for the evaluation of material degradation. In this paper, the applicability of nonlinear acoustic effect to the evaluation of degradation of 2.25Cr-1Mo steel is investigated. Firstly, a number of 2.25Cr-1Mo steel samples were heat-treated, and their damage mechanism was examined. Secondly, Ultrasonic nonlinear parameter was measured. Nonlinear acoustic parameter was found to be clearly sensitive to the material degradation.

• Journal of the Korean Society for Nondestructive Testing
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• v.22 no.2
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• pp.170-176
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• 2002

Nonlinear acoustic effect has been considered as an effective tool for the evaluation of material degradation. In this paper, the applicability of nonlinear acoustic effect to the evaluation of degraded 2.25Cr-1Mo steel is investigated. Firstly, artificial aging was performed to simulate the microstructural degradation in 2.25Cr-1Mo steel arising from long time exposure at $540^{\circ}C$. Secondly, ultrasonic nonlinear parameter was quantitatively measured by bi-spectrum and power spectrum. Nonlinear acoustic parameter from bi-spectrum was found to be clearly sensitive to the aging time.

• Journal of the Korean Society for Nondestructive Testing
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• v.21 no.5
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• pp.532-541
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• 2001

Developments of nondestructive evaluation techniques for reduction of strength or toughness by aging of material have been carried out, and the method using electrical resistivity is one of them. In this study, to examine the application of electrical resistivity to the evaluation of degradation of metallic alloy, ten different non-magnetic materials were selected as test materials. Electrical resistivities measured by DC two-point probe method and those measured by non-contact type eddy current method were compared with each other. In addition, to examine the application possibility of four-point probe technology in field, the electrical resistivities for 1Cr-lMo-0.25V steel measured by DC two-point probe method and four-point probe method were compared with each other Differences between two measured values for the 1Cr-1Mo-0.25V steel were 0.6%. Therefore, the four-point probe method can be applied to the estimation of the degradation of metallic alloy. ect.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.37 no.3
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• pp.353-358
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• 2013

The ultrasonic characteristics of 2.25Cr-1Mo steel were investigated in relation to the isothermal heat treatment temperature and time. Charpy impact tests and hardness tests were conducted on individual specimens with three different heat treatment conditions. A pulse-echo method with longitudinal waves was used to measure the attenuation and velocity of ultrasonic waves. The FATT (fracture appearance transition temperature) increased with an increase in the isothermal heat treatment time, which implies that the toughness decreased. As the isothermal heat treatment time and temperature increased, the longitudinal wave velocity and ultrasonic attenuation coefficient were raised.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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• 2003.10a
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• pp.97-99
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• 2003

In order to confirm the possibility of application of laser welding process to 2.25Cr-1Mo steel, the characteristic of residual stress distribution in welds by SMAW and $CO_{2}$ Laser welding process have been investigated and compared using the numerical analysis. As the Result of the numerical analysis, the possibility of application of laser welding process has been found out in respect to the welding residual stress distribution and mechanical properties in welds.

• Proceedings of the KWS Conference
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• 2010.05a
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• pp.19-19
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• 2010

Mo 변화에 따른 Cr-Mo 강의 미세조직 및 물성병화를 알아보기 위해 새로 디자인된 용접봉을 사용하여 Flux cored arc welding(FCAW) 공정으로 용접하였다. 또한 고온에서의 용접부 물성을 알아보기 위하여 각각의 시편을 $400^{\circ}C$, $500^{\circ}C$, $600^{\circ}C$, $700^{\circ}C$에서 24시간 동안 열처리 하였다. 용접부의 미세조직은 미세한 베이나이트 및 침상 페라이트로 구성되었으며 Mo의 함량이 높아질수록 베이나이트 조직이 증가하여 경도 및 강도가 증가하였다. 높은 항복강도와 인장강도를 가지며 연신율이 매우 낮음을 관찰하였다. 열처리후의 미세조직은 $400^{\circ}C$, $500^{\circ}C$는 템퍼드 베이나이트 조직이 나왔으나 $600^{\circ}C$에서 베이나이트 조직이 성장하였다. $700^{\circ}C$ 로 갈수록 베이나이트가 감소하고 페라이트로 미세조직이 변태 하였으며 탄화물의 석출 및 성장이 관찰되었다. 이로 인하여 경도값이 $400^{\circ}C$, $;500^{\circ}C$ 에서 증가하였고 $600^{\circ}C$는 소폭 감소하였으며 $700^{\circ}C$의 경우 완전 페라이트 조직의 형성으로 경도가 크게 감소하고 Mo 함량에 따른 경도 차이 또한 보이지 않았다.

• Journal of the Korean institute of surface engineering
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• v.51 no.3
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• pp.149-156
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• 2018

The corrosion and strength degradation characteristics of 1.25Cr-0.5Mo steels were studied under $650^{\circ}C$ in $76%N_2+6%O_2+16%CO_2+2%SO_2$ gas condition up to 500 hrs. Corroded specimens were characterized by weight gain, scanning electron microscope(SEM), energy dispersive X-ray spectroscopy(EDS), and X-ray diffraction(XRD). The tensile test was conducted to evaluate the mechanical strength and fracture mode with corrosion at high temperature. As the results of the experiments, thick Fe-rich oxide layers over $200{\mu}m$ were formed on the surface within 500 hrs. The thick oxide layers are formed with reduction of the cross-sectional area of the specimens. Thus, the strength tended to decrease with reduction of the cross-sectional area.

• Journal of the Korean institute of surface engineering
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• v.51 no.6
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• pp.354-359
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• 2018

NaCl-induced hot corrosion behavior of ASTM T22 (Fe-2.25Cr-1Mo), T91 (Fe-9Cr-1Mo), T92 (Fe-9Cr-1.8W-0.5Mo), 347HFG (Fe-18-Cr-11Ni), and 310H (Fe-25Cr-19Ni) steels was studied after spraying NaCl on the surface. During corrosion at $600-800^{\circ}C$ for 50-100 h, thick, non-adherent, fragile, somewhat porous oxide scales formed. All the alloys corroded fast with large weight gains owing to fast scaling and destruction of protective oxide scales. Corrosion rates increased progressively as the corrosion temperature and time increased. Corrosion resistance increased in the order of T22, T91, T92, 347HFG, and 310H, suggesting that the alloying elements of Cr, Ni, and W beneficially improved the corrosion resistance of steels. Basically, Fe oxidized to $Fe_2O_3$, and Cr oxidized to $Cr_2O_3$, some of which further reacted with FeO to form $FeCr_2O_4$ or with NiO to form $NiCr_2O_4$.

• Proceedings of the KWS Conference
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• 2000.10a
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• pp.214-215
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• 2000

• Journal of the Korean Society for Heat Treatment
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• v.30 no.2
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• pp.43-52
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• 2017

Heat treatment condition for dissolution of the M23C6 carbides in 2.25Cr-1Mo-V-Ti material for thermal power plant tube was investigated using a dilatometer method. 2.25Cr-1Mo-V-Ti material was heat-treated at $900{\sim}1,100^{\circ}C$ for 0, 10, 30 min to find the proper dissolution condition of M23C6 carbides. The phase identification and volume fraction of the carbide were measured by using OM, SEM, EBSD and TEM analysis. Optimal heat treatment condition of M23C6 carbide dissolution was selected by predicting dissolution temperature of carbide using Bs points appeared at dilatometer curve. Experimental results showed that the conditions of carbide dissolution was 900, 1,000, $1,100^{\circ}C$ for 30 min. Eventually, the optimal heat treatment condition for dissolution was 30 min at $1,000^{\circ}C$ considering the minimum coarsening of Austenite grain size.