• Polymer(Korea)
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• v.37 no.1
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• pp.47-51
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• 2013

In this work, the effect of alumina nanofibers on thermal conductivity and fracture toughness of alumina nanofibers and powder filled epoxy (EP) composites were investigated with varying alumina nanofiber content from 20 to 100 phr. Thermal conductivity was tested using a laser flash analysis (LFA). The fracture toughness of the composites were studied through the critical stress intensity factor ($K_{IC}$) measurement. The mophologies were observed by scanning electron microscopy (SEM). From the results, it was found that the thermal conductivity was enhanced with increasing alumina nanofiber content, which played a key factor to determine the thermal conductivity. The $K_{IC}$ value was increased with increasing alumina nanofiber content, whereas the value decreased above 40 phr alumina nanofiber content. This was probably considered that the alumina nanofiber entangled each other in EP due to an excess of alumina nanofibers.

• Restorative Dentistry and Endodontics
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• v.32 no.3
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• pp.208-221
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• 2007

The fracture toughness test is believed as a clinically relevant method for assessing the fracture resistance of the dentinal restoratives. The objectives of this study were to measure the fracture toughness $(K_{1C})$ and microtensile bond strength of dentin-resin composite interface and compare their relationship for their use in evaluation of the integrity of the dentin-resin bond. A minimum of six short-rod specimens for fracture toughness test and fifteen specimens for microtensile bond strength test was fabricated for each group of materials used. After all specimens storing for 24 hours in distilled water at $37^{\circ}C$, they were tensile-loaded with an EZ tester universal testing machin. Statistical analysis was performed using ANOVA and Tukey's test at the 95% confidence level, Pearson's coefficient was used to verify the correlation between the mean of fracture toughness and microtensile bond strength. FE-SEM was employed on fractured surface to describe the crack propagation. Fracture toughness value of Clearfil SE Bond (SE) was the highest, followed by Adper Single Bond 2 (SB), OptiBond Solo (OB), ONE-STEP PLUS (0S), ScotchBond Multi-purpose (SM) and there was significant difference between SE and other 4 groups (p < 0.05). There were, however, no significant difference among SB, OB, OS, SM (p > 0.05). Microtensile bond strength of SE was the highest, followed by SB, OB, SM, OS and OS only showed significant lower value (p < 0.05). There was no correlation between fracture toughness and microtensile bond strength values. FE-SEM examination revealed that dentin bonding agent showed different film thickness and different failure pattern according to the film thickness. From the limited results of this study, it was noted that there was statistically no correlation between K1C and ${\mu}TBS$. We can conclude that for obtaining the reliability of bond strength test of dentin bonding agent, we must pay more attention to the test procedure and its profound scrutiny.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 1995.05a
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• pp.127-138
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• 1995

대형 복합재 연소관 금속 보스용 고강도 알루미늄 합금 7175-T74를 개발하기 위하여, 고순도 7175 합금을 이용하여 링롤 단조법으로 대형링을 제조하였으며, 열처리와 가공 조건을 정밀제어한 특수공정을 적용하여 기존의 재료와 재질 특성을 비교 분석하였다. 분석결과 특수공정의 7175S-T74는 기존의 7175-T74 및 7075-T73에 비해 2차상 입자의 분률이 작고, 동일한 SCC특성(38% IACS) 수준에서 강도와 파괴인성이 동시에 증가한 이상적인 강도-인성-SCC 조합특성을 가졌다. 이는 특수공정에서의 고온열처리에 의한 2차상 입자의 재고용과 그에 따른 석출량 증가 때문이며, 결국 7175 합금, 링롤단조 그리고 T74 특수공정을 조합 적용하면 구조적 신뢰성과 경제성 면에서 유리한 보스용 대형링을 개발할 수 있다.

• Journal of the Korean Institute of Gas
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• v.2 no.1
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• pp.7-13
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• 1998

In this study, for the safety performance of LNG storage tank, the fracture toughness in X-grooved weld HAZ(heat-affected zone) of $9\%$ Ni steel was evaluated qualitatively and quantitatively, and the relation with the change in microstructure was analyzed. The toughness assessment was peformed through the modified CTOD test proposed for thick weldment with X-groove. Additionally, microstructures of HAZ were evaluated by OM, SEM and XRD. From the results, HAZ toughness of SMA(shielded metal arc)-welded $9\%$ Ni steel decreased as the evaluated region approached the fusion line. The decrease in toughness was apparently caused by the increase in the fraction of coarse-grained zone within HAZ. On the other hand, toughness drop with decreasing test temperature in F.L.(fusion line) ${\~}$F.L.+3mm was larger than that in F.L.+5mm${\~}$F.L.+7mm region due to the fact that in the former regions, retained austenite had poor stability.

• Korean Journal of Materials Research
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• v.2 no.5
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• pp.330-336
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• 1992

Four distinctive hot pressed and heat treated S${i_3}{N_4}$ceramics, S${i_3}{N_4}$-8%${Y_2}{O_3}$, S${i_3}{N_4}$-6% ${Y_2}{O_3}$-2% $A{l_2}{O_3}$, S${i_3}{N_4}$-4% ${Y_2}{O_3}$-3% $A{l_2}{O_3}$, 그리고 S${i_3}{N_4}$-1% MgO-1% Si$O_2$(in wt%), were prepared and characterized by X-ray diffraction, scanning electron microscopy, image analysis and mechanical tests. The fracture toughness of S${i_3}{N_4}$-8% ${Y_2}{O_3}$specimens containing large elongated grains showed the highest value of about 9.8MPa$m^{1/2}$. Two out of four S${i_3}{N_4}$, ceramics(S${i_3}{N_4}$-6% ${Y_2}{O_3}$-2% $A{l_2}{O_3}$and S${i_3}{N_4}$-4% ${Y_2}{O_3}$-3% $A{l_2}{O_3}$) heat treated at 200 $0^{\circ}C$retained the fracture strength of over 900MPa and fracture toughness of over 8.0MPa$m^{1/2}$. Large ${\beta}$-S${i_3}{N_4}$grains having a diameter larger than 1${\mu}$m appeared to contribute to increase in fracture toughness.

• Composites Research
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• v.16 no.4
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• pp.44-50
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• 2003

The damage zone around a crack tip occurring before the fracture is a significant domain. which affects the toughening mechanism of materials. In this study. the growth process of damage zone in the vicinity of crack tip for rubber-modified epoxy resin is investigated using an acoustic emission(AE) analysis. The weight fractions of rubber(CTBN 1300$\times$B) in rubber-modified epoxy resin are 5 wt% and 15 wt%. The fracture toughness($K_{IC}$) and the fracture energy($G_{IC}$) were measured using 3 point bending single-edge notched specimens. The damage zone and rubber particles distributed around the crack tip were observed by a polarized optical microscope and an atomic force microscope(AFM). The damage zone around crack tip of rubber-modified epoxy resin was formed at 13 % loading and developed until 57 % loading of the fracture load. The crack initiated at 57 % loading grew repeatedly in the stick-slip propagation behavior. Based on time-frequency analysis, it was confirmed that AE signals with frequency bands of 0.15~0.20 MHz and 0.20~0.30 MHz were generated from cavitation and stable/unstable cracking inside the damage zone.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.14 no.6
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• pp.1319-1327
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• 1994

Since fatigue cracks in rail can be the source of fractures and subsequent derailments, quantitative evaluation of the fatigue behavior and fracture properities due to the analysis results of laboratory test are drawn on the basis for predicting fatigue life and making a decision of safe inspection interval. Charpy V-notch and fracture toughness behavior were evaluated from the results of Charpy impact test. Fatigue test was performed by using CT type specimen under constant amplitude loading, and finally the effects of the following parameters; crack orientation, temperature, and stress ratio, on the fatigue crack growth behavior were studied.

• Journal of Navigation and Port Research
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• v.26 no.4
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• pp.435-440
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• 2002

The quantitative assessment of the effect of the residual stress on fracture behavior was executed by some experiment and numerical analysis. First of all, artificial residual stresses were imposed on CT(Compact Tension) specimens by local heating using gas torch, and an appropriate distribution of residual stresses was obtained by thermal elastic-plastic FE analysis. To certify the result of the FE analysis, an experimental measurement was performed in accordance with ASTM standard. Fracture toughness test was executed on the several types of specimens. The first type was the specimen without residual stresses, and the others had different peak value of compressive residual stress at crack front via controlling the heat flux. All the test results were presented on th J resistance(JR) curves and discussed to verify the effect of compressive residual stresses on fracture behavior.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.12 no.4
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• pp.95-106
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• 1992

This paper presents a comparative evaluation of five different types of steel fibers used as reinforcing material in concrete beams. Two types of plain and RC beams were prepared to compare the relative flexural behavior. The fibers used were dog bone (paddled), both ends hooked. コ-type straight. crimped and wavy type with aspect ratio of 43 to 75. Fiber volume fraction of 1 to 2% were used while shear span to depth ratio (aid) and steel ratio p were fixed. Fiber reinforcement effect index Ef and effective toughness index Te were adopted to evaluate fiber reinforcing effects. The effect of fiber reinforcement on flexural strength is higher in plain beams than in RC beams. Hooked and dog bone type fibers were found to be more effective than the other type ones in enhancing the flexural strength and post-peak energy absorption capacity of concrete beams.

• Tunnel and Underground Space
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• v.31 no.6
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• pp.415-427
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• 2021

This technical report briefly introduced the rock cutting splitting method under development. This method is a method of excavating the rock by splitting the block after the rock cutting process. After designing the cutting geometry of the rock face, the chisel is press-fitted to remove the rock block. At this time, when the cutting block is properly designed, the tensile crack propagates smoothly at the bottom of the rock block. An analytical solution was devised to estimate the indentation force required for splitting rock blocks using fracture toughness mode 1 required for tensile crack growth. The impact force of the hydraulic breaker of the excavator was analyzed, and the grade of the excavator that can be constructed according to the rock block design geometry was analyzed.