• 제목/요약/키워드: 합금층

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AZ9lD 상용 마그네슘합금에 코팅된 Cr$_2$O$_3$층의 기계적 및 내마모 특성에 미치는 플라즈마 용사조건의 효과 (Effect of Plasma Spraying Parameter on Mechanical and Tribological Property of Cr$_2$O$_3$ Coating Layer on AZ9lD Commercial Magenesium Alloy)

  • 이수완;박종문;이명호;김진수
    • 한국표면공학회지
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    • 제30권6호
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    • pp.400-405
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    • 1997
  • The experimental study has been performed to deposit to deposit chromia powder on magnssium alloy for tribological and mechanical properties. The optimal condition was obtained by changing the spray condition such as working distance and gun power. As ceramics was coated onto the a light metal such as Mg according to the weight reduection of the car engine block, it could acquire that the engine efficiency deu to the weight reduction and properties such as resistance to heat, as well as wear. Coating qualities are discussed with respect to hardness, tribologicalproperty, and microstructure. The tribological and mechanical properties are investigated by using the reciprocal configuration tribometer and microharduess tester. Wear mode is determined by observing the SEM morhpology of wear track and cross section view of wear track.

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전기도금법에 의해 생성된 Ni-B 합금도금층의 물성에 미치는 B 함량의 영향 (Influence of B Content on Properties of Ni-B Electrodeposit)

  • 이규환;장도일;권식철
    • 한국표면공학회지
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    • 제37권4호
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    • pp.208-214
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    • 2004
  • The influence of the boron content on the various properties of Ni-B alloy films produced by electrodeposition was investigated. The considerable reduction in grain size was observed with increasing boron content. The internal stress was tensile and increased linearly with increasing boron content. Hardness increased up to $750H_{v}$ at 2 at% boron and then kept the value to 11 at% boron for as-plated Ni-B coatings. The hardness of Ni-B films increased up to $1,250H_{v}$ due to the intermetallic$ Ni_3$B precipitation by the heat treatment, and maximum hardness of each coating increases with boron content. Wear resistance decreased with increasing the boron content because of high friction coefficient and brittle fracture of film which has higher content of boron.

Co-Ni-P합금도금층의 자기적 성질에 관한 연구 (Magnetic Properties of Electrodeposited Co-Ni-P Alloys)

  • 백민선;김영근;강탁;손헌준
    • 한국표면공학회지
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    • 제24권2호
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    • pp.96-102
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    • 1991
  • Co-Ni-P alloys were electrodeposited from NH4Cl-sulfate-hypophosphite baths under various plating conditions. Their effective anisotropic magnetic field which is one of the important properties for magnetic recording materials were investigated as the function of alloy compositions and c-axis orientation. The preferred orientation and the contents of Ni and P depend on the pH of solutions and also on the current density. It was found that the alloy films deposited from the solutions of pH4 at high current density had c-axis orientation parallel to the growth direction and the effective anisotropic fields sufficient for perpendicular magnetic recording application.

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아연-니켈합금 전기도금층의 부식특성 (Corrsion of Ni-Ze Electrodeposited Alloy)

  • 예길촌;신현준
    • 한국표면공학회지
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    • 제21권2호
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    • pp.39-46
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    • 1988
  • Corrosion behavior of 5-26wt% Ni-Zn electrodeposited alloys was investigated by means of dipping electrochmical polarization measurement and galvanic coupling test. The weight loss and anodic polarization curve of coatings were measured by means of dipping and polarization measurement respectively. The galvanic protection effect of alloy coatings was measured by galvanic coupling test and the surface morpholgy of coatings was observed after corrosion testing. Our findings support thous of previous investigations showing that ${\gamma}$single phase coatings, while galvanic pprotection effect of dual phase coatings improved in comparison with ${\gamma}$single phase coating. The formation of colony in coating of ${\gamma}$and η+${\gamma}$ dual phsae caused the localized corrsion and increased the corrosion rate of the Ni-Zn coating.

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알루미나의 Ag-33.5Cu-1.5Ti 브레이징 합금 계면에서 생성되는 반응층의 미세조직 관찰과 상 동정 (Identification and Microstructure Observation of Reaction Products formed at Alumina/Ag-33.5Cu-1.5Ti Brazing alloy Interface)

  • 최시경;권순용
    • 한국세라믹학회지
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    • 제33권9호
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    • pp.1045-1049
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    • 1996
  • Pressureless-sintered polycrystalline alumina and carbon steel were joined with Ag-33.5Cu-1.5Ti (wt%) brazing alloy. SEM observation revealed that two reaction layers with different thicknesses were continuously formed between the alumina and the brazing alloy. A thick layer formed on the brazing alloy side was identified as Ti3(Cu0.93Al0.07)3O phase with diamond cubic structure. Another thin layer adjacent to the alumina was revealed as $\delta$-TiO phase of which the crystal structure was HCP with a lattice parameter of a0=0.419 nm and c0=0.284 nm. It was confirmed using XPS analysis that $\delta$-TiO was formed directly by a redox reaction of alumina with titanium ir, molten brazing alloy.

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물 첨가된 열 화학 기상 증착법을 이용한 다중벽 탄소나노튜브의 저온 합성 (Low Temperature Growth of Multi-walled Carbon Nanotubes by Water-assisted Chemical Vapor Deposition)

  • 김영래;전홍준;이내성
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 하계학술대회 논문집 Vol.9
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    • pp.430-430
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    • 2008
  • 열화학기상 증착법으로 2원계 합금인 Invar 36(63wt% Fe, 37wt% Ni)을 이용하여 다중벽 탄소나노튜브를 360도의 저온에서 까지 합성이 가능함을 확인하였다. 촉매와 Si 기판과의 silicide형성을 막기 위한 Ti층의 두께가 증가함에 따라서 탄소나노튜브의 길이가 잘 자라는 것을 확인하였으며, 미량의 물이 첨가 되었을 경우 탄소나노튜브의 길이 성장에 큰 변화가 있음을 확인하였다. 또한 물을 포함하는 실험에서는 촉매인 Invar36의 두께가 0.5 nm 일 때에 비하여 0.25 nm 두께에서 물에 대한 영향이 더 크게 나타남을 SEM 사진을 통해 확인할 수 있었다.

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Properties of Boron Carbide Thin Films Deposited by Partially Reactive Magnetron Sputtering

  • Lee, K. E.;Kim, C. O.;Kim, J. H.;Lee, J. Y.;Park, M. J.;Lee, C. B.
    • 한국자기학회:학술대회 개요집
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    • 한국자기학회 2002년도 동계연구발표회 논문개요집
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    • pp.124-125
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    • 2002
  • 최근 자성막의 놀은 자기기록 밀도증가에 따른 고밀도 자성기록매체인 하드디스크(HDD)는 현재 80GByte까지의 저장용량을 가진 하드디스크의 자성합금층 보호막으로 DLC(Diamond-Like Carbon)가 이용되고 있다. 고저장용량을 가지는 하드디스크의 보호막 두께가 점차 얇아짐에 따라 보호막 재료의 경도 및 윤활성은 더욱 중요시되고 있다. 그러나, 보호막의 두께가 감소하면서 현재 적용되고 있는 DLC막으로는 조만간 물리적 한계에 도달할 것으로 예상된다. (중략)

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3-D 복합재료 샌드위치 구조물의 2층 경전철 철도차량 구조체 적용성에 관한 연구 (A Study on the Application of 3-D Sandwich Composite Structures to the Double-deck Light Train Carbody)

  • 이영신;김재훈;이호철;길기남;박병준
    • 한국철도학회논문집
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    • 제3권2호
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    • pp.92-99
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    • 2000
  • Composites are very useful material for light train carbody due to its high specific strength and lightweight characteristics. The composites, called 3-D board, are developed with a special stitching method. In this process, the glass fiber fabrics of skin material and foam core material are stitched together with glass fiber thread. The glass thread in Z-axis turns into FRP form. The conventional delamination problem can be solved with 3-D sandwich structure. In addition, with the lower density of foam, the weight of the panel and the operation expenses can be highly reduced. To evaluate the usefulness of the 3-D board, the double-deck light train carbody is studied. The stress analyses are carried out under various loads and boundary conditions with FEM Code, ANSYS. On comparing with the aluminum carbody, 3-D board carbody can be reduced by about 2 ton for the total weight of carbody.

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$ZrO_2$와 NiTi 합금의 반응접합 : 분석투과전자현미경을 이용한 $ZrO_2/NiTi$ 접합층 반응생성물 분석 (Reaction Bonding of $ZrO_2$ and NiTi : Reaction Products Analyses on $ZrO_2/NiTi$ Bonding Interface with AEM)

  • 김영정;김환
    • 한국세라믹학회지
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    • 제30권11호
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    • pp.949-954
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    • 1993
  • Microstructural development at the ZrO2/NiTi bonding interface and reaction products were examined and identified with SEM and AEM. Ti-oxide, Ti2Ni and Ni2Ti layer were observed whose thickness depends on bonding temperature typically. The development of Ti-oxide layer is related with oxygen ion in ZrO2 and liquid phase Ti2Ni. It is considered that compositional deviation from homogeneity and residual stress caused by thermal expansion mismatch are closely related with the formation of the Ti2Ni phase.

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Cr-C합금 도금층 제조 및 특성 연구 (The study on Cr-C alloy electroplating and its characteristics)

  • 김동수;김만;박상언;남기석;장도연;권식철;신동수
    • 한국표면공학회지
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    • 제34권1호
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    • pp.49-55
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    • 2001
  • The addition of organic compound containing -COOH, X$800_2$, -CHO group such as formic acid, formamide, formaldehyde or diethyleneamine to a chromium electroplating bath results in a chromium deposit in which carbon is incorporated. Such deposits have fewer defects than chromium layers produced by a conventional method. It was found that the as-deposited layers were amorphous and auger electron spectroscopy (AES) showed that carbon is distributed uniformly in the deposit. During heat treatment, Cr-C deposits began to crystallize at $400^{\circ}C$, and at $800^{\circ}C$ they were crystallized into chromium carbides and oxides. The effects of current density, amount of additives, applied current waveform on Cr-C alloy electroplating were examined.

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