• Title/Summary/Keyword: 2-Phase Matrix Structure

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Effect of Deposition Parameter and Mixing Process of Raw Materials on the Phase and Structure of Ytterbium Silicate Environmental Barrier Coatings by Suspension Plasma Spray Method (서스펜션 플라즈마 스프레이 코팅법으로 제조된 Ytterbium Silicate 환경차폐코팅의 상형성 및 구조에 미치는 증착인자 및 원료혼합 공정의 영향)

  • Ryu, Ho-lim;Choi, Seon-A;Lee, Sung-Min;Han, Yoon-Soo;Choi, Kyun;Nahm, Sahn;Oh, Yoon-Suk
    • Journal of Powder Materials
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    • v.24 no.6
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    • pp.437-443
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    • 2017
  • SiC-based composite materials with light weight, high durability, and high-temperature stability have been actively studied for use in aerospace and defense applications. Moreover, environmental barrier coating (EBC) technologies using oxide-based ceramic materials have been studied to prevent chemical deterioration at a high temperature of $1300^{\circ}C$ or higher. In this study, an ytterbium silicate material, which has recently been actively studied as an environmental barrier coating because of its high-temperature chemical stability, is fabricated on a sintered SiC substrate. $Yb_2O_3$ and $SiO_2$ are used as the raw starting materials to form ytterbium disilicate ($Yb_2Si_2O_7$). Suspension plasma spraying is applied as the coating method. The effect of the mixing method on the particle size and distribution, which affect the coating formation behavior, is investigated using a scanning electron microscope (SEM), an energy dispersive spectrometer (EDS), and X-ray diffraction (XRD) analysis. It is found that the originally designed compounds are not effectively formed because of the refinement and vaporization of the raw material particles, i.e., $SiO_2$, and the formation of a porous coating structure. By changing the coating parameters such as the deposition distance, it is found that a denser coating structure can be formed at a closer deposition distance.

A Form Clustering Algorithm for Web-based Application Reengineering (웹 응용 재구성을 위한 폼 클러스터링 알고리즘)

  • 최상수;박학수;이강수
    • The Journal of Society for e-Business Studies
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    • v.8 no.2
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    • pp.77-98
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    • 2003
  • A web-based information system, that is a dominant type of information systems, suffers from the "web crisis" in development and maintenance of the system. To cope with the problem, a technology of software clustering to web-based application, which is one of web engineering, is strongly needed. In this paper, we propose a Form Clustering Algorithm along with an application example, which are used for internal-system reengineering to web-based information system. A Form Clustering Algorithm focuses on Page-model which is the feature of the web among the various web-based information system's structural model. Specially, we applying distance matrix to navigation model of graph form for easily analyzing, and web log analysis for identifying core function object that have a highly loading. Also, we create web software structure that can be used to maximize reusability and assign hardware effectively through 2-phase clustering step. Form Clustering Algorithm might be used at web-based information system development and maintenance for reusable web component development and hardware assignment, respectively.

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Structure and Electrical Properties of PbTe Thin Film According To The Substrate Temperature (기판온도에 따른 PbTe 박막의 구조 및 전기적 물성)

  • Lee, Hea-Yeon;Choi, Byung-Chun;Jeong, Jung-Hyun
    • Journal of Sensor Science and Technology
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    • v.8 no.2
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    • pp.184-188
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    • 1999
  • PbTe thin films of high quality were deposited on HF-treated Si(100) substrates at various substrate temperature by pulsed laser deposition technique. XRD patterns showed that PbTe layers were well-crystallized to a cubic phase with (h00) preferred orientation with the substrate temperature up to $300^{\circ}C$. PbTe films could not form at substrate temperature above $400^{\circ}C$ because of reevaporation of the Pb. According to AFM image, the surface of films was composed of small granular crystals and flat matrix. According to the increase of substrate temperature, the grain size at film surface becomes larger. By Hall-effect measurement, the carrier concentration and Hall mobility of n-type PbTe films grown by $T_{sub}=300^{\circ}C$ were $3.68{\times}10^{18}cm^{-3}$ and $148\;cm^2/Vs$, respectively.

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Development of the high elonagation and high strength steel sheets utilizing two step heat treatment (2단열처리를 이용한 고연신율 고장력 강판의 개발)

  • Kim, Y.H.;Kim, Y.H.;Kim, H.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.10 no.1
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    • pp.1-9
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    • 1997
  • The variation of the mechanical properties and the formation of retained austenite with heat treatment conditions in austempered Si bearing carbon steels has been investigated. In the case of a steel containing 0.35C-1.48Si-0.95Mn, it has been found that a feather shape bainite structure of lath are obtained under a isothermal treated condition at just below the Ms temperature, and the martensite, bainitic ferrite and retained austenite of second phase particles on the ferrite matrix for a isothermal treated steels after intercritical annealing are precipitated in a linked shape. The retained austenite with $2{\mu}m$ size induced as TRIP is found to increase with increasing the formation rate of retained austenite for the intercritical annealing and high Si containing steels. The tensile strength is increased as austempering temperature increases in all isothermal treatment temperature, whereas the elongation is shown to roughly decrease as the tensile strength increases. The values of tensile strength-elongation balance have showed a marked dependence upon the elongation rather than the tensile stregth, and their values are increased for high Si containing steels and intercritical annealing condition. The most optimum result has been shown to be the tensile stregth-elongation balance of $2882.4kgf/mm^2.%$ and the elongation of 33.3% for a "B" steel in the heat treating temperature range of $780{\sim}370^{\circ}C$.

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Vibrational characteristics of sandwich annular plates with damaged core and FG face sheets

  • Xi, Fei
    • Steel and Composite Structures
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    • v.44 no.1
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    • pp.65-79
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    • 2022
  • The main goal of this paper is to study the vibration of damaged core laminated annular plates with FG face sheets based on a three-dimensional theory of elasticity. The structures are made of a damaged isotropic core and two external face sheets. These skins are strengthened at the nanoscale level by randomly oriented Carbon nanotubes (CNTs) and are reinforced at the microscale stage by oriented straight fibers. These reinforcing phases are included in a polymer matrix and a three-phase approach based on the Eshelby-Mori-Tanaka scheme and on the Halpin-Tsai approach, which is developed to compute the overall mechanical properties of the composite material. In this study the effect of microcracks on the vibrational characteristic of the sandwich plate is considered. In particular, the structures are made by an isotropic core that undergoes a progressive uniform damage, which is modeled as a decay of the mechanical properties expressed in terms of engineering constants. These defects are uniformly distributed and affect the central layer of the plates independently from the direction, this phenomenon is known as "isotropic damage" and it is fully described by a scalar parameter. Three complicated equations of motion for the sectorial plates under consideration are semi-analytically solved by using 2-D differential quadrature method. Using the 2-D differential quadrature method in the r- and z-directions, allows one to deal with sandwich annular plate with arbitrary thickness distribution of material properties and also to implement the effects of different boundary conditions of the structure efficiently and in an exact manner. The fast rate of convergence and accuracy of the method are investigated through the different solved examples. The sandwich annular plate is assumed to have any arbitrary boundary conditions at the circular edges including simply supported, clamped and, free. Several parametric analyses are carried out to investigate the mechanical behavior of these multi-layered structures depending on the damage features, through-the-thickness distribution, and boundary conditions.

Using three-dimensional theory of elasticity for vibration analysis of laminated sectorial plates

  • Liyuan Zhao;Man Wang;Rui Yang;Meng Zhao;Zenghao Song;N. Bohlooli
    • Steel and Composite Structures
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    • v.48 no.1
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    • pp.1-17
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    • 2023
  • The main goal of this paper is to study vibration of damaged core laminated sectorial plates with Functionally graded (FG) face sheets based on three-dimensional theory of elasticity. The structures are made of a damaged isotropic core and two external face sheets. These skins are strengthened at the nanoscale level by randomly oriented Carbon nanotubes (CNTs) and are reinforced at the microscale stage by oriented straight fibers. These reinforcing phases are included in a polymer matrix and a three-phase approach based on the Eshelby-Mori-Tanaka scheme and on the Halpin-Tsai approach, which is developed to compute the overall mechanical properties of the composite material. Three complicated equations of motion for the sectorial plates under consideration are semi-analytically solved by using 2-D differential quadrature method. Using the 2-D differential quadrature method in the r- and z-directions, allows one to deal with sandwich annular sector plate with arbitrary thickness distribution of material properties and also to implement the effects of different boundary conditions of the structure efficiently and in an exact manner. The fast rate of convergence and accuracy of the method are investigated through the different solved examples. The sandwich annular sector plate is assumed to be simply supported in the radial edges while any arbitrary boundary conditions are applied to the other two circular edges including simply supported, clamped and free. Several parametric analyses are carried out to investigate the mechanical behavior of these multi-layered structures depending on the damage features, through-the-thickness distribution and boundary conditions.

Effect of 3-Amino-1,2,4-triazole on Microstructure and Properties of Maleated HDPE/Maleated EPDM Blend (3-Amino-1,2,4-triazole이 Maleated HDPE/Maleated EPDM 블렌드의 미세구조 및 물성에 미치는 영향)

  • Kim, Tae Hyun;Chang, Young-Wook;Lee, Yong Woo;Kim, Dong Hyun
    • Elastomers and Composites
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    • v.49 no.1
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    • pp.24-30
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    • 2014
  • 3-Amino-1,2,4-triazole (ATA) (2.5 and 5.0 phr) was incorporated into a immiscible maleated ethylene propylene diene rubber(mEPDM)/maleated high density polyethylene(mHDPE) (50 wt%/50 wt%) blend by melt mixing. Effects of the ATA on structure, mechanical and rheological properties of the blend was investigated. FT-IR and DMA results revealed that supramolecular hydrogen bonding interactions between the polymer chains occur by reaction of ATA with maleic anhydride grafted onto the component polymers in the blend, which induces the physical crosslinks in the blend. FE-SEM analysis showed that mEPDM forms a dispersed phase in continuous mHDPE matrix, and the blend with the ATA has finer phase morphology as compared to the blend without the ATA. By the addition of ATA in the blend, there were significant increases in tensile strength, modulus and elongation-at-break as well as elastic recoverability. Melt rheology studies revealed that ATA induced substantial increase in storage modulus and complex viscosity of the blend at the melt state.

Mechanical Properties and Morphology of Polyamide 6/Maleated Polypropylene Blends (폴리아미드6/반응성 폴리프로필렌(PA6/PP-g-MA) 블렌드의 기계적 특성과 모폴로지)

  • Koh, Jae Song;Jang, Yoon Ho
    • Applied Chemistry for Engineering
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    • v.10 no.8
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    • pp.1136-1140
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    • 1999
  • Melt blends of polymide 6(PA6) and polypropylene grafted maleic anhydride(PP-g-MA) were prepared to study the influence of chemical reaction between the two polymer components. The tensile, flexural, izod impact, dynamic mechanical properties and phase structure were investigated for this blend system. Tensile strength and modulus of the blends showed synergetic effect upon blending of two polymer components. Flexural properties maintained the value of numerical mean calculated from the weight ratio of two components. Also, notched izod impact strengths showed maximum in th PA6/PP-g-MA 50/50 wt % blend. From the change of tan ${\delta}$ observed, we confirmed the increase of miscibility in this blend system by chemical reaction between PA6 and PP-g-MA. Blends of good impact resistance could be obtained when the PP-g-MA particles of $2{\mu}m$ was dispersed in the PA6 matrix.

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A Design of the New Three-Line Balun (새로운 3-라인 발룬 설계)

  • 이병화;박동석;박상수
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.14 no.7
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    • pp.750-755
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    • 2003
  • This paper proposes a new three-line balun. The equivalent circuit of the proposed three-line balun is presented, and impedance matrix[Z]of the equivalent circuit is derived from the relationship between the current and voltage at each port. The design equation for a given set of balun impedance at input and output ports is presented using[S]parameters, which is transferred fom impedance matrix,[Z]. To demonstrate the feasibility and validity of design equation, multi-layer ceramic(MLC) chip balun operated in the 2.4 GHz ISM band frequency is designed and fabricated by the use of the low temperature co-fired ceramic(LTCC) technology. By employing both the proposed new three-line balun equivalent circuit and multi-layer configuration provided by LTCC technology, the 2012 size MLC balun is realized. Measured results of the multi-layer LTCC three-line balun match well with the full-wave electromagnetic simulation results, and measured in band-phase and amplitude balances over a wide bandwidth are excellent. This proposed balun is very easily applicable to multi-layer structure using LTCC as shown in the paper, and also can be realized with microstrip lines on PCB. This distinctive performance is very favorable for wireless communication systems such as wireless LAN(Local Area Network) and Bluetooth applications.

Ultra-high Temperature EM Wave Absorption Behavior for Ceramic/Sendust-aluminosilicate Composite in X-band (X-Band 영역에서의 세라믹/샌더스트-알루미노실리케이트 복합재의 초고온 전자파 흡수 거동)

  • Choi, Kwang-Sik;Sim, Dongyoung;Choi, Wonwoo;Shin, Joon-Hyung;Nam, Young-Woo
    • Composites Research
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    • v.35 no.3
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    • pp.201-215
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    • 2022
  • This paper presents the development of thin and lightweight ultra-high temperature radar-absorbing ceramic composites composed of an aluminosilicate ceramic matrix-based geopolymer reinforced ceramic fiber and sendust magnetic nanoparticles in X-band frequency range (8.2~12.4 GHz). The dielectric properties with regard to complex permittivity of ceramic/sendust-aluminosilicate composites were proportional to the size of sendust magnetic nanoparticle with high magnetic characteristic properties as flake shape and its concentrations in the target frequency range. The characteristic microstructures, element composition, phase identification, and thermal stability were examined by SEM, EDS, VSM and TGA, respectively. The fabricated total thicknesses of the proposed single slab ultra-high temperature radar absorber correspond to 1.585 mm, respectively, exhibiting their excellent EM absorption performance. The behavior of ultra-high temperature EM wave absorption properties was verified to the developed free-space measurement system linked with high temperature furnace for X-band from 25℃ to 1,000℃.