• Composites Research
• /
• v.34 no.5
• /
• pp.330-336
• /
• 2021

Alumina powder is one of the widely used materials for industry, but there is a problem that the strength of the product changes depending on the powder packing state. To solve the above problem, previous studies have been conducted to increase the particle packing efficiency, but most of the existing studies analyzed the packing characteristics of millimeter-scale particles, so the physical properties are different from those of the micrometer scale. It is difficult to apply to the micrometer scale. In this paper, a three-step experiment was performed using a statistical method to increase packing using micrometer-scale alumina powder. First, a size combination with high packing and a mixing ratio were selected using the mixture test design method, and an appropriate excitation frequency was selected by analyzing the height change according to the frequency change in the vibration test apparatus. Finally, an alumina powder packing experiment was performed based on the experimental results mentioned above. As a result, it was confirmed that the maximum height variation was 42% higher than the maximum value of the 155 measurements performed when selecting the packing size combination. It is thought that this study will serve as basic data for processing and packing research using fine powder.

• Journal of the Korean Applied Science and Technology
• /
• v.41 no.2
• /
• pp.318-328
• /
• 2024

In this study, we enhanced the emulsifying power and solubilization of sucrose stearate (SS) by creating mixtures with sodium deoxycholate (SDOC) and PEG-40 hydrogenated castor oil (HCO). We employed the design of mixture experiments (DOME) methodology to identify the optimal composition of the mixture, and the impact of varying the mixture composition on its characteristics was examined through regression analysis of the experimental data. It was revealed that the emulsifying power for coconut oil was most improved when only SDOC was added to SS, and solubilization was most improved when only HCO was added, while the emulsifying power for cetyl ethylhexanoate (CEH) was most significantly improved when SDOC and HCO were added together. As a result of simultaneous optimization of three characteristics, emulsifying power for each of coconut oil and CEH, and solubilization, the optimal surfactant mixture composition was determined as SS 0.7939, SDOC 0.0586, and HCO 0.1475.

• Journal of the Korean Applied Science and Technology
• /
• v.39 no.5
• /
• pp.623-631
• /
• 2022

Using the design of experiment (DOE), factors affecting the particle size of hydrated liquid crystalline vesicles containing a high content of ceramide were analyzed and the mixture composition was optimized. Manufacturing temperature, amount of ethanol, and ultrasonic time were selected as the main variables affecting the droplet size of the vesicles, and the effect of these variables on the droplet size was examined through the signal to noise (S/N) ratios of Taguchi method and ANOVA analysis. In addition, mixture composition experiments of three lipid components constituting the vesicle membrane, hydrogenated phosphatidyl choline (HPC), cholesterol (Chol), and ceramide (Cer), were performed according to the simplex central design matrix of the mixture. Regression analysis was conducted with the experimental data to obtain a model equation, and the optimal mixing composition of the three lipid components to minimize the vesicle droplet size was determined as HPC (0.6), Chol (0.1), and Cer (0.3).

• Applied Chemistry for Engineering
• /
• v.32 no.5
• /
• pp.574-580
• /
• 2021

The main goal of this study was to find an optimal surfactant mixture composition for the development of the best performing cleansing products. Three different surfactants including sodium cocoyl alaninate (SCoA), cocamidopropyl betaine (CPB), and decyl glucoside (DG) were selected, which showed excellent properties in detergency, foaming height, and contamination rate through preliminary experiments. The experiments by simplex centroid design matrix for surfactant mixtures were performed, and the regression analysis was conducted with the experimental data. Surface response model equations, which is statistically significant (p < 0.05), were obtained. The optimal composition of the surfactant mixture was also determined as SCoA (0.22), CPB (0.78), and DG(0.00) from simultaneous optimization of three response variables.

• Korean Journal of Food Science and Technology
• /
• v.35 no.4
• /
• pp.617-622
• /
• 2003

Experimental designs were applied to optimize the mixture ratio for the extrudate made by soymilk residue and corn grits. Nine candidate points were examined for their significance on extrudate using the modified distance design. Bending force, expansion ratio, bulk density, water solubility index (WSI), water absorption index (WAI) and color $(L^*,\;a^*,\;b^*)$ were the significant factors improving the extruded cereal production, and these values were applied to the mathematical models. Results showed that bending force, expansion ratio WSI, WAI and color $(L^*,\;b^*)$ increased with increasing the corn grits, whereas bulk density tended to decrease. The statistical study showed that the fitted models were adequate to describe the contour plot and all responses. Optimum mixture ratio allowing to maximize the two responses (expansion ratio and $b^*$) and minimize the response (WAI) were examined with a numerical optimization methods. The numerical optimization method was obtained as 53.18% : 46.19% (corn grits : soymilk residue).

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.13 no.3
• /
• pp.1002-1007
• /
• 2012

The manufacturing method of the pillar is one of the main process where it is used in vacuum glazing and semi-conductor display field. Pillar can be arranged by screen printing method. However it may unable to spread all pattern of metal mask according to the ingredient of the mixture. In addition, spreaded mixture doesn't maintain the original shape according to the viscosity. In this research, the pillar tried to be arranged through the screen printing by using the inorganic compound of the alumina and silica base. This study suggested a method in which it can decrease the test frequency and design the composition of the vacuum glass pillar by using the mixture design.

• Journal of Adhesion and Interface
• /
• v.9 no.1
• /
• pp.22-27
• /
• 2008

The effect of functional monomers on the acrylic pressure sensitive adhesive (PSA) property was measured. Design of experiments in order to optimal peel adhesion was applied and commercial program (MINITAB) was used. Analysis was used to mixture design (special cubic model) in response surface methodology. Optimal monomer compositions was construed by 2-EHA (0.8861), EA (0.0639), MAA (0.03) and AAm (0.02). The estimated regression equation was as follows : $$y=54.8816x_1+80.7067x_2-44.4700x_3-99.0288x_1x_2+60.7706x_1x_3-441.030x_2x_3+974.341x_1x_2x_3$$.

• The Korean Journal of Food And Nutrition
• /
• v.20 no.1
• /
• pp.1-8
• /
• 2007

Tortillas were prepared using rice and wheat flour. The experimental design incorporated thee independent variables(rice, wheat flour and moisture content) producing 14 samples of different proportions of each variable for each tortilla. The following were analysed using Design Expert 6 to unveil the influences of these variables on tensile strength and color(L, a, b). Results indicated that tensile strength increased with increasing rice and wheat flour content, however, decreased with increasing moisture content. Lighteness(L), of the tortilla increased with increased rice content whereas yellowness(b) increased with increased wheat flour content. The model suggests that tensile strength and color(L, a, b) in tortillas are highly correlated(SD Comment - give correlation coefficient and p-value). As well, the numerical optimization method suggests that the ratio of wheat flour to rice flour to moisture content which maximizes the three responses(tensile strenth, L and b) is 18.26 : 33.92 : 39.24%, 28.15 : 25.77 : 37.50%.

• Elastomers and Composites
• /
• v.41 no.1
• /
• pp.3-9
• /
• 2006

Optimal conditions for preparation of starch/PVA blends were investigated with the consideration of factors that may influence mechanical properties of the blends. Multiplex mixture optimal method as a statistical method were performed and then tensile strength, strain at break, Young's modulus and tear strength of films of the blends were measured to determine the optimal conditions for preparation. The mechanical properties needed for the degradable agricultural mulch were the target of this experiment. Results showed that although the strain at break was a little insufficient, the other properties were very close to the target. This means that the mechanical properties of the film from this blend as a whole are very compatible with those of the reference mulch.

• Journal of the Korean Recycled Construction Resources Institute
• /
• v.7 no.1
• /
• pp.37-43
• /
• 2019

This research studied production of lightweight filling production for sink hole restoration utilizing various industrial by-products(2kinds of fly ash, petro-cokes CFBC ash, blast furnace slag fine particle). For this purpose, the mixed raw material properties(compressive strength) behaviors according to the blending ratio of industrial by-products were examined by applying the experimental design method and statistical analysis was performed using the commercial program MINITAB. Compressive strengths of industrial by-products were strongly dependent on blast furnace slag powder. Compressive strength(3days aging) was 3~11MPa depending on the amount of blast furnace slag powder used. The use of CFBC fly ash was evaluated to have the least effect on compressive strength. In addition, the compressive strength and the coefficient of permeability were measured by preparing foamed concrete for the experimental batch 1 condition in the mixture experimental design. In this case, the bulk density is 0.9 to 1.0, the apparent porosity is 30 to 50%, the compressive strength(3days old) is 1 to 2MPa, and the permeability coefficient is $10^{-2}$ to $10^{-3}cm/sec$.