• Title/Summary/Keyword: 표준오차

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X-ray Fluorescence Analysis of Chemical Ingredients for Portland Cement (X-선 형광분석법에 의한 포틀란드 시멘트의 정량분석)

  • 임헌진;백연봉;김도생;윤준수;이경원
    • Journal of the Korean Ceramic Society
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    • v.33 no.8
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    • pp.928-934
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    • 1996
  • Quantitative analysis each portland cement components was conducted by standard calibration method using X-ray fluorescence spectrometer. Standard sample and the unknown sample were prepared by fused cast bead method. In checking the errors of standard cement 227A372 the relative errors of constituents such as CaO, SiO2, Al2O3, Fe2O3, MgO and SrO were less than 1% and the relative errors of constituents such as So3, K2O, TiO2, Na2O P2O5, and Mn2O3 were less than 5% Sample preparation was mainly contributed to the errors. Compared with general wet chemical method the results of X-ray fluorescence analyses were more precise and accurate. Moreover it is possible to analyze precisely a little amount of the constituents such as SrO, Mn2O3 and P2O5 the analyses of which were very difficult using the wet chemical method.

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Systematic Error Correction of Sea Surveillance Radar using AtoN Information (항로표지 정보를 이용한 해상감시레이더의 시스템 오차 보정)

  • Kim, Byung-Doo;Kim, Do-Hyeung;Lee, Byung-Gil
    • Journal of Navigation and Port Research
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    • v.37 no.5
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    • pp.447-452
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    • 2013
  • Vessel traffic system uses multiple sea surveillance radars as a primary sensor to obtain maritime traffic information like as ship's position, speed, course. The systematic errors such as the range bias and the azimuth bias of the two-dimensional radar system can significantly degrade the accuracy of the radar image and target tracking information. Therefore, the systematic errors of the radar system should be corrected precisely in order to provide the accurate target information in the vessel traffic system. In this paper, it is proposed that the method compensates the range bias and the azimuth bias using AtoN information installed at VTS coverage. The radar measurement residual error model is derived from the standard error model of two-dimensional radar measurements and the position information of AtoN, and then the linear Kalman filter is designed for estimation of the systematic errors of the radar system. The proposed method is validated via Monte-Carlo runs. Also, the convergence characteristics of the designed filter and the accuracy of the systematic error estimates according to the number of AtoN information are analyzed.

A Residual Ionospheric Error Model for Single Frequency GNSS Users in the Korean Region (한국지역에서의 단일주파수 GNSS 사용자를 위한 전리층 잔류 오차 모델 개발)

  • Yoon, Moonseok;Ahn, Jongsun;Joo, Jung -Min
    • Journal of Advanced Navigation Technology
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    • v.25 no.3
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    • pp.194-202
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    • 2021
  • Ionosphere, one of the largest error sources, can pose potentially harmful threat to single-frequency GNSS (global navigation satellite system) user even after applying ionospheric corrections to their GNSS measurements. To quantitatively assess ionospheric impacts on the satellite navigation-based applications using simulation, the standard deviation of residual ionospheric errors is needed. Thus, in this paper, we determine conservative statistical quantity that covers typical residual ionospheric errors for nominal days. Extensive data-processing computes TEC (total electron content) estimates from GNSS measurements collected from the Korean reference station networks. We use Klobuchar model as a correction to calculate residual ionospheric errors from TEC (total electron content) estimate. Finally, an exponential delay model for residual ionospheric errors is presented as a function of local time and satellite elevation angle.

Development and validation of an analytical method for the determination of lepimectin residues by HPLC-PDA (HPLC-PDA를 이용한 lepimectin 잔류량 분석법 개발 및 확인)

  • Do, Jung-Ah;Kwon, Ji-Eun;Kim, Mi-Ra;Lee, Eun-Mi;Kuk, Ju-Hee;Kwon, Kisung;Oh, Jae-Ho
    • Analytical Science and Technology
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    • v.26 no.2
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    • pp.142-153
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    • 2013
  • A new, rapid, and simple analytical method was developed and validated using high performance liquid chromatograph-photodiode array detector (HPLC-PAD) for the determination of lepimectin residues in agricultural commodities. The lepimectin residues in samples were extracted with methanol, partitioned with dichloromethane, and then purified with glass column filled with subsequently to aminopropyl ($NH_2$) solid phase extraction (SPE) cartridge. The purified samples were detected using HPLC-PAD. Correlation coefficient ($R^2$) of both lepimectin $A_3$ and $A_4$ solutions were 0.9999. The method was validated using cucumber spiked with lepimectin at 0.02 and 0.2 mg/kg and pepper, mandarin, hulled rice, potato, soybean at 0.02 and 0.5 mg/kg. Average recoveries were 76.0~114.8% with relative standard deviation less than 10%, and limit of detection (LOD) and limit of quantification (LOQ) were 0.005 and 0.01 mg/kg, respectively. The result of recoveries and overall coefficient of variation of a laboratory results in Gwangju regional KFDA and Daejeon regional KFDA was followed with Codex guideline (CAC/GL 40). Therefore, developed method in this study is accurate, rapid, and appropriate for lepimectin determination and will be used to keep safety of lepimectin residues in agricultural products.

Development of OTF measurement system for evaluation of digital camera (디지털 카메라 평가용 OTF 측정 장치 개발)

  • Song, Jong-Sub;Lee, Yoon-Woo;Cho, Hyun-Mo;Cho, Jae-Heung;Jang, Soo;Park, Sang-Ki;Kim, Young-Jun;Min, Woon-Sik
    • Proceedings of the Optical Society of Korea Conference
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    • 2000.02a
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    • pp.202-203
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    • 2000
  • 광학 렌즈계의 성능 평가를 위한 OTF(Optical Transfer Function) 측정 방법은 Hopkins$^{(1)}$ 에 의해 기본 이론이 확립된 이래 세계 각국에서 활발하게 연구되어 왔으며, 가장 합리적이고 신뢰도가 높은 평가방법으로 인정되고 있다. OTF 측정 방법은 간섭계를 이용하는 측정 방법$^{(2)}$ 과 광학계에 의해 맺혀진 상을 주사 해석하는 방법$^{(3)}$ 으로 대별될 수 있으며, 세계적으로 20여가지 이상의 측정 장치가 개발되었다. 현재 세계 각국은 다양한 형태의 OTF 측정 장치를 보유하고 있으며, OTF의 정확도를 비교 검토하는 연구가 활발해져서 측정 표준을 확립하였고,$^{(4)}$ 국제적인 측정 비교 오차를 0.02 이하로 줄일 수 있게 되었다.$^{(5)}$ 특히 선진국에서는 측정 장치들 간의 상호 비교를 위해 표준 렌즈를 설계, 제작하였고, 이러한 표준 렌즈를 적절한 측정 조건하에서 측정 오차의 원인과 측정 정확도를 평가하는데 사용하였다. (중략)

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Absolute Measurement of the Quantum Efficiency of Photodetectors Using Correlated Photon Pairs (광자쌍을 이용한 광검출기의 양자효율 절대측정)

  • 안경진
    • Korean Journal of Optics and Photonics
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    • v.4 no.4
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    • pp.452-456
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    • 1993
  • The quantum efficiencies of photomultiplier tubes were measured by counting the coincidence photon pairs generated in the process of spontaneous parametric down-conversion. They were measured within 3% accuracy over the range of wavelength from 560 to 850 nm without any standard light source or detector. The values for 633 nm correspond to those obtained with a calibrated laser power meter within the measurement error.

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A Study on the proficiency test of pH measurements (pH 측정의 숙련도 시험에 대한 연구)

  • Lee, Hwashim;Kim, Myungsoo;Choi, Jongoh
    • Analytical Science and Technology
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    • v.14 no.3
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    • pp.230-237
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    • 2001
  • In general, the pH measurement follows calibration of glass electrode system using pH standard solution. When pH is measured at constant temperature, uncertainty factors are mainly related to the accuracy of pH standard solution and the accuracy and precision of glass electrode. Participants in this proficiency test were the volunteers trying to know the distribution of the measured pH values for the same sample and the sources of error through 1998 and 1999. The samples for proficiency test are phosphate salt standard solutions specially prepared in KRISS, of which pH values were 6.860, 7.415(at $25^{\circ}C$), and the stability test was performed for the same periods of proficiency test. The results of the proficiency test were plotted according to Youden plot, which shows whether the error is random or systematic. The results of Youden plot showed that the source of error was from the systematic effect of laboratories in each year. This shows that the source of error is the standard solutions used in laboratories.

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Evaluation and Selection of MEMS-Based Inertial Sensor to Implement Inertial Measurement Unit for a Small-Sized Vessel (소형 선박용 관성측정장치 개발을 위한 MEMS 기반 관성 센서의 평가와 선정)

  • Yim, Jeong-Bin
    • Journal of Navigation and Port Research
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    • v.35 no.10
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    • pp.785-791
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    • 2011
  • This paper describes the evaluation and selection of MEMS(Micro-Elect Mechanical System) based inertial sensor to fit to implement the Inertial Measurement Unit(IMU) for a small-sized vessel at sea. At first, the error model and the noise model of the inertial sensors are defined with Euler's equations and then, the inertial sensor evaluation is carried out with Allan Variance techniques and Monte Carlo simulation. As evaluation results for the five sensors, ADIS16405, SAR10Z, SAR100Grade100, LIS344ALH and ADXL103, the combination of gyroscope and accelerometer of ADIS16405 is shown minimum error having around 160 m/s standard deviation of velocity error and around 35 km standard deviation of position error after 600 seconds. Thus, we select the ADIS16405 inertial sensor as a MEMS-based inertial sensor to implement IMU and, the error reducing method is also considered with the search for reference papers.

Error Analysis of Trilateration Network by Confidence Ellipse (신뢰타원에 의한 삼변망의 오차해석)

  • 백은기;구재동
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.13 no.1
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    • pp.13-20
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    • 1995
  • Error analysis is important in horizontal positioning. In case of error analysis, standard error ellipse is generally used to establish the precision regions, but it will be replaced by 95% confidence ellipse. It is more effective than standard error ellipse in resection for measured procedures and establishment for criterias of relative error. Therefore, In this paper deals with analysis of application to 95% confidence ellipse in horizontal positioning. This study deals with error analysis of plane trilateration network which are various types of control point. also, this paper have studied for theory of error analysis in order to using least square adjustment. Thus, This paper's conclusion are as follows; 95% confidence ellipse could be used to establish of specification in korea, also, it is possible for us to predesign for optimum surveying network by 95% confidence ellipse.

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Compensation of Systematic Error of Various Schemes for Measuring Pumping Speed (진공펌프 배기속도 측정방식에 따른 구조적 오차 및 보정)

  • In, S.R.
    • Journal of the Korean Vacuum Society
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    • v.20 no.6
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    • pp.387-394
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    • 2011
  • Standard devices and procedures for measuring the pumping speed, one of the most important parameters indicating the operation performance of the vacuum pump, have been developed and widely utilized. Though the standard system has a firm theoretical basis, it is, sometimes, inevitable to alter something in the system for a practical purpose compared with ideal conditions, which may lead to a large measurement error. In this paper, characteristics and systematic errors of various ideal or practical schemes for measuring the pumping speed are analyzed, and compensation terms are proposed.