• Title/Summary/Keyword: 필러

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A STUDY ON TOOTHBRUSH ABRASION OF CERVICAL RESTORATIVE MATERIALS (치경부 심미수복재의 잇솔질 마모에 관한 연구)

  • Baik, Byeong-Ju;Yang, Jeong-Sook;Lee, Doo-Cheol;Kim, Jae-Gon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.28 no.1
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    • pp.118-128
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    • 2001
  • This study was performed to evaluate the toothbrush abrasion characteristics of seven commercially available light-cured cervical restorative materials one resin-modified glass-ionomer material(Fuji II LC) three polyacid-modified composites(Compoglass, Dyract, F2000), and three light-cured composites(Heliomolar, Palpique Estelite, UniFil F). All samples were stored in distilled water at $37^{\circ}C$ for 10 days. 2.0N of weight was loaded during the test and the abraded surfaces were examined with profilometer and SEM after 100,000 cycles. The results obtained were summarized as follows; 1. The highest hardness value of 79.7 was observed in the FT group and the lowest value of 20.0 was observed in the HM group. Results of Tukey test showed that an overall significant difference was indicated except the CG and DR groups(p<0.05). 2. The highest surface roughness was observed in the FL group and the lowest was observed in the UF group. Results of Tukey test showed the significant difference between the FL or FT and UF groups(p<0.05). 3. Statistically higher abrasion and surface roughness were observed for the dentifrice of paste type, Perio A+, than for that of gel paste type, Tom & Jerry. 4. The surface roughness values increased on the abraded surfaces because of the protrusion of filler particles due to selective removal of matrix resin.

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Evaluating Stability and Functionality of Hybrid Erosion Control Dam for Reducing Debris Flow Damage in Forested Catchment Nearby Urban Area (도시생활권의 토석류 피해 저감을 위한 복합형 사방댐의 안정성 및 기능성 평가)

  • Kim, Kidae;Kim, Dongyeob;Seo, Junpyo;Lee, Changwoo;Woo, Choongshik;Kang, Minjeng;Jeong, Sangseom;Lee, Dongkyun
    • Journal of Korean Society of Forest Science
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    • v.107 no.1
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    • pp.59-70
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    • 2018
  • The objective of this study was to develop erosion control dam for preventing disaster in consideration of characteristics of forested catchment near urban area, and to assess its stability and functionality to see its practicability in the field. Two types of hybrid erosion control dams were developed including debris flow prevention dam by using pillar and float board screen type and debris flow control dam by using groyne. Also, review about their static (sliding, overturning, bearing capacity) and dynamic (member force) stability was carried out. According to the result, most of the assessed items met standard safety level although there were some cases where assessed items were short of stability criteria against impact. Also, after miniature flume experiments based on the developed erosion control dam to prove structure function (material catch, deposit), it turned out the dam decreased flow sediment amount and velocity while increasing sediment-capturing capacity by 3.5 times on average compared to the one controlled without erosion control dam. When function of erosion control dam for forested catchment near urban area is quantified based on future flume experiments in a variety of conditions, the dams can be practically used in the urban area, contribution to effectively reducing debris flow damage.

Extraction of Micro Filler from Bio-waste Material (Bio waste 소재로부터의 마이크로 필러 추출)

  • Nam, Gibeop;Song, Jung-Il
    • Composites Research
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    • v.31 no.5
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    • pp.209-214
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    • 2018
  • This paper explain about the development of environmental friendly, low cost and stable supply material i.e., rice husk and shell were used as micro incorporating bio waste filler. Those were processed by ball mill and analyzed through micro observation by FE-SEM, EDS and particle size distribution. The obtained filler was mixed with epoxy resin for the manufacturing of CFRP composite and study tensile properties. In EDS analysis main contents of rice husk and rice husk ash are C, O and Si. When rice husk was burned C and Si ration were increased. Shell powder has C, O and Ca. It caused $CaCO_3$ from shell. Surface weighted mean of rice husk powder is $6.19{\mu}m$ and volume weighted mean is $14.77{\mu}m$. And it has rod type particles which caused hair and husk structure parts. Surface weighted mean of rice husk ash powder is $1.55{\mu}m$ and volume weighted means is $8.20{\mu}m$. Surface weighted mean of shell powder is $2.53{\mu}m$ and volume weighted mean is $5.79{\mu}m$. The tensile decreased with increasing the content of micro filler in CFRP composites. In case of rice husk, the significant decrement of tensile strength was observed. and in case of shell powder, there is no effect of changes take place in tensile strength.

Development of welding process to rootpass for U-Groove without gap in pipe 1GR butt welding (파이프 1G 회전 맞대기 용접에서 갭 없는 U-그루브의 루트패스 용접공정 개발)

  • Son, Chang-Hui;Kim, Nam-Gyu;Cho, Sang-Myeong
    • Proceedings of the KWS Conference
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    • 2010.05a
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    • pp.40-40
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    • 2010
  • 산업현장에서는 파이프 또는 탱크류의 1GR용접에서 안정적인 이면비드를 가지는 루트패스 용접을 위해 2~3mm의 루트갭을 띄우고 용접봉 또는 필러와이어를 사용하는 TIG용접을 주로 한다. TIG용접은 고품질의 이면비드가 얻어지며, 용접인자의 제어가 쉽다는 장점이 있어 루트패스 용접에 많이 사용되고 있지만, 루트갭을 띄우면 이면비드는 잘 얻어지지만 용착금속량이 많아지게 되어 제작원가가 상승되고, 또한 소모성 와이어를 사용하는 GMAW에 비해 생산성이 낮다. 따라서, 안정적인 이면비드를 가지면서 생산성이 높은 1GR GMAW 루트패스 용접공정의 개발이 요구되지만, 이 경우도 루트갭이 2~3mm로 정해져 있으면 Fit-up공정에서 공수가 많이 필요하므로 근본적으로 루트갭이 없는 그루브에 대한 루트패스 용접이 더 바람직하다. 본 연구에서는 루트면 2.7mm를 가지는 U-그루브의 갭 없는 루트패스 용접에서 안정적인 이면비드가 형성되는 조건을 검토하기 위해 2.7t의 평판에 대하여 경사상진 각을 주고 기초 실험 후, U-그루브 맞대기 용접 실험을 진행하였다. 이 때, 경사상진 각은 용융금속이 중력으로 인해 아크 후방으로 밀리게 되고, 그로 인해 아크가 모재에 직접 닿게 되어 용입이 더 깊게되므로, 이면비드의 형성에 더 유리하다. 두께 2.7t의 연강 시편 2개를 갭 없는 I-그루브 맞대기 이음에서 Ǿ1.2 연강 솔리드 와이어를 사용하여 GMAW용접을 실시하였고, 용접전류, 용접속도, 경사상진 각, 위빙 폭, 위빙 주파수를 변경하여 각 조건에 대한 이면비드를 관찰하였다. 그 결과 경사상진 각 $25^{\circ}$, 전류 200A, 위빙폭 3mm, 위빙주파수 3Hz의 조건에서 안정적인 이면비드를 얻을 수 있었다. 또한, 현장에서 Fit-up중 발생할 수 있는 루트갭의 문제에 대하여 루트갭 1.2mm의 I-그루브 맞대기 용접에서 경사상진 각, 위빙 폭, 위빙 주파수는 갭 없이 실시한 실험에서 얻어진 가장 안정적인 결과를 사용하였고, 용접 전류, 용접 속도를 변경하여 이면비드를 관찰하였다, 그 결과 갭이 없을 때보다 약 80A 낮은 전류 조건인 120A에서 안정적인 이면비드를 얻을 수 있었다. 앞선 실험들을 기초로 하여 U-그루브 맞대기 용접을 실시 하였고, I-그루브 맞대기 용접에서 사용한 조건들과 유사한 용접 전류, 용접 속도에서 안정적인 이면비드를 얻을 수 있었다.

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HYDROLYTIC DEGRADATION OF DENIAL COMPOSITE RESINS (수종 치과용 복합레진의 가수분해)

  • Yang, Kyu-Ho;Kim, Jung-Ran
    • Journal of the korean academy of Pediatric Dentistry
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    • v.27 no.2
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    • pp.370-378
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    • 2000
  • The composite restorative resins have their insufficient resistance to wear. The subsurface degradation within the restoration is considered to be associated with wear. The aim of this study was to evaluate the resistance to degradation of six commercial composite resins in an alkaline solution. The brands studied were Clearfil APX(Kuraray), Heliomolar(Vivadent), Surefil(Dentsply), TPH(Dentsply), Tetric Ceram(Vivadent), and Z100(3M). Preweighed discs of each brand were exposed 0.1N NaOH solution at $60^{\circ}C$. After 14 days they were removed, neutralized with HCL, washed with water and dried to constant mass at $60^{\circ}C$. Resistance to degradation was evaluated on the basis of the following parameters: (a) mass loss(%) - determined from pre-and post-exposure specimen weights; (b) Si loss (ppm)-obtained from ICP-AE analysis of solution exposed to specimens; and (c) degradation depth$({\mu}m)$ - measured microscopically (SEM) from polished circular sections of exposed specimens. The results were as follows: 1. The mass loss was in descending order by Z100, TC H, S, CL, TPH and in the range of $0.45\sim3.64%$ 2. The degradation layer depth was in descending order by H, Z100, S, TC, TPH, CL and in the range of $10.85\sim73.38{\mu}m$ 3. For the Si concentration, Z100 was the highest of all 4. The highly significant correlation(r=0.81, p<0.05) was observed between mass loss and degradation depth. 5. Under scanning electronmicroscopy, the degradation of connection between resin matrix and fillers was observed 2 weeks after soaking in NaOH solution.

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Acid Neutralizing Capacity of Giomer in an Acidic Solution (자이오머의 산성용액에 대한 산중화능)

  • Ahn, Ha-Na;Kim, Seon-Mi;Choi, Nam-Ki
    • Journal of the korean academy of Pediatric Dentistry
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    • v.40 no.3
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    • pp.168-176
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    • 2013
  • The aim of this study was to evaluate the acid neutralizing capacity and to observe surface changes of giomer in comparison with composite resin, when it comes in contact with an acidic solution. A packable giomer(Beautifil II) and a flowable giomer(Beautifil Flow F02) were used as experimental groups, while a packable composite resin($Filtek^{TM}$ Z-250) was used as control group. pH values were measured after mixing the specimens of the disc and powder types with a pH 2.0 hydrochloric acid solution, respectively. Also, in the case of powder type giomers used in the earlier experiment, their pH values were measured again after mixing them with a fresh acid solution. Moreover, surface structure changes of disc type specimens were observed by using a scanning electron microscopy(SEM). In the disc type test, the pH values of packable giomer were significantly increased after 24 hours(p < 0.05). In contrast, in the powder type test, the pH values of packable and flowable giomers were dramatically increased within 30 minutes. The pH value of packable giomer, in particular, was higer than that of flowable giomer(p < 0.05). In the repeated neutralizing test, the degree of pH variation was lower than that of the previous neutralizing test(p < 0.05). Erosive changes on the surface of packable giomer were observed to be more than those on composite resin and flowable giomer as well. In conclusion, giomer has a acid neutralizing capacity, when it comes in contact with an acidic solution. Especially, packable giomer with high filler content has a greater acid neutralizing capacity than flowable giomer.

Evaluation of Resistance Spot Weldability of SGAFC1180 Steel (SGAFC1180 TRIP강재의 저항 점용접성 평가)

  • Shin, Seok-Woo;Lee, Jong-Hun;Kim, Dae-Hwan;Park, Sang-Heup
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.12
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    • pp.644-649
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    • 2017
  • In the automobile industry, there is growing demand for lightweight vehicles due to environmental problems and rising oil prices. Therefore, aluminum alloys and special materials are being used to reduce the weight of vehicles, but there are still many difficulties to overcome in terms of cost and strength. Therefore, the application of advanced high strength steel (AHSS)is increasing. AHSS has good strength and formability.Safety regulations are becoming stricter, and 1.2-GPa super-high-strength steels are gradually being applied for the center pillar and roof rails. Thus, the application of different kinds of steels in automobile bodiesis also increasing gradually. This study evaluates the resistance point weldability and the characteristics of a welded part of SGAFC1180 1.2t steel. A simulation was used to observe the nugget formation and its growth behavior. The prediction performance showed a similar tendency within an error rate of 10%. Also, the effect of this behavior on the process resistance and dynamic resistance was investigated,along with the correlation between the shear tensile strength and nugget diameter.

Effects of Cavity Configuration on Bond Strength and Microleakage of Composite Restoration (와동의 형태에 따른 복합레진의 결합강도 및 변연누출에 관한 연구)

  • Choi, Seung-Mo;Choi, Gi-Woon;Choi, Kyoung-Kyu;Park, Sang-Jin
    • Restorative Dentistry and Endodontics
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    • v.27 no.5
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    • pp.479-487
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    • 2002
  • 복합레진의 중합시 발생하는 수축과 응력은 와동의 형태에 의하여 영향을 받으며 이는 수복재는 물론 접착계면의 물성을 결정하는 요인이 된다. 본 연구는 다양한 C-factor를 갖는 와동에 상아질 접착제 Clearfil SE Bond(Kuraray)를 도포하고 혼합형 복합레진인 Clearfil AP-X(Kuraray)와 미세혼합형의 Esthet-X(Dentsply)를 충전하여 미세인장강도 및 변연누출을 측정 평가함으로써 중합수축이 수복물과 치아계면에 미치는 영향을 평가하고자 시행하였다. 98개의 Bovine 하악전치를 이용하여 표면의 상아질을 #600 SiC paper로 연마한 대조군 및 와동의 넓이를 조절하여 C-factor 2.3, 3.0, 3.7이 되도록 제작한 실험군 와동에 복합레진을 충전한 후 37의 증류수에 24시간 보관하였다. 저속 diamond saw(Buehler)를 이용하여 1mm 두께로 수직절단 후 고속 diamond point(#104 Shofu)를 이용하여 단면적 1mm$^2$가 되도록 hour-glass모양으로 형성하여 시편을 제작하였고, Universal testing machine(EZ-Test; Shimadzu, Japan)에 시편을 부착하고 cross head speed 1mm/min으로 인장력을 가하여 미세인장 결합강도를 측정하였다. 각 C-factor에 따른 변연누출실험을 위하여 복합레진이 수복된 치아를 37$^{\circ}C$의 증류수에 24시간 보관한 후 와동을 제외한 부위에 nail varnish를 도포하고 3mol/L silver nitrate용액에 24시간 암보관한 다음 수세하여 현상액에 24시간 경과시킨 후 치아의 장축에 따라 절단하여 침투된 색소의 정도를 광학현미경상에서 40배로 관찰하였다. 각각의 실험결과는 ANOVA/Tukey's test 및 Kruskal-Wallis non-parametric independent analysis와 Mann-Whitney U test에 의하여 통계 분석하여 다음과 같은 결론을 얻었다. 1. 대조군에 있어서 혼합형 복합레진의 미세인장 결합강도는 미세혼합형에 비하여 높았으며, 실험군 사이에는 유의차를 보이지 않았다. 2.모든 복합레진의 미세인장 결합강도는 와동의 C-factor증가에 따라 감소하는 경향을 나타내었고, 혼합형 복합레진의 실험군은 대조군에 비하여 낮게 나타났으며, 미세혼합형 복합레진에서는 유의차를 보이지 않았다. 3. 절단측 및 치은측 변연부의 미세누출정도는 혼합형 복합레진이 미세혼합형에 비하여 대체로 높게 나타났다. 4. 모든 실험군에서 미세누출은 C-factor증가에 따라 증가하였고 절단측에 비하여 치은측 변연이 높게 나타났으나 통계학적 유의차는 보이지 않았다. C-factor의 변화에 대하여 필러함량과 탄성계수가 높은 혼합형 복합레진이 미세혼합형에 비하여 더 민감한 결과를 보인다. 이는 복합레진 수복시 재료의 선택과 중합수축의 적절한 조절이 중요한 요소임을 시사한다.

Cell Patterning on Various Substrates Using Polyelectrolyte Multilayer and Microstructure of Poly(Ethylene Glycol) (다양한 기판 위에서 고분자 전해질 다층 막과 폴리에틸렌글리콜 미세 구조물을 이용한 세포 패터닝 방법)

  • Shim, Hyun-Woo;Lee, Ji-Hye;Choi, Ho-Suk;Lee, Chang-Soo
    • Korean Chemical Engineering Research
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    • v.46 no.6
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    • pp.1100-1106
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    • 2008
  • In this study, we presented rapid and simple fabrication method of functionalized surface on various substrates as a universal platform for the selective immobilization of cells. The functionalized surface was achieved by using deposition of polyelectrolyte such as poly(allyamine hydrochloride) (PAH), poly(diallyldimethyl ammonium chloride) (PDAC), poly(4-ammonium styrene sulfonic acid) (PSS), poly(acrylic acid) (PAA) and fabrication of poly(ethylene glycol) (PEG) microstructure through micro-molding in capillaries (MIMIC) technique on each glass, poly(methyl methacrylate) (PMMA), polystyrene (PS) and poly(dimethyl siloxane) (PDMS) substrate. The polyelectrolyte multilayer provides adhesion force via strong electrostatic attraction between cell and surface. On the other hand, PEG microstructures also lead to prevent non-specific binding of cells because of physical and biological barrier. The characteristic of each modified surface was examined by using static contact angle measurement. The modified surface onto several substrates provides appropriate environment for cellular adhesion, which is essential technology for cell patterning with high yield and viability in the micropatterning technology. The proposed method is reproducible, convenient and rapid. In addition, the fabrication process is environmentally friendly process due to the no use of harsh solvent. It can be applied to the fabrication of biological sensor, biomolecules patterning, microelectronics devices, screening system, and study of cell-surface interaction.

Preparation and characterization of poly(dimethylsiloxane) foam prepared by hydrogen condensation reaction (수소 축합 반응에 의한 폴리디메틸실록산 미세 발포체의 제조 및 물성분석 연구)

  • Lee, Soo;Moon, Sung Jin
    • Journal of the Korean Applied Science and Technology
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    • v.33 no.4
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    • pp.802-812
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    • 2016
  • Silicone foam is very useful as flame resistant material for many industrial areas such as high performance gasketing, thermal shielding, vibration mounts, and press pads. A silicone foam was prepared through simultaneous crosslinking and foaming by hydrogen condensation reaction of a vinyl-containing polysiloxane (V-silicone) and a hydroxyl-containing polysiloxane (OH-silicone) with hydride containing polysiloxane (H-silicone) in the presence of platinum catalyst and imorganic filler at room temperature. This is more convenient process for silicone foam manufacturing than the conventional separated crosslinking and foaming systems. Funtionalized silicones we used in this experiment were consisted with a V-silicone containing 1,0 meq/g of vinyl groups and a viscosity of 20 Pa-s, an OH-silicone with 0.4 meq/g of hydroxyl groups and a viscosity from 50 Pa-s, and an H-silicone containing 7.5 meq/g of hydride groups and a viscosity of 0.06 Pa.s. The effects of compositions of functionalized silicones and additives, such as catalyst and filler on the structure and mechanical properties of silicone foam were studied. 0.5 wt% of Pt catalyst was enough to accelerate the foaming rate of silicone resins. The addition of OH-silicone with lower viscosity accelerates the initial foaming rate and decreases the foam density, but the addition of V-silicone with lower viscosity reduces the tensile strength as well as the elongation. The final foam density, tensile strength, and elogation of silicone foam prepared under the SF-3 condition increase maximum to $0.58g/cm^3$, $3,51kg_f/cm^2$, and 176 %, repectively. We found out the filler alumina also played an important role to improve the mechanical properties of silicone foams in our foaming system.