• Korean Journal of Materials Research
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• v.7 no.7
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• pp.623-631
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• 1997

본 연구에서는 주조 2상 스테인리스강의열시효에 대한 시효온도, 시효시간 및 Nb함유량의 영향을 관찰하기 위해 기계적 성질 및 조직을 조사하였으며 Nb을 함유한 주조 2상 스테인리스강의 파괴기구를 규명하기 위해 SEM에 의한 파단면 관찰과 WDS성분분석을 통해 파괴기구의 특성을 고찰하였다. 시효온도와 시효시간이 증가함에 따라 페라니트으 미소경도가 증가하였으며 항복강도의 경우 시효온도와 시효시간에는 영향을 받지 않았으나 Nb을 함유한 재료들이 Nb을 함유치 않은 재료들에 비해 다소 낮은 항복강도 값을 보였다. 충격흡수에너지 값은 시효시간 및 시효온도의 증가에 따라 시험된 모든 재료에서 저하되었는데 0.4% Nb을 함유하는 경우 Nb을 약간 함유하거나 함유치 않은 재료들에 비해 시효시간에 따라 급격한 감소 경향을 보였다. 파단면 관찰결과 페라이트 기지 또는 페라이트/오스테나이트 상경계에서 석출된 VbC를 비롯한 탄화물들이 취성저항성을 낮추는데 크게 기여했음을 알 수 있었다.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2013.05a
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• pp.87-87
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• 2013

복합조직강의 미세조직제어를 통한 자동차용 고강도 강판재의 개발이 주요 연구과제로 있다. 하지만 고강도화에 따라 수소에 의한 지연파괴의 문제점이 있어, 이를 규명하고 해결하기 위한 많은 연구가 함께 이루어지고 있다. 본 연구에서는 연구, 개발되고 있는 복합조직강 중 DP강과 TRIP강의 수소취성에 미치는 미세조직의 영향을 분석하고, 수소주입조건에 따른 수소취성 및 지연파괴 거동에 대하여 조사하고자 하였다. 이를 위해 음극전기분해법을 이용, 주입수소량을 달리하여 주입수소가 복합조직강의 지연파괴에 미치는 영향을 분석하였다. Hydrogen determinator를 통해 시편 내 수소량을 측정하였고, 소형펀치시험에 의한 기계적물성 변화를 조사하였다. 또한 파단부위의 넓이와 깊이를 비교측정하였고, 파단면을 SEM으로 관찰하여 수소지연파괴 거동을 평가하고자 하였다.

• Journal of Korean Ophthalmic Optics Society
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• v.13 no.4
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• pp.89-94
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• 2008

Purpose: To observe the high temperature creep test and the fracture surface of the samples of 9% Ni alloy steel generally used for all kinds of mahine parts and predict the durability of that by determining a constant of C with a Larson-Miller variable. Methods: The equipment of this test was made into lever-beam style designed by Andrade and F. Garofalo et al.. The condition of creep test was set under 16 kinds of conditions after fixing 4 kinds of temperature condition and 4 kinds of stress condition to check how it effects the samples. Results: The temperature of creep test was increased, the stress index (n) of creep deformation was gradually decreased from 3.97 to 3.55. The activation energy of creep deformation was decreased from 90.39 to 83.64 kcal/mol when the stress was increased. A constant of C value by calculation of larson-Miller variable was about 22 and if temperature for use is suggested, the durability could be calculated. Conclusions: By analyzing the fracture phenomenon and suggesting the observation result of the fracture surface of the samples and creep test of 9% Ni alloy steel, the basic design data for the practical use of accessories in the field of equipment could be constructed and used to predict the durability of the equipment.

• Tunnel and Underground Space
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• v.19 no.2
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• pp.158-166
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• 2009

As a basic study for investigating the development of the stress-induced crack in Hoek-Brown rock, a homogenization technique of elastic cracks is proposed. The onset of crack is monitored by Hoek-Brown empirical criterion, while the orientation of the crack is determined by the critical plane approach. The concept of volume averaging in stress and strain component was invoked to homogenize the representative rock volume which consists of intact rock and cracks. The formulation results in the constitutive relations for the homogenized equivalent anisotropic material. The homogenization model was implemented in the standard FEM code COSMOSM. The numerical uniaxial tests were performed under plane strain condition to check the validity of the propose numerical model. The effect of friction between the loading plate and the rock sample on the mode of deformation and fracturing was examined by assuming two different contact conditions. The numerical simulation revealed that the homogenized model is able to capture the salient features of deformation and fracturing which are observed commonly in the uniaxial compression test.

• Proceedings of the KSME Conference
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• 2007.05a
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• pp.268-273
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• 2007

As the industrial society develops rapidly, the weight reduction and high strength are gradually demanded. In case of the welded joint for the rolling stock which receives the repeated load, the fracture can be easily occurred. However, the durability and fatigue characteristics can be improved if the shot peening technique is applied. The optimal peening process should be applied to the metal surface because the over peening can lower the durability of parts. Thus, the fatigue characteristics and Fractography of welded A6061-T6 alloy for a rolling stock were studied in the paper. The optimal peening condition and Fractography were examined. The experimental result show that over peening can lower fatigue life caused by micro crack, fold and incrustation. The fatigue life of welded A6061-T6 was tremendously improved.

• Analytical Science and Technology
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• v.5 no.2
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• pp.203-211
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• 1992

Fracture behavior and martensite substructure of Ni-36.5at.%Al alloy were investigated with the addition of vanadium which is known as scavenging element of grain boundary. The fracture surfaces were examined by scanning electron microscopy and the EDX spectrometer was applied for composition analysis of fracture surfaces. The substructure of martensite was studied by transmission electron microscopy. By addition of vanadium, fracture surfaces show mixed modes of intergranular and transgranular fracture and more Al content is found on the grain boundaries. For Ni-36.5at.%Al alloy, the planar faults observed in the martensite plates are the internal twins. By increasing the vanadium content, the modulated structure with stacking faults and dislocations dominates while the twinned martensite disappears. The stacking fault is determined to be extrinsic due to the substitution of V for Al. It is concluded that the segregation of sulfur on the high-energy state stacking fault area suppresses the intergranular fracture.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.38 no.9
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• pp.1043-1048
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• 2014

As micro screws feature reduced screw lengths and pitches, the resulting clamping force diminishes because of the reduced length of the actual joints. The elements of the clamping force are material, geometry, and friction. We studied the shrinking size of the screw and the methods to improve the clamping force by changing the material. We developed a micro screw using SWCH18A and SUS XM7 materials, and obtained the precision and thickness of the pitch through three-dimensional measurement. We also measured the external resistance of the micro screw by applying the Vicker's hardness test and conducted a break surface analysis using a break torque test and SEM for obtaining the break characteristics.

• Analytical Science and Technology
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• v.17 no.4
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• pp.355-362
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• 2004

Fission products and Inter reaction layer of $U_3Si-Al$ dispersion fuel, irradiated in HANARO research reactor with 121 kW/m of maximum liner power and 63 at% of average burn-up, was characterization by EPMA (Electron Probe Micro Analyzer). The fuel punching system developed by Irradiated Materials Examination Facility (IMEF) has used to make these samples for the EPMA. With this system a very small and thin specimen which is 1.57 mm in diameter and 2 mm in thickness respectively has been fabricated to protect the EPMA operator from high radioactive fuel and to mini-mize the equivalent dose rate less than 150 mSv/h. EPMA was performed to observe layers of sectional, Inter-reaction and oxide with specimens of cutting and polished. Stoichiometry in the Inter-reaction layer with $16{\mu}m$ of thickness was $U_{2.84}$ Si $Al_{14}$ with calibration of $UO_2$ and $U_{3.24}$ Si $Al_{14.1}$ with calibration of standard specimen. metallic precipitates in this layer were not observed using fission products examination.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.39 no.11
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• pp.1091-1097
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• 2015

Graphite material has been widely used for making the rocket nozzle throat because of its excellent thermal properties. However, when compared with typical structural materials, graphite is relatively weak with respect to both strength and toughness, owing to its quasi-brittle behavior, and gets oxidized at $450^{\circ}C$. Therefore, it is important to evaluate the thermal and mechanical properties of this material for using it in structural applications. This study presents an experimental method to investigate the fracture behavior of ATJ graphite at elevated temperatures. In particular, the effects of major parameters such as temperature, loading, and oxidation conditions on strength and fracture characteristics were investigated. Uniaxial compression and tension tests were conducted in accordance with the ASTM standard at room temperature, $500^{\circ}C$, and $1,000^{\circ}C$. Fractography analysis of the fractured specimens was carried out using an SEM.

• Journal of the Korean Society of Propulsion Engineers
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• v.7 no.4
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• pp.73-79
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• 2003

The tensile strength test and the analysis for the section of brazing were performed in the cases of materials used for combustion chamber of regeneratively cooled liquid rocket engine. BNi-2 and BNi-7 based on nickel were used for brazing as filler metal. The properties of material and filler metal were analyzed by tensile strength test and metal microscope for 12 specimens. The tensile-strength of brazing for chrome-copper alloy and other kinds of alloy was higher than that of chrome-zirconium-copper alloy and other kinds of alloy The tensile strength in the case of BNi-2 as filler metal was higher than that of BNi-7 because the wetting property of BNi-2 was better than that of BNi-7.