• Resources Recycling
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• v.19 no.5
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• pp.58-67
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• 2010

Platy silver powders with varied size and thickness were prepared by polyol process with $PdCl_2$ in ethylene glycol and characterized its properties and investigated the effects of reaction time, $NH_4OH$, PVP(poly-vinylpyrrolidone) and $PdCl_2$. The characteristics of the products were verified by scanning electron microscopy(SEM), high resolution transmitted electron microscopy(HR-TEM), X-ray diffraction(XRD) and particle size analyzer(PSA) and image analyzer. Platy silver powder was prepared about $5.5\;{\mu}m$ of size and $0.2\;{\mu}m$ at 120minute. It was found that the size of powders increased by the increasing of $NH_4OH$ and $PdCl_2$ concentrations, and the thickness of powders was decreased by increasing of PVP concentration.

• Applied Chemistry for Engineering
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• v.28 no.5
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• pp.587-592
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• 2017

Uniform and optimum sized silver nanoplates were synthesized through the liquid phase reduction method by using silver nitrate solution as a starting chemical, dimethylformmide (DMF) as a reducing solvent, and polyvinylpyrrolidone (PVP) as reducing and surfactant agents. Synthesized and also film samples were characterized by using SEM, TEM, UV-Vis-NIR spectroscopy, particle size analyzer (PSA), and XRD. Triangle nanoplates with the size of 100~200 nm were found from the sample synthesized at $70^{\circ}C$ for 72 h using silver nitrate, DMF and 26 wt% PVP. The sample could reflect near-infrared light because it showed the maximum absorbing peak at about 1,000 nm. When the content or particle size of silver nanoplates increased in coating solutions, the transmittance decreased and the reflectance increased in film samples.

• Journal of the Mineralogical Society of Korea
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• v.1 no.2
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• pp.117-130
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• 1988

The morphology of the Ca-montmorillonites from the Gampo area was investigated by the use of scanning and transmission electron microscope. These bulk samples show an irregular or rugged surface with well developed cavities and relict outline of original ash material at low magnification by SEM, indicating that montmorillonites are derived from volcanogenic material. Two different types of morphology of montmorillonites by SEM were observed which appear to depend very much on the space available for crystal growth. One is honeycomb structure montmorillonite growing in an open space. The other is the closely packed aggregates of intergrown montmorillonite showing platy particles where available space for the growth is limited. Several different habits of montmorillonite within a single sample can be observed by TEM. The dominant habit observed is the irregularly shaped and foliated aggregates and the platy shaped particles. In general, platy shaped particles are relatively abundant in the samples from Yongdongri compared with those from Jugjeonri area.

• Korean Journal of Ichthyology
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• v.10 no.2
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• pp.231-240
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• 1998

The characteristics of cranium, vertebral column and fin supports of Acanthorhodeus gracilis were examined. The fish did not have a fontanell in cranium nor process of supraethmoid. It had double orbitosphenoids and a basioccipital process developed from anterior portion of basioccipital. It had a high and triangular dorsal process on supraoccipital. In the urohyal, hypohyal attachment was bifurcated and horizontal and vertical plate were in an elongated rhombus shape with posterior edge pointed. It had teeth of 1-rowed, 5/5 and 4 free teeth. The fish did not have a coracoid foramen on shoulder girdle. It does not have a uroneural on ural centrum. It had a long and slender posterior process of pelvic bone. It had a large and flat supraneural. The fish had 14 or 15 interneural spines, of which the 1st, 2nd, 3rd and 4th had single basiosts and the rest had double basiosts. It had 11 or 12 interhemal spines, of which the 1st, 2nd, 3rd and 4th had single basiosts and the rest had double basiosts.

• Journal of the Korean Ceramic Society
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• v.38 no.8
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• pp.765-770
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• 2001

광촉매용 ZnO 나노크기의 분말은 시작원료와 연료의 종류에 따라 용액연소법에 의해 제조되었다. 결정상은 XRD로부터 확인할 수 있었으며 분말의 하소온도는 TG 분석으로부터 결정되었다. 분말의 비표면적은 BET 법에 의해 측정되었으며 평균입자크기와 형태를 SEM과 TEM으로부터 조사하였다. 또한 분말의 순도를 조사하기 위해 적외선 흡수스펙트럼을 측정하였으며 광촉매 효율로서 은이 첨가된 사진현상액을 이용하여 은의 수거율을 측정하였다. 용액연소법으로 제조한 경우 시작원료와 연료에 관계없이 단상의 ZnO 분말을 쉽게 얻을 수 있었다. 그러나 합성된 ZnO 분말의 입자크기와 형태는 연료의 종류에 따라 서로 다르게 보였다. 특히, 연료로 glycine을 사용한 경우, ZnO 분말의 입자 형태는 균일한 나노 크기의 구형이었으나 carbohydrazide을 사용한 경우에는 판상과 같은 형태를 보였다. 이러한 결과를 기초로 하여 시작원료와 연료로 Zn(OH)$_2$와 glycine을 사용하여 합성된 ZnO 분말이 우수한 분말 특성을 보였으며 75nm의 입자크기와 94$m^2$/g의 비표면적을 보였다. 또한 사진현상액에 존재하는 은이 3분 이내에 완전히 제거되는 우수한 광촉매 성질을 보였다.

• Journal of Korean Society of Forest Science
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• v.78 no.4
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• pp.396-400
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• 1989

The oxygen index test was carried out to obtain the relative flammability of wood-based materials (plywood, MDF, particleboard) and their oxygen indices. The oxygen index is the minimum concentration of oxygen, expressed as volume percent, in a mixture of oxygen and nitrogen that will just support flaming combustion of a material under the specified laboratory conditions. In this study the oxygen indices were calculated by using the Dixon and Massey's Up and Down method("N" Large method). The obtained results were as follows : 1. The oxygen indices calculated with Up and Down method were 27.9% for plywood, 26.9% for MDF, and 26.2% for particleboard, indicative of plywood being more difficult to burn than MDF and particleboard Lender the same surrounding conditions. 2. The oxygen indices were not affected by the total gas flow rate.

• Economic and Environmental Geology
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• v.41 no.5
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• pp.587-595
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• 2008

The geology of the Capim region in Brazil is composed of Ipixua Formation in Mesozoic-Tertiary(Miocene), sedimentary rocks in Miocene, Barreiras Formation(sedimentary rocks) in Pleistocene and sediments in Holocene. Kaolin deposit consists of Barreiras Formation(average depth in 120m) composed of sandstone, clay, fine sand of Miocene to Pliocene age. Kaolin of the high grade is white in color and its thickness averages 7m. The orebody formed by kaolinite was confirmed by XRD, is shape of hexagonal, SK is above 33 degree. It is class A also suit for producing a paper without filtration. According to the CPRM report, the reservation of kaolin ore is amounts of 566,819,164 tons.

• Korean Institute of Interior Design Journal
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• v.16 no.5
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• pp.98-106
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• 2007

With the recent increase in the amount of interior materials, the medium-density fiberboard(MDF) has continued to be produced at an increasing rate. Accordingly, to prevent the deformation of MDF after its construction, secure the precision of its finishing and improve the performance of its design, this study attempted to investigate the effect of environment humidity conditions on flatness according to the field used in MDF and its relationship to other physical properties. An attempt was made to conduct this study by changing the conditions of surface treatment by moisture and by thickness. For this purpose, it is judged that it is desirable to prevent scheme to maintain the flatness by defining the coefficient of water absorption-induced length change as in the regulation on low-density soft fiberboard and adjusting the standard for wet bending strength upward. It is thought that is further studies will be conducted about the effect of material, adhesive and thermal pressure condition, production system and processing method used in MDF on its scheme to maintain the flatness and changes in length and thickness expansion.

• Proceedings of the Korean Vacuum Society Conference
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• 2011.02a
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• pp.461-461
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• 2011

최근의 나노기술의 발전과 함께 나노미터크기의 물질들의 물성과 미세구조 등을 분석하기 위한 노력들이 활발히 이루어지고 있다. 투과전자현미경(transmission electron microscope; TEM)은 나노물질의 미세구조 관찰, 화학성분 분석, 전자기적 특성평가가 가능한 초정밀 분석장비이다. TEM 관찰을 위한 시편의 제작방법중 TEM 그리드(grid)를 사용하는 방법은, 분석하고자 하는 물질을 망(mesh) 형태의 그리드에 도포하여 샘플을 준비하는 방법으로 다른 방법에 비해 아주 빠르고 간편한 장점이 있다. 그러나 TEM 그리드에 나노물질을 분산/도포하여 공중에 떠있는 형태로 샘플을 제작하려면, 나노물질이 mesh 사이로 빠져나오지 않도록 그리드 mesh의 간격이 아주 미세하여야 하는데, 일반적으로 mesh의 크기가 미세할수록 그리드의 가격은 높아진다. 또한 기존에 사용되고 있는 비정질 탄소박막으로 덮여진 그리드는 극미세 크기의 나노물질 및 탄소나노물질을 분석할 경우, 고해상도의 TEM상을 얻는데 한계가 있다. 한편 그래핀은 2차원의 육각판상의 구조로 탄소원자가 빼곡히 채워진 흑연 한 층의 나노재료이다. 이는 원자단위 두께로 가장 얇은 물질로서 기계적 강도가 우수하여 지지막으로의 응용이 가능하다고 알려져 있다. 따라서 TEM grid막으로 사용할 경우 기존의 고가의 미세한 mesh가 형성된 그리드를 사용하지 않아도 나노물질을 효과적으로 분석할 수 있을 것으로 예상 된다. 본 연구에서는 열화학증기증착법(thermal chemical vapor deposition; TCVD)을 이용하여 300 nm 두께의 니켈박막이 증착된 기판위에 대면적으로 합성한 그래핀을 TEM 관찰용 그리드 위에 전사(transfer)함으로써 나노물질이 그리드 mesh사이로 빠져나오지 않는 저가의 TEM 그리드 제작 방법 및 응용 가능성에 대하여 보고한다.

• Korean Journal of Ichthyology
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• v.9 no.1
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• pp.130-140
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• 1997

The osteological features of Rhodeus uyekii were examined. In this study, the detailed descriptions of cranium, vertebra and fin skeleton of Rhodeus uyekii are presented. R. uyekii had the following characteristics ; there was no fontanell in the cranium ; there was no process of supraethmoid ; the free interneural spine was large and flat ; the dorsal process of the supraoccipital was high and triangular ; the fourth infraorbital was reduced ; in the urohyal, the hypohyal attachment is bifurcated, the horizontal and vertical plate has a elongated rhombus shape with posterior edge pointed ; there was no coracoid foramen in the shoulder girdle ; there was no uroneural in the first preural centrum.