• Title/Summary/Keyword: 화학성분 분석

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A Study on Chemical Analysis of Reclaimed Asphalts and Rejuvenators for Property Restoration (성상복원을 위한 폐아스팔트의 화학적 분석 및 재생첨가제 연구)

  • Jung, Du-Hwoe
    • International Journal of Highway Engineering
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    • v.3 no.1 s.7
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    • pp.177-184
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    • 2001
  • A recycling agent has been manufactured on the basis of the chemical composition of reclaimed asphalt binders and virgin asphalt binders. The chemical compositions of reclaimed asphalt binders extracted from reclaimed asphalt pavements have been analyzed according to the ASTM method and the results were compared to those of virgin asphalt binder AP-3. Reclaimed asphalt binders have shown that asphaltenes was increased whereas saturates, naphthene aromatics, and polar aromatics fractions were decreased. A recycling agent made of aromatic compounds, in which its chemical composition is similar to the aromatics fraction in asphalt binders, has been produced to reduce the amount of asphaltenes in reclaimed asphalt hinders. The evaluation of the recycling agent produced was performed by testing ductility, rolling and ball softening point, penetration at $25^{\circ}C$ and viscosity at $60^{\circ}C$. It was found that, by adding the recycling agent 20% by weight to the reclaimed asphalt binders, the physical properties of reclaimed asphalt binders was recovered to the level of virgin asphalt binder AP-3.

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Chemical Properties of the Horticultural Soils in the Plastic Film Houses in Korea (우리나라 시설원예(施設園藝) 재배지(栽培地) 토양(土壤) 화학적특성(化學的特性))

  • Jung, Beung-Gan;Choi, Jeong-Weon;Yun, Eul-Soo;Yoon, Jung-Hui;Kim, Yoo-Hak;Jung, Goo-Bok
    • Korean Journal of Soil Science and Fertilizer
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    • v.31 no.1
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    • pp.9-15
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    • 1998
  • A survey was conducted to investigate the chemical properties of soils such as pH, electrical conductivity, total organic matter content, soluble nitrate, available phosphate and major exchangeable canons, in plastic film houses at 513 sites. All the parameters surveyed in the plastic film house were much higher than those of open field soils. Particularly conspicuous was the accumulation of available P, exchangeable K and the occurrence of nitrate at relatively high concentration in both top soil(0-20 cm) and sub-soil(20-40 cm). In 70-80% of cases, the contents of available P and exchangeable K in top soils, were found to be higher than optimum levels. There was positive linear correlation between the content of exchangeable rations, and nitrate and EC of soils. The correlation coefficient was greater in the order of nitrate-EC > Mg-nitrate > K-nitrate > Ca-nitrate. The successive cultivation of horticultural crops in the plastic houses tended result in the accumulation of available P, exchangeable K and total organic matter in the soil.

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A TECHNIQUE TO OPTICALLY DETERMINE THE STOICHIOMETRY OF $C_2$ GROWN LITHIUM NIOBATE CRYSTALS (Czochralski법으로 성장시킨 $LiNbO_3$단결정의 화학양론(Stoichiometry)을 결정하기 위한 광학적 방법)

  • Kim, You-Song
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.1 no.2
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    • pp.1-14
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    • 1991
  • In growing single crystals, which exhibit incongruent melting behavor, it is extremely difficult to maintain the stoichiometry of its chemical compositions for given crystals. For instance, $LiNbO_3$ is a typical one which exhibits such incongruent melt, especially with a large solid solution region that makes it difficult to maintain the chemical compositions. Such a variation can then cause a serious problem for the practical applications in designing a precision electro /optic device. Of the known methods of determining its composition and quality, an optical technique of measuring refractive index of the crystals has been implemented. This technique is also capable of determining optical uniformity of the grown crystals and the chemical compositions. The technique used for such characterizations is herein described and some of results are discussed.

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Volatile Component Analysis of Commercial Japanese Distilled Liquors (Shochu) by Headspace Solid-Phase Microextraction (헤드스페이스 고체상미량추출(Solid-Phase Microextraction)을 이용한 시판 일본소주의 휘발성 향기성분 분석)

  • Shin, Kwang-Jin;Lee, Seung-Joo
    • Korean Journal of Food Science and Technology
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    • v.47 no.5
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    • pp.567-573
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    • 2015
  • In this study, volatile compounds in nine commercial Japanese distilled liquors (Shochu) were isolated by headspace solid-phase microexrraction (SPME) and analyzed by gas chromatography (GC) and GC-mass spectrometry (MS). A total of 76 volatile components, including 48 esters, 13 alcohols, and 15 miscellaneous components, were identified. Esters and alcohols constituted the largest groups of quantified volatiles. Differences in volatile components among the distilled liquors and possible sample grouping were examined by applying principal component analyses to the GC-MS data sets. The first and second principal components explained 77.92% of the total variation across the samples. The samples using barley koji showed higher overall concentrations of total volatile components. Additionally, the principal component analysis did not reveal any sample grouping based on the raw material used.

Measurement of Oxygen Isotope Ratio in Water Vapor by using Tunable Diode Laser Absorption Spectroscopy(TDLAS) - II (다이오드레이저 흡수분광법을 이용한 수증기의 산소 동위원소 성분비 측정 - II)

  • Jung, Do-Young;Park, Sang-Eon;Kim, Jae-Woo;Ko, Kwang-Hoon;Im, Kwon;Jung, Eui-Chang;Kim, Chul-Joong
    • Proceedings of the Optical Society of Korea Conference
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    • 2003.02a
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    • pp.202-203
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    • 2003
  • 여러 가지 원소의 동위원소 성분 분석은 생물학, 화학, 환경학, 연대학, 기후학 연구에 있어서 중요한 정보를 제공하는 유용한 수단이다. 동위원소 성분비를 측정하는 방법으로는 가스 동위원소 질량분석기를 이용한 방법이 사용되어 왔지만, 최근 다이오드 레이저의 발달과 함께 다이오드레이저 흡수분광법(TDLAS)이 개발되어 사용되고 있다. TDLAS 방법의 경우 질량분석기를 이용하는 방법에서는 측정이 불가능한 동일질량 분자의 동위원소 성분비를 측정할 수 있다. (중략)

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Gemological and Minearlogical Properties of the Red Garnet Stones (적색 석류석 보석의 보석.광물학적 특징)

  • 김금조;김진섭;김원사;최진범
    • Journal of the Mineralogical Society of Korea
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    • v.16 no.1
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    • pp.19-31
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    • 2003
  • Chemical composition, crystal structure, refractive index, specific gravity, color, and luster were studied fur pyrope-almandine series garnets. The main coloring agents determining the reddish or brownish garnets were also investigated. It was also examined if there is any relationship between mineralogical properties with respect to the various chemical compositions in the solid solution, in the hope to figure out the existing classification values of R.I. and S.G. using gem- testing facilities to distinguish pyrope from almadine. It was found that 17 out of the 24 specimens belong to pyrope and the rest almandine. R.I. of pyrope goes up to 1.77 and that of almandine is higher than the value.5.5. of pyrope reaches to 3.88 and that of almandine is greater than the value of pyrope. X-ray diffraction data revealed that pyrope-almandine garnets are isometric with space group Ia3d, and also show that the variation of cell parameters are not significant enough to parallel with the chemical compositions of the series. R.I. and S.G. increase with FeO content. Fe and Mn are most responsible to the red-purple and orange coloration of the specimens, respectively. Both zircon and rutile crystals are most common inclusions in the reddish stones.

Influence of Microhardness and Mineral Content on Fluoride Materials Containing Low Concentration with Sodium Fluoride (저농도의 불화나트륨을 함유한 불소제제가 치질의 강도와 화학적 성분에 미치는 영향)

  • Kim, Hye-Young;Nam, Seoul-Hee;Jeong, Mi-Ae
    • The Journal of the Korea Contents Association
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    • v.13 no.4
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    • pp.312-319
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    • 2013
  • The purpose of this study was to evaluate the efficacy of gargle and toothpaste containing low concentration with sodium fluoride on the remineralization through the surface microhardness and mineral content in enamel. After 4 weeks-application, the enamel surface was measured using microhardness tester and the calcium (Ca) and phosphorous (P) concentration of mineral content by electron probe microanalyzer (EPMA) analysis. By combining fluoridated gargle with toothpaste, a remineralized enamel resulted in significantly significant differences among the four groups (p<0.05). The Ca change treated with 0.23% fluoridated toothpaste and 0.02% fluoridated gargle with 0.23% toothpaste demonstrated the highest among the other groups. In conclusion. the fluoridated gargle with toothpaste by low concentration showed a significantly greatest synergistic effect on remineralization of the enamel than the other groups.

Analysis of Phytochemicals in Popular Medicinal Herbs by HPLC and GC-MS (HPLC와 GC/MS를 활용한 약용식물 유래 phytochemicals 분석)

  • Cho, Hyun-Jung;Yoo, Dong-Chan;Cho, Hyun-Nam;Fan, Lu-An;Kim, Hee-Joon;Khang, Kong-Won;Jeong, Ho-Soon;Yang, Seun-Ah;Lee, In-Seon;Jhee, Kwang-Hwan
    • Korean Journal of Food Science and Technology
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    • v.40 no.3
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    • pp.277-282
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    • 2008
  • Oriental herbs are reported as having potent functions for preventing many types of diseases. They also appear to have positive effects and potential capabilities for skin care. Among the many oriental herbs that are available, we chose to analyze four medicinal herbs, Korean red ginseng, Artemisia capillaries Thunb, Schizonepeta tenuifolia Briq, and Foeniculum vulgare Mill, because all are popular and considered as favorite medicinal plants in Korea. Extracts of the herbs were obtained by various methods such as using distilled water, ethyl ether, methanol, ethanol, benzene, 1-butanol, and chloroform. Nine phytochemicals were detected in the extracts: maltol, adenosine, b-pinene, menthone, pulegone, limonene, anethole, estragole, and fenchone, which reportedly have multi-functionalities. All phytochemicals were analyzed quantitatively by various chromatographic techniques such as HPLC and gas chromatography-mass (GC-MS) spectrometry. This article also presents the optimum conditions for extracting these 9 targeted phytochemical compounds that were derived from 4 popular oriental herbs, which could be useful for the efficient preparation of each phytochemical.