• Title/Summary/Keyword: 13세기 2

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The Crystal Structure of N-(Diphenylmethylene) aminomethylphosphonate (N-(Diphenylmethylene)aminomethylphosphonate의 결정 구조)

  • 김문집;박호종;김대영
    • Korean Journal of Crystallography
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    • v.13 no.2
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    • pp.86-90
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    • 2002
  • The structure of N-(Diphenylmethylene)aminomethylphosphonate has been determined by X-ray diffraction methods. The crystal system is triclinic, space group P(equation omitted), unit cell constants, a=8.967(2) (equation omitted), b=9.309(2) (equation omitted), c= 10.981(2) (equation omitted), α=101.42(2)°, β=92.22(2)°, γ=92.23(2)°, V=896.8(3) (equation omitted), T=296 K, Z=2, D/sub c/=1.227 Mgm/sup -3/. The intensity data were collected on an Enraf-Nonius CAD-4 Diffractometer with graphite monochromated MoKα radiation (λ=0.7107(equation omitted)). The molecular structure was solved by direct methods and refined by full-matrix least-squares to a final R=7.3% for 979 unique observed F/sub o/>4σ(F/sub o/) refections and 209 parameters.

A study on plans for improving the classification system of job field in the national technical qualification (국가기술자격 직무분야 분류체계 개선방안 연구)

  • Cho Jeong-Yoon;Park Jong-Sung
    • Journal of Engineering Education Research
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    • v.5 no.2
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    • pp.54-62
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    • 2002
  • The study reviewed the properness of a present job field with 26 items so that the classification system of the national technical qualification can meet the needs of the industrial structure and the technical changes of the 21st century. In addition, it aimed not only to improve the efficiency and effectiveness of the management and operation of the national technical qualification system but to design a new classification system of the job field to stimulate qualification holders' employment. For the purpose of this study, materials and data relevant to the national technical qualification system were comprehensively collected and analyzed. Besides, a new job field with 13 job items was proposed in this study on a basis of the collective advice of experts on the properness of the job field in the national technical qualification system.

A Study on Implementation of Return Channel for DVB-H with Efficient Interface Selection Algorithm in Heterogeneous Networks (이기종망 환경에서의 효율적인 인터페이스 선택을 통한 DVB-H 리턴채널 구현 방안)

  • Lim Jae-Won;Seo Sung-Hoon;Song Joo-Seok
    • The KIPS Transactions:PartC
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    • v.13C no.4 s.107
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    • pp.533-540
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    • 2006
  • WDMB technology has merits of high bandwidth and high mobility. But WDMB also has uni-directional communication problem. This paper provides solution to supplements uni-directional communication problem of WDMB with embodying return channel using WWAN to offer high quality multimedia service to user. Also this paper proposes intelligent network interface selection algorithm using various network information and return channel type. As a result of simulation, our proposed scheme is better as compared with other handoff scheme in energy efficiency of $7{\sim}8%$ and about two time of handoff number of time decrease.

Modification of Silica Nanoparticles with Bis[3-(triethoxysilylpropyl)]tetrasulfide and Their Application for SBR Nanocomposite (Bis[3-(triethoxysilylpropyl)]tetrasulfide에 의한 실리카 입자의 표면개질 반응과 SBR 나노 복합체 응용)

  • Ryu, Hyun Soo;Lee, Young Seok;Lee, Jong Cheol;Ha, KiRyong
    • Polymer(Korea)
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    • v.37 no.3
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    • pp.308-315
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    • 2013
  • In this study, we performed surface modification of silica nanoparticles with bis[3-(triethoxysilylpropyl)]tetrasulfide (TESPT) silane coupling agent to study the effects of treatment temperature, treatment time, and amount of TESPT used on the silanization degree with Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), elemental analysis (EA) and solid state $^{13}C$ and $^{29}Si$ cross-polarization magic angle spinning (CP/MAS) nuclear magnetic resonance spectroscopy (NMR). We found peak area of isolated silanol groups at $3747cm^{-1}$ decreased, but peak area of $-CH_2$ asymmetric stretching of TESPT at $2938cm^{-1}$ increased with the amount of TESPT from FTIR measurements. We also used universal testing machine (UTM) to study mechanical properties of styrene butadiene rubber (SBR) nanocomposites with 20 phr (parts per hundred of rubber) of pristine and TESPT modified silicas, respectively. The tensile strength and 100% modulus of modified silica/SBR nanocomposite were enhanced from 5.65 to 9.38MPa, from 1.62 to 2.73 MPa, respectively, compared to those of pristine silica/SBR nanocomposite.

A Policy Study on the Public and School Library Cooperation (공공도서관과 학교도서관의 협력 방안에 관한 연구)

  • 정동열;김성진
    • Journal of the Korean BIBLIA Society for library and Information Science
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    • v.13 no.2
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    • pp.5-28
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    • 2002
  • This study suggests a cooperation policy between public and school library. For the purpose of the objective, this research overviews cooperation theories, current situations of public and school libraries in Korea, and analyze cooperation methods and policies of them both Korea and foreign countries.

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A study of girl's costume in nineteenth century (19세기(世紀) 소여복(小女服)에 대한 연구(硏究))

  • Lee, Yun-Young;Kim, Jin-Gu
    • Journal of the Korean Society of Costume
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    • v.13
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    • pp.73-79
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    • 1989
  • During nineteenth century, there broke out a great revolution in the history of girl's costume and with new condition toward girls. 1. Girl's costume followed their mother's attitude of the era and it was influenced by mother's costume. 2. Girl's costume was closely related with politics, economy, society culture and thought of the era. 3. Rousseau's Englightment made a revolution on girl's costume and it was direct revolution which affected on the French Revolution and the independence America. 4. Development of textile industry by industrial revolution brought on a change in raw material, quality, and quantity of textile, more gave a variety to raw material and ornament of girl's costume. 5. The invention of Sewing machine made it possible ready made production of girl's costume.

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회원사탐방 - 성마기업(주)

  • 대한기계설비건설협회
    • 월간 기계설비
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    • s.307
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    • pp.71-79
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    • 2016
  • 21세기에 기업의 운명을 결정짓는 것은 기업문화이다. 바람직한 기업문화는 훌륭한 일터 만들기 위한 전제조건이다. 그런 까닭에 오늘날 대부분의 기업들이 각사 특성에 적합한 바람직한 기업문화 정착에 많은 관심을 기울이고 있다. 성마기업(주)가 그렇다. 성마기업은 투명경영을 통해 임직원 모두 주인의식을 갖고 소통하는 기업문화를 갖고 있다. 또 매년 전직원이 모여서 교육을 실시한다. 성마기업은 지난 1월 13일 오후 1시부터 15일 오후 6시까지 인천광역시 소재 건설기술교육원에서 60여명의 전 직원이 참석한 가운데 2박 3일간 직무능력 향상교육을 실시했다. 이 교육에 예외란 없다. 본사를 비롯, 전국에 있는 현장의 모든 직원들이 참석하여 교육을 받는다. 본지는 성마기업(주)가 실시한 2016년도 직무 능력 향상 교육을 직접 다녀왔다.

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The Effect of Micro Constituent Element on the Development of Unique Color of Koryo Celadon (고려 청자 유약 발색에 미량 성분이 미치는 영향)

  • 김형태;이세용;함청순;최의석
    • Journal of the Korean Ceramic Society
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    • v.38 no.6
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    • pp.522-530
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    • 2001
  • 발굴된 과거 고려청자의 화학성분조성과 물리적 특성에 대한 평가를 하고 미량성분의 청자의 발색에 미치는 영향을 고찰한 결과, 고려 청자 태토는 Fe$_2$O$_3$가 2%, TiO$_2$가 0.8% 함유되어 있었으며, 청자유는 석회.장석유로서 Fe$_2$O$_3$가 1.0~1.2%, TiO$_2$가 0.16% 포함되어 있었다. 비색청자의 경우 미량성분인 MnO$_2$가 P$_2$O$_{5}$의 함량이 0.37%와 0.76%, CuO는 300~500ppm 정도 함유하고 있었다. 반사율 측정 결과 일반적인 청자가 540~570nm의 장파장대에서의 반사율이 급격히 떨어지는데 반하여, 13세기 비색 청자의 것은 적색 파장대에서 10%이상 높았다. CoO는 미량 첨가로도 유약의 청색 파장대 반사율이 높고, 적색 파장대의 반사율이 급격히 떨어지며 청자 발색에 부정적인 영향을 미쳤다. CuO는 0.05%를 첨가했을 경우 적색 파장대에서 반사율 곡선이 높게 나타나고 있어 비색 청자발색에 효과적이었다. 또한 명도를 나타내는 L*값도 CuO가 첨가된 유약이 가장 높았고, 비색청자의 색상은 녹청자에 비해 맑고 깊은 색감을 보였다.

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Species Identification and Radiocarbon Dating for the Wooden Board from Daebudo Shipwreck No.2 Using Wiggle Matching (대부도2호선 목부재의 수종과 위글매치를 이용한 방사성탄소연대 분석)

  • Nam, Tae Gwang;Yoon, Yong Hee;Kim, Eung Ho
    • Journal of Conservation Science
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    • v.34 no.5
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    • pp.359-368
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    • 2018
  • The purpose of this study was to analyze the wood species of the stern plank and persimmon seed from Daebudo shipwreck No.2 excavated from Daebudo, Danwon-gu, Ansan-si, and Gyeonggi-do by wiggle-matching of radiocarbon measurements. Results of the analysis showed that all the wooden boards of the hull were made from Pinus Hard Pine Group. The other parts of hull and wooden pegs were made from Pinus Hard Pine Group, Castanea spp., Quercus spp. sect. Lepidobalanus, Alnus spp., and Zelkova serrata Makino. Excavated wide-tooth wooden comb and fine-tooth bamboo comb were made from Acer spp. and Bambusoideae. Excavated rope was made from Pueraria thunbergiana Benth. The stern plank, wooden support, and persimmon stone showed ${\pm}2{\sigma}$ radiocarbon date(95.4% confidence interval) of AD 1151-1224. This indicated that the Daebudo shipwreck No.2 occurred during the early or middle 12-13th century. Our radiocarbon dating results confirmed the date speculated by archeologists based on the ceramic style.

The Nature Cognition and Lyricism Reflected in the Pavilion Tablets - Focusing on the Pavilions in the Damyang Poetry Culture Area Built during in 16th Century - (누정편액(樓亭扁額)에 반영된 자연인식과 서정 - 16세기 담양 시가문화권의 누정을 중심으로 -)

  • Lee, Hyun-Woo;Kim, Jai-Sik
    • Journal of the Korean Institute of Traditional Landscape Architecture
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    • v.28 no.3
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    • pp.1-13
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    • 2010
  • This research is the semantic study on the nature cognition and lyricism of pavilion builders as reflected in the pavilion tablets in the Damyang poetry culture area built during 16th century. The names of pavilions, pavilion writings and "poetry with given theme" were studied by actual site visits. The view on the nature and aesthetic awareness of the pavilion builders at the time were explored together with surrounding landscapes. Following conclusions were drawn. 1. Pavilion names borrowed phrases from the famous historical events left by the sages. Or, they took the compliment on the beautiful nature surrounding orthe academic achievement of pavilion owners as the theme, then elaborated them with thinking based on Sung Confucianism. 2. The writings of pavilion literature were the idealistic view on the nature. They think the nature and human as "object and ego are one, object and ego communicate each other, object and ego become one". 3. The nature in the 16th century was the "principle of birth-death-grow-wither" for the intellectuals. They thought that the nature is the ultimate place to return for the realization of life with self-respect. 4. The introduction of fairy land among literary activities in the pavilion was the symbolic means healing the frustrated ego. It was confirmed that they temporarily entrusted their depressed feelings by borrowing the fairy land, far from the reality. The pavilion was the space to escape from the reality and soothe the anger and discord in the reality. 5. The pavilion literature in the Damyang poetry culture area during 16th century sang their pleasure of enjoying the beautiful scenery in the rural area using their social status. The literary works also contained their agony due to the frustration of difficulty in the realization of ideal. When the intellectuals, who already mastered literature, history and philosophy, came down to rural area, built pavilions at the location with beautiful scenery, and spent time while composing poetry, it was an escape from the burden that they should take the social responsibility as the model intellectuals of the society. The pavilions in Damyang poetry-culture area during 16th century were the idealized conceptual world and the space of awareness reflecting the philosophy and thinking of the time.