• Title/Summary/Keyword: 화학성분시험

Search Result 419, Processing Time 0.027 seconds

Study on individual characterization of sweat components (개체별 땀의 성분분포에 관한 연구)

  • Choi, Mi Jung;Ha, Jaeho;Yoo, Seok;Park, Sung Woo
    • Analytical Science and Technology
    • /
    • v.20 no.5
    • /
    • pp.434-441
    • /
    • 2007
  • The aim of this paper is to investigate composition of fatty acids in sweat on purpose of latent fingerprint detectant developing and crime evidence searching. Fingerprint from 5 male donors (aged 29-50 years) were collected. We identified fatty acid components on sweat using methylester mixture (37species) as standard fatty acid and analyzed them by GC-FID. As donor was aged, the level of total fat was found to decrease markedly (aged 20-30 years: 56.4-72.0 %, aged 50 years : 32.4-45.4 %). We identifided 28 species fatty acid, primarilly C16:0(palmitic acid), C16:1 (palmitoleic acid), C18:1n9c(oleic acid), C18:0 (stearic acid), C14:0 (tetradecanoic acid) and all sweats were found to contain C12:0 (lauric acid), C15:0 (pentadecanoic acid), C18:2n6c (linoleic acid), C18:2n6t (linolelaidic acid), C20:0 (arachidic acid), C24:0/C20:5n3 (lignoceric acid/eicosapentaenoic acid), but with differing frequencies and at varying levels. C14:1 (myristoleic acid), C15:1 (pentadecenoic acid), C21:0 (heneicosanoic acid), C22:1n9 (erucic acid) were often observed in sample. Ratio of saturated and unsaturated fatty acid was from 0.94:1 to 2.6:1. And decrease of total fatty acids components caused by loss of saturated fatty acid and monounsaturated fatty acid. In case of sweat amino acids, we detected serine ($0-31.9{\mu}L/mL$), threonine ($0-26.2{\mu}L/mL$), glycine ($0-18.9{\mu}L/mL$) and 20-30 years old, highly protein intake ratio individuals increased (10 times) than 50 years old. We observed greatly individual characterization of amino acid compounds in sweat.

Influence of Nutritional Supplementation to the Substrate on Vegetative and Reproductive Growth of Winter Mushroom, Flammulina velutipes (Curt. ex Fr.) Sing. and Chemical Changes of the substrates Produced during Growth of the Fungus (톱밥 배지(培地)에 대(對)한 영양첨가(營養添加)가 팽이버섯의 생장(生長)및 배지(培地)의 화학적(化學的) 성분(成分) 변화(變化)에 미치는 영향(影響))

  • Chang, Hak-Gil
    • The Korean Journal of Mycology
    • /
    • v.4 no.1
    • /
    • pp.31-44
    • /
    • 1976
  • The studies were carried out to examine the effects of supplementation of nutritional substances and physical conditions in substrate on the mycelial growth and yield of fresh sporophores of winter mushroom, Flammulina velutipes(Curt. ex Fr.) Sing. and to obtain further informations on the nutritional requirements of the fungus with reference to improvement of substrate through [analysis of chemical composition of the substrates during the cultivation period. The results obtained are summarized as follows: 1. The best yield of fresh sporophores, 84.4 g per 280 g substrate in a bottle, was obtained from the mixture of poplar sawdust 10 and rice bran 3 by volume when Flammulina velutipes was cultivated on the poplar sawdust supplemented by rice bran, wheat bran, cattle manure and various combinations of these materials as nutrient sources. The substrates of poplar sawdust 10 plus rice bran 3 and 2 or wheat bran 3 with a higher yield of fresh sporophores showed a comparatively higher content of total nitrogen. total sugar, and potassium. 2. The mycelial growth of the fungus was compared on the substrates of poplar sawdust supplemented by the several nutrient sources and poplar sawdust alone. The fastest linear growth occurred on substrates of poplar sawdust alone and poplar sawdust plus cattle manure deficient in sugar and nitrogen sources, but mycelial density was more sparse on the substrates. Also, growth in a solution extracted from these substrates was very meager. 3. In the substrates which varied with bulk density and moisture content optimum bulk density and moisture content for mycelial growth was 0.2g/cc and 72% on a dry weight basis, respectively, but the highest yield of fresh sporophores was obtained at the bulk density of 0.3g/cc and moisture content of 67%. 4. By increasing the ratio of rice bran in poplar sawdust the loss of total weight and ash, content at each stage was increased, and during the cultivation period of 75 days, loss of total weight of the substrates at inoculation was 17.8 to 28.8% and ash content increased about 12%. 5. 11 to 14% of the cellulose and 3 to 4% of the lignin content per original substrate were decreased without a great difference depending of the mixing ratio of rice bran. The soluble glucose concentration in the substrates was increased during the same period. 6. In the process of vegetative and reproductive growth of the fungus upon the substrates, the total nitrogen was increased in quantity per dry weight of sample but was reduced in absolute quantity to a minute extent. There is no great changes in content of organic nitrogen including amino acid nitrogen, and hydrolysable ammonium nitrogen during the vegetative growth period, but occurrence of sporophores resulted in a decrease in the nitrogen content of these forms. On the one hand, by an increase of additive amounts of rice bran, nitrogen contents of these forms were higher and the reduction range during the reproductive growth period became wider. 7. Mycelial growth of the fungus was accelerated in various liquid media supplemented with organic nitrogen sources such as peptone and yeast extract in comparison with addition of inorganic nitrogen sources. Furthermore, mycelial growth was mere vigorous in the media with higher content of organic nitrogen sources.

  • PDF

Newly Recommended Rates of N P K Fertilizers Based on Soil Testing for Some Upland Crops (토양검정치(土壤檢定値)에 의한 몇가지 밭작물(作物)의 삼요소(三要素) 기준량(基準量) 조정(調整))

  • Lee, Choon-Soo;Song, Yo-Sung;Lee, Ju-Young;Kwak, Han-Kang;Park, Young-Dae;Kim, Dong-Soo
    • Korean Journal of Soil Science and Fertilizer
    • /
    • v.26 no.2
    • /
    • pp.111-120
    • /
    • 1993
  • An attempt was made to investigate the yield response to the N P K fertilizer application for barley, soybean, corn, garlic, onion and potato in the famers' fields from 1971 to 1989. 1. The yield index of without-fertilizers plot when yield of N P K plot is regarded as 100, were 43~92 in plot without N, 71~94 in plot without $P_2O_5$ and 88~96 in plot without $K_2O$. The effects of each fertilizer application for upland crops were greater in barley, potato and corn for N, barley and soybean cultivated in reclaimed soil for $P_2O_5$ and potato and barley for $K_2O$. 2. The optimum levels of N, P and K fertilizers varied with the kinds of soil and crop in the ranges of 4.0~23.2kg/10a for N, 6.0~45.0kg/10a for $P_2O_5$ and 6.6~21.9kg/10a for $K_2O$. 3. The efficiencies of applied fertilizers were increased in cultivated soil in comparison with the reclaimed soil and the efficiencies were in order of potato, onion>barley, corn>soybean. 4. The regression equations of fertilizer recommendation for 5 crops excepting onion were obtained from relations between the organic matter in soil and the amount of N fertilizer applied, between the available $P_2O_5$ in soil and the amount of P fertilizer applied, and between the exchangeable K of soil and the amount of K fertilizer applied. 5. The reduced rates of P and K fertilizer application based on soil testing varied with regions in the ranges of 11.8~80.0 and 0~62.5%, respectively. And the recommendation for N fertilizer amount was necessary to increase or decrease depending on regions.

  • PDF

Studies on Dry Matter Yields , Chemical Composition and Net Energy Accumulation in Three Leading Temperate Grass Species II. Synthesis and accumulation pattern of nonstructural carbohydrate (주요 북방형목초의 건물수량 , 화학성분 및 New Energy 축적에 관한 연구 II. 비구조성탄수화물의 합성 및 축적형태)

  • ;;F. Muhlschlegel
    • Journal of The Korean Society of Grassland and Forage Science
    • /
    • v.6 no.2
    • /
    • pp.111-118
    • /
    • 1986
  • Sysnthesis and accumulation pattern or nonstructural carbohydrates in orchardgrass (Dactylis glomerata L.) cv. Potomac and Baraula, perennial ryegrass (Lolium perenne L.) cv. Reveille and Semperweide and meadow fescue (Festuca pratensis Huds.) cv. Cosmos 11 and N.F.G. were studied under different meteorological environments and cutting managements. The field experiments were conducted as a split plot design with three cutting regimes of 6-7 cuts at grzing stage, 4-5 cuts at silage stage and 3 cuts at hay stage in Korea and West Germany from 1975 to 1979. The results obtained are summarized as follows: 1. Accumlation of nonstructural carbohydrates in temperate grasses was influenced by grass species and regional climatic environments. Total nonstructural carbohydrates (TNC) of orchardgrass, perennial ryegrass and meadow fescue in Korea, taken as average of all cutting regimes, were shown a value of 4.39%, 6.08% and 8.01%, respectively, while those under cool summer climatic condition in West Germany accumulated to 10.42% (orchardgrass), 18.02% (perennial ryegrass) and 12.73% (meadow fescue). 2. Nonstructural carbohydrates in orchardgrass were accumulated mainly as mono-and disaccharose, while those in perennial ryegrass resreved as fructosan. The contents of fructosan and mono-and disaccharose were 1.34% and 3.04% for orchardgrass, 3.25% and 2.83% for perenninal ryegrass, respectively. Meadow fescue had a concentration of 3.93% fructosan and 4.08% mono-and disaccharose. 3. Synthesis and accumulation of nonstructural carbohydrates in temperate grasses were negative associated with increasing of air temperature (P$\leq$ 0.1%). Under hot stress during summer season in Korea, the contents of fructosan, mono-and disaccharose were decreased to about 0.34% nd 1.28% from a value of 1.34% and 2.69% in spring season. In Freising and Braunschweig, the concentration of reserved carbohydrates was less influenced by growing season. 4. Synthesis and accumulation pattern of nonstructural carbohydrates were shown a great respons to cutting frequency of the plants. Frequent cutting system under high temperature lowered the accumulation of reserved carbohydrates, especially fructosan and also caused to decrease the plant regrowth. However, under cool temperature, it shows a less differences of tructosan, mono-and disaccharose in the plants at all cutting systems.

  • PDF

Effects of Composted Pig Manure on Rice Cultivation in Paddy Soils of Different Texture (논토양검정에 의한 토성별 돈분퇴비 적정 시용량 결정)

  • Song, Yo-Sung;Kwak, Han-Kang;Hyun, Byung-Keun;Yeon, Byeong-Yeol;Kim, Pil-Joo
    • Korean Journal of Soil Science and Fertilizer
    • /
    • v.34 no.4
    • /
    • pp.265-272
    • /
    • 2001
  • A manure compost has been identified as an alternative to fertilizer to increase soil fertility and crop production in farming fields. The aim of the present study was to evaluate the effects of pig manure compost on soil properties and rice productivity as well as to determine the optimum application rate. In 1997, a field experiment was carried out to evaluate the growth of rice on sandy loam, loam, and clay loam soils amended with 0, 5, 10, and $20Mg\;ha^{-1}$ of pig manure compost plus NPK, which decided by soil testing. Rice yields were higher in soils receiving manure compost amendment. The maxim um yields were evaluated with $7,520kg\;ha^{-1}$ in the levels of $4.2Mg\;ha^{-1}$ of pig manure compost application plus NPK in sandy loam, $7,320kg\;ha^{-1}$ in the levels of $10.7Mg\;ha^{-1}$ in loam, and $6,320kg\;ha^{-1}$ in $17.2Mg\;ha^{-1}$ in clay loam soil. The optimum application rate of pig manure compost, which decided for 95% of maximum yields, was $4.0Mg\;ha^{-1}$ in sandy loam and $7.0Mg\;ha^{-1}$ in loam and clay loam soils under the condition of chemical fertilization by soil diagnosis. An increase in rice yield indicated a better nutrient status in compost-amended soil which was supported by the higher nutrient contents of N, P and K in shoot of plants grown in soil with manure compost amendment. Addition of manure compost increased available phosphate, silicate and exchangeable K in the amended soils according to the rate of compost application rate. It can be concluded that the manure compost could be a suitable organic fertilizer for improving rice productivity and soil fertility, and an application rate of $4.0Mg\;ha^{-1}$ in sandy loam and $7.0Mg\;ha^{-1}$ in loam and clay loam soils would give the optimum rice yields in the standard fertilization by chemical fertilization.

  • PDF

Development of Protein-rich Food Mixtures for Infants and Growing Children in Korea -(4) Nutritional and Biochemical Evaluation of Formulas F-P-5, F-P-6, F-P-7 and storage stability of F-P-4- (유유아(乳幼兒) 및 성장기아동을 위한 영양식품 개발에 관한 연구 -(4) F-P-5, F-P-6 및 F-P-7의 영양학적, 생화학적 검토 및 그 저장성-)

  • Kwon, Tai-Wan;Cheigh, Hong-Sik;Kim, Sook-He;Lee, Hyun-Keum
    • Journal of Nutrition and Health
    • /
    • v.3 no.3
    • /
    • pp.129-135
    • /
    • 1970
  • From the previous studies, F-P-4 formula was found to be comparable to full fat dry milk in its nutritive value and feeding performance. However, an attempt was made in order to make sure whether or not any possibility might exist, by which further improvement of nutritive quality and simultaneous reduction of product costs may be achieved. Using F-P-4 as a control, modifications were made in new formulas, F-P-5, F-P-6 and F-P-7 by reducing FPC, eliminating yeast from the mixture, and by enriching with methionine as needed. In particular, F-P-7 is completely free of FPC, hydrogenated oil and yeast. Yet, levels of total protein and fat were kept equal to those of F-P-4 in all formulas. An animal feeding test for all formulas using 10 female rats per group for 8 weeks and an infant feeding trial for F-P-5 and F-P-6 with 5 of each female infants under age of one for one month were conducted along with F-P-4 as a control. Almost the same results were obtained with F-P-4, 5 and 6, but F-P-7 showed the lowest body weight gain. FER of F-P-5 and 6 was 0.20 as was with F-P-4, while that of F-P-7 was 0.16. Acceptability to infants was excellent; growth, appearance and biochemical data were normal. As an example F-P-4 packed in 0.04mm polyethylene bags was used for storage study at $25^{\circ}C$ and relative humidity of $65{\sim}85%$ for 8 months. Although viable bacterial counts and vitamin C contents were reduced, peroxide and TBA values were increased gradually during such storage. Since there are also significant changes in color and organoleptic quality, the expected shelf life under the given conditions is considered to be about 2 months and thus further works are needed both on the product and packaging in order to improve the storage stability. Either elimination of yeast form F-P-4, that is F-P-5, or partial replacement of FPC with methionine, that is F-P-6 may well reduce material costs about 10%. Considering blending process of ingredients, F-P-5 is thus found to be the best formula developed. While F-P-7 free of FPC is inferior in its nutritive quality than that of others, but significantly superior than of rice. Furthermore, the material cost of the product can be reduced about 20% from that of F-P-4. And thus this vegetable blend is considered to be useful as a low cost supplementary food mixture for growing children.

  • PDF

Changes of chemical Composition According to the Ensiling Periods of Total Mixed Fermentation Feeds using Rice Straw and Green Forages (청초와 볏짚을 이용한 완전배합발효사료의 저장기간에 따른 화학조성분의 변화)

  • Lee, H.J.;KIm, W.H.;Kim, H.S.;Lim, K.B.;Ahn, B.S.;Cho, K.K.;Kang, S.H.;Kang, S.K.;Lee, H.G.;Woo, J.H.;Choi, Y.J.
    • Journal of Animal Science and Technology
    • /
    • v.44 no.6
    • /
    • pp.769-782
    • /
    • 2002
  • Three kinds of green forages(rye, oats and mixed forages) was harvested and mixed with rice straw, wheat bran and 2 grains(corn and soybean), which harvested 2 different dates(common harvesting dates, 7 days early to common harvesting dates). And each mixture was ensiled in 6 poly vinyl chlorides that was 60 liter, immediately. They were opened at 0, 5, 10, 25, 35, 60 and 100 days after ensiling for chemical analysis. And its effects of those TMFFs on feed values were observed. Average contents of water, crude protein, ADF, NDF, Ca and P of formulated TMFs were 72 to 75%, 14.75 to 18.24, 12.47 to 19.07, 39.82 to 47.01, 0.99 to 1.07 and 0.38 to respectively. Crude protein content was the highest in the mixed forages-TMFF and the lowest in the rye-TMFF. The ADF and NDF contents of rye-TMFF were higher than orthers. And CP, ADF, NDF, TDN, P and Ca contents were no significant difference among treatments regardless of storage period and harvest time, but all treatments indicated good quality. Intenal temperatures of TMFF were shown to be 1 to 5$^{\circ}C$ higher than ambient temperatures. The temperature of the Oat-TMFF formulated during winter sustained higher to the level of 6${\sim}$9$^{\circ}C$ for 10 days. The pH of TMFF were 4.0 to 4.2 and the content of $NH_3$-N was shown to be 7.79 to 8.23mg/$d{\ell}$. In the VFA contents, any tendency was not shown at all treatments depending on harvest time. Even though rye-TMFF showed the lowest VFA value. At all treatments except rye-TMFF, propionate production was increased and stable after 25 days of storage. Digestibility of rice straw from TMFF on DM basis was 15${\sim}$20% higher compared with non-treated rice straw.

Neutralization of Pyrophyllite Mine Wastes by the Lime Cake By-Product (부산석회를 이용한 납석광산 폐석의 중화처리)

  • Yoo, Kyung-Yoal;Cheong, Young-Wook;Ok, Yong-Sik;Yang, Jae-E.
    • Korean Journal of Environmental Agriculture
    • /
    • v.24 no.3
    • /
    • pp.215-221
    • /
    • 2005
  • Numerous abandoned or closed mines are present in the steep mountain valleys in Korea due to the depression of the mining industry since the late 1980s. From the mines, enormous amounts of wastes were dumped on the slopes causing sedimentation and acid mine drainage to be discharged directly into streams causing detrimental effects on surrounding environment. Objective of this research was to evaluate the feasibility of the lime cake by-product from the soda ash production (Solvay process) to neutralize the pyrophyllite mine wastes, which have discharged the acid drainage to soil and stream in the watershed. The pH of mine wastes was strongly acidic at pH 3.67 containing over 16% of $Al_2O_3$ and 11% of $Fe_2O_3$. Whereas the lime cake by-product was strongly basic at pH 9.97 due to high contents of CaO, MgO and $CaCl_2$ as major components. Column experiments were conducted to test the neutralizing capacity of the lime cake by-product for the acidic pyrophyllite mine wastes. The column packed with the wastes (control) was treated with the lime cake by-product, calcium carbonate, the dressing soil or combination. The distilled water was eluted statically through the column and the leachate was collected for the chemical analyses. Treatments of the mine wastes with the lime cake by-product (or calcium carbonate) as mixtures increased pH of the leachate from $3.5{\sim}4.0\;to\;7{\sim}8$. Concentrations of Fe and Al in the leachate were also decreased below 1.0 mg $L^{-1}$. A Similar result was observed at the combined treatments of the mine waste, the lime by-product (or calcium carbonate) and the dressing soil. The results indicated that the lime cake by-product could sufficiently neutralize the acid drainage from the pyrophyllite mine wastes without dressing soils.

Soil CO2 Monitoring Around Wells Discharging Methane (메탄 유출 관정 주변의 토양 CO2 모니터링)

  • Chae, Gitak;Kim, Chan Yeong;Ju, Gahyeun;Park, Kwon Gyu;Roh, Yul;Lee, Changhyun;Yum, Byoung-Woo;Kim, Gi-Bae
    • Economic and Environmental Geology
    • /
    • v.55 no.4
    • /
    • pp.407-419
    • /
    • 2022
  • Soil(vadose zone) gas compositions were measured for about 3 days to suggest a method for monitoring and interpreting soil gas data collected around wells from which methane(CH4) is outflowing. The vadose zone gas samples were collected within 1 m around two test wells(TB2 and TB3) at Pohang and analyzed for CO2, CH4, N2 and O2 concentrations in situ. CO2 flux was measured beside TB2. In addition, gas samples from well head in TB2 and atmospheric air samples were collected for comparison. Carbon isotopes of CO213CCO2) of samples collected on the last day of the study period were analyzed in the laboratory. The two test wells (TB2 and 3) were 12.7 m apart and only TB3 was cemented to the surface. According to the bio-geochemical process-based interpretation, the relationships between CO2 and O2, N2, and N2/O2 of vadose zone gas were plotted between the lines of CH4 oxidation and CO2 dissolution. In addition, the CH4 concentrations of gas samples from the wellhead of the uncemented well (TB2) were 5.2 times higher than the atmospheric CH4 concentration. High CO2 concentrations (average 1.148%) of vadose zone gas around TB2 seemed to be attributed to the oxidation of CH4. On the other hand, the vadose zone CO2 around the cemented well(TB3) showed a relatively low concentration(0.136%). This difference indicates that the vadose zone gas(including CO2) around the CH4 outflowing well were strongly affected by well completion(cementing). This study result can be used to establish strategies for environmental monitoring of soil around natural gas sites, and can be used to monitor leakage around injection and observation wells for CO2 geological storage. In addition, the method of this study is useful for soil monitoring in natural gas storage and oil-contaminated sites.

Physical Properties of Volcanic Rocks in Jeju-Ulleung Area as Aggregates (제주도 및 울릉도에서 산출되는 화산암의 골재로서의 물성 특징)

  • Byoung-Woon You;Chul-Seoung Baek;Kye-Young Joo
    • Economic and Environmental Geology
    • /
    • v.57 no.2
    • /
    • pp.205-217
    • /
    • 2024
  • This study evaluated the physical characteristics and quality of volcanic rocks distributed in the Jeju Island-Ulleung Island area as aggregate resources. The main rocks in the Jeju Island area include conglomerate, volcanic rock, and volcanic rock. Conglomerate is composed of yellow-red or gray heterogeneous sedimentary rock, conglomerate, and encapsulated conglomerate in a state between lavas. Volcanic rocks are classified according to their chemical composition into basalt, trachybasalt, basaltic trachytic andesite, trachytic andesite, and trachyte. By stratigraphy, from bottom to top, Seogwipo Formation, trachyte andesite, trachybasalt (I), basalt (I), trachybasalt (II), basalt (II), trachybasalt (III, IV), trachyte, trachybasalt (V, VI), basalt (III), and trachybasalt (VII, VIII). The bedrock of the Ulleung Island is composed of basalt, trachyte, trachytic basalt, and trachytic andesite, and some phonolite and tuffaceous clastic volcanic sedimentary rock. Aggregate quality evaluation factors of these rocks included soundness, resistance to abrasion, absorption rate, absolute dry density and alkali aggregate reactivity. Most volcanic rock quality results in the study area were found to satisfy aggregate quality standards, and differences in physical properties and quality were observed depending on the area. Resistance to abrasion and absolute dry density have similar distribution ranges, but Ulleung Island showed better soundness and Jeju Island showed better absorption rate. Overall, Jeju Island showed better quality as aggregate. In addition, the alkaline aggregate reactivity test results showed that harmless aggregates existed in both area, but Ulleungdo volcanic rock was found to be more advantageous than Jeju Island volcanic rock. Aggregate quality testing is typically performed simply for each gravel, but even similar rocks can vary depending on their geological origin and mineral composition. Therefore, when evaluating and analyzing aggregate resources, it will be possible to use them more efficiently if the petrological-mineralological research is performed together.