• 대한기계학회논문집
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• 제18권9호
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• pp.2374-2385
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• 1994

SiCw/Al composite material is especially attractive because of their superior specific strength, specific stiffness, corrosion fatigue resistance, creep resistance, and wear resistance compared with the corresponding wrought Al alloy. In this study, Fatigue crack growth behavior and fatigue crack path morphology(FCPM) of SiC whisker reinforced Al 6061 alloy with 25% SiC volume fraction and Al 6061 allay were performed. Result of the fatigue crack growth test sgiwed that fatigue crack growth rate of SiCw/Al 6061 composite was slower than that of Al 6061 matrix therefore it was confirmed that Sic whisker have a excellent fatigue resistance. And Al 6061 matrix had only FCPM perpendicular to loading direction. On the other hand SiCw/Al 6061 composite had three types in fatigue crack path morphology. First type is that both sides FCPM of artificial notch are perpendicular to loading direction. Second type is that a FCPM in artifical notch has slant angle to loading direction and the other side FCPM is perpendicular to loading direction. Third type is that both sides FCPM of notch have slant angle to loading direction. It was considered that this kinds of phenomena were due to non-uniform distribution of SiC whisker and confirmed by SEM observation for fracture mechanism study.

• 한국결정성장학회지
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• 제26권4호
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• pp.150-154
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• 2016

$K_2Ti_6O_{13}$ 휘스커를 합성하는 방법은 고상법, 수열합성법, 소성법, 융제법, 서냉법, 용융법, KDC법, 졸-겔법 등이 있다. 융제법을 이용하여 $K_2Ti_6O_{13}$을 합성하는 연구를 진행하였다. 칼륨 전구체의 종류와 반응온도와 시간을 조절하여 합성 된 $K_2Ti_6O_{13}$의 입자크기와 분포를 제어하였고, 합성된 $K_2Ti_6O_{13}$의 평균입자 크기는 $500nm{\sim}2{\mu}m$였다. KOH와 $TiO_2$의 비율, pH(KOH 첨가량), 반응온도와 반응시간 등의 공정변수에 대해 연구를 진행하였다. 합성된 $K_2Ti_6O_{13}$은 X-선 회절분석기와 전계방사 주사전자현미경을 이용하여 특성평가를 실시하였다.

• 한국세라믹학회지
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• 제41권7호
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• pp.541-547
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• 2004

일반적으로 혼합분말의 소결에서 작은 입자에 큰 입자의 첨가는 소결성의 저하를 가져온다. 본 연구에서는 이러한 원리를 이용하여 작은 SiC 입자에 큰 SiC 휘스커 또는 큰 SiC 입자를 첨가하여 소결성을 저하시키고, YAG(Y$_3$A1$_{5}$O$_{12}$)상을 소결 첨가제로 사용함으로서 다공질 SiC 세라믹스를 제조하였다. 제조된 다공질 SiC 세라믹스의 기공율은 큰 입자의 함량과 소결 압력을 제어함으로서 0.3-39% 범위에서 제어할 수 있었다. 기공율은 큰 입자의 함량이 증가함에 따라 증가하였고, SiC 휘스커를 첨가하는 것이 큰 SiC 입자를 첨가하는 것 보다 기공율을 높이는데 효과적이었다. 제조된 다공질 세라믹스에서 기체의 통기성은 기공율이 증가함에 따라 증가하였고, 굽힘강도는 기공율이 증가함에 따라 감소하였다. 기공율이 18% 이상인 다공질 SiC 세라믹스의 경우에 주목할 만한 변형율이 관찰되었다.

• 한국자동차공학회논문집
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• 제4권6호
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• pp.18-26
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• 1996

A two dimensional thermo elasto-plastic finite element stress analysis was performed to study residual stress distributions in AI composites reinforced by SiC whisker and $ZrO_2$ ceramic joints. The influences on the residual stress distributions due to the difference of the reinforcement volume fraction and interlayer material property were investigated. Specifically, stress distributions between AI interlayer material property were investigated. Specifically, stress distributions between AI interlayer and $ZrO_2$ ceramic and between the AI interlayer and AI composite were computationally analzed.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1993년도 춘계학술대회 및 공장견학
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• pp.59-62
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• 1993

고품위의 동력전달 장치와 같은 고정밀 기능 부품들은 보다 높은 비강도, 고경도, 내마모성 및 내식성을 가져야 하며, 특히 소재의 마찰, 마모 특성은 기아제품 등의 수명, 정밀도 및 에너지 손실을 좌우하는 것으로서 물성의 열화를 극복할 수 있는 소재의 개발이 요구되고 있다. 지난 수년동안 금속기지에 $Al_2O_3$나 SiC등의 보강재를 첨가하여 복합재의 응착 및 연삭마모에 대한 저항성을 향상시키는 시도를 하고 있다. 주로 제조비용이 낮고 거의 등방적인 성질을 가지며 가공성이 좋은 입자 보강 복합재료에 대한 연구가 지배적이었지만, 입자 보강 복합재료의 경우 강도 및 탄성계수의 향상 정도가 적다는 단점을 지니고 있다. 본 연구에서는 분말야금법을 이용하여 금속기지에 세라믹상으로 SiC 입자 및 휘스커가 첨가된 복합재를 제조하여 제조공정변수에 따라 마모거동을 pin-on-disk 형태의 마모시험기에서 실험하였으며, 주사전자현미경으로 마모표면관찰 등으로 복합재의 마모기구를 연구하였다.

• 대한기계학회논문집
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• 제19권9호
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• pp.2122-2132
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• 1995

There are some cases which require to grasp the abrasion resistance property in the fields of the high-technology to be required the high specific strength and modulus. In this study, wear test with the various test temperature and velocity were performed in the SiCw/A16061 composite and A16061 matrix using the wear test machine of the ring-on-disc type. As the results, the friction and wear properties by various test temperature and velocity were examined. The worn surface has observed by scanning electron microscope in order to examine the wear mechanism.

• 한국세라믹학회지
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• 제31권12호
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• pp.1513-1520
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• 1994

Mechanical properties of hot-pressed SiC whisker/Al2O3 composites were strongly dependent on the granular characteristics of mixed powder, which were controlled by co-dispersion condition, the existence of steric barrier on whisker surface, and granulating method, etc. Heat-treatment of SiC whiskers at $700^{\circ}C$ for 1 hr in air was very effective both for achieving dispersion stability of whiskers with PVA adsorption and for obtaining excellent mechanical properties of resulting composites. It is believed from the fractography of composites prepared with various whisker dispersion conditions that the most common fracture origin of Al2O3 agglomerate could be attributed to whisker clusters arising due to flocculation. Further improvement of mechanical properties of composites were achieved by hot pressing green tapes prepared by Doctor-blade process, which promoted two-dimensional random alignment of whiskers.

• 한국세라믹학회지
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• 제33권12호
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• pp.1380-1386
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• 1996

The effects of urea addition and reaction conditions were examined in the prepareation of zirconia coated SiC whiskers through surface precipitation taking place during high-temperature aging of Zr(SO4)2 solutions containing the whiskers. More dense zirconia-hydrate was precipitated on the surfaces of the whiskers in the presence of urea. The ratio of the concentration of Zr(SO4)2 to the amount of added whiskers was the most important factor to confine the precipitation of zirconia-hydrate only at the surfaces of the whiskers The from of the coating layers was unchanged after heat-treatment leading to the dehydration and crystallization of the layers.

• 한국세라믹학회지
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• 제32권10호
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• pp.1139-1146
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• 1995

$\beta$-SiC whiskers could be formed from a system of mullite-carbon-hydrogen by VLS mechanism at elevated temperatures. It was considered that methane gases were generated from the reaction of hydrogen gases with carbon black, and were reacted with mullite to produce two kinds of gases; silicon suboxide (SiO) and carbon monoxide (CO) of precursors of SiC. With increasing the synthesizing temperature up to 146$0^{\circ}C$, the formation of $\beta$-SiC whisker increased from 0.58 mg/$\textrm{cm}^2$ to 3.98 mg/$\textrm{cm}^2$ on the basis of unit area of carbon block, and the diameters of whiskers had their uniformity due to the reduction in stacking faults.

• 한국세라믹학회지
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• 제43권6호
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• pp.376-382
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• 2006

In the $Al(OH)_3-SiO_2-AlF_3$ system, leaf-shaped fluorotopaz was first formed at $800^{\circ}C$ and mullite whisker was formed at $1,100^{\circ}C$. The mass transportation of Al and Si as gas phase, the fast reaction and growth, and the absence of liquid phase existence in mullite whisker showed that the formation and growth of mullite was from the solid-vapor reaction.