• Title/Summary/Keyword: 측정 불확도

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Uncertainty improvement in measurement of mean diameter of 0.3-$\mu\textrm{m}$-diameter polystyrene sphere by using quasi-elastic light scattering (준탄성광산란을 이용한 0.3 $\mu\textrm{m}$ 폴리스티렌구의 평균지름 측정 불확도 향상)

  • 박병천;정명세
    • Korean Journal of Optics and Photonics
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    • v.9 no.4
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    • pp.258-263
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    • 1998
  • Quasi-elastic light scattering is utilized to measure the mean diameter of the 0.3 $\mu\textrm{m}$-dimeter polystyrene sphere. The mean diameter of the polystyrene sphere is required to be known within the uncertainty of a few per centages. The systematic error has been considerably reduced by improving the system for the angle alignment and temperature measurement of cell. NIST SRM 1691 (0.269$\pm$0.007 $\mu\textrm{m}$: TEM; 0.275$\pm$0.007 $\mu\textrm{m}$: QELS) is measured to be 0.273 $\mu\textrm{m}$$\pm$0.006 $\mu\textrm{m}$ in mean diameter. Detailed description is given of the improved method and the resultant uncertainty, and the comparison of results with NIST is followed.

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Uncertainty Analysis of the Calculated Radioactivity in Liquid Effluent Released as Batch Mode from a Nuclear Power Plant (발전용원자로에서 뱃치방식으로 배출되는 액체상 방사성물질의 방사능 평가결과에 대한 불확도 해석)

  • 정재학;박원재
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2003.11a
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    • pp.562-571
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    • 2003
  • A series of factors such as sampling, pretreatment measurement, volume estimation which induces uncertainty of the calculated radioactivity in liquid effluent released from a nuclear power plant were analyzed. It is innately impossible to estimate exact error of the calculated radioactivity, since most of the input parameters are determined by a single measurement and true value of the released radioactivity cannot be known. In this paper, a systematic model to calculate uncertainty of the released liquid radioactivity was developed based upon the guidance report published by the ISO in 1993, and the model was applied to a set of hypothetical batch release conditions. As a result, the Priority of each input parameter was turned out to be (1) wastewater volume, (2) sample volume, and (3) measured radioactivity of the sample. In addition, probability distribution of the released radioactivity was simulated by Monte Carlo method combining the probability distribution of each input parameter It was shown that the radioactivity released to the environment, which has been reported as a single value, has a certain form of probability distribution.

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Uncertainty evaluation of the analysis of 11-nor-9-carboxy-Δ9-tetrahydrocannabinol in hair by GC-NCI-MS/MS (GC-NCI-MS/MS를 이용한 모발 중 대마 대사체 분석의 측정불확도 평가)

  • Kim, Jin-Young;Lee, Jae-Il;Cheong, Jae-Chul;Suh, Yong-Jun;In, Moon-Kyo
    • Analytical Science and Technology
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    • v.24 no.1
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    • pp.1-9
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    • 2011
  • We described an estimation of measurement uncertainty in quantitative analysis of 11-nor-9-carboxy-${\Delta}^9$-tetrahydrocannabinol (THC-COOH), the metabolite of ${\Delta}^9$-tetrahydrocannabinol, in hair samples by using the bead-assisted liquid-liquid extraction and gas chromatography-tandem mass spectrometric (GC-NCI-MS/MS) detection. Traceability of measurement was established through the use of reference materials, calibrated volumetric tubes, volume measuring devices, and measuring instruments. The analytical results were compared and the different contributions to the uncertainty were evaluated. Inter-day variation was performed by using statistical analysis of several indicative factors. Measurement uncertainty associated with the analyte in real forensic hair samples were estimated using QC data. The major factor of contribution to combined standard uncertainty was inter-day repeatability, while those associated with preparation of analytical standard and also sample of weight were insignificant considering the degree of contribution. Relative uncertainty of relative extended standard uncertainty divided into the measured concentration of the analyte was 17% in a hair sample. The uncertainty of result evaluation will be invaluable to improve quality of the analysis.

Lateral Cephalometric Measurements of Class I Malocclusion Patients with Uncertainty (불확도를 고려한 Class I 부정교합 환자의 측방두부방사선영상 계측값)

  • Lee, Ji Min;Song, Ji-Soo;Hyun, Hong-Keun;Kim, Young-Jae;Kim, Jung-Wook;Jang, Ki-Taeg;Lee, Sang-Hoon;Kim, Hojae;Cho, Hyo-Min;Shin, Teo Jeon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.45 no.1
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    • pp.65-74
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    • 2018
  • The aim of this study was to obtain the traceability of the software used to analyze lateral cephalometry and to calculate the uncertainty of the measurements. Furthermore, this study aimed to provide a basis for obtaining standard references for measurement values for orthodontic treatment in children. Cephalometric data were collected from 100 children diagnosed with class I malocclusion between the ages 6 to 13 years who visited the pediatric dentist at Seoul National University Dental Hospital. To ensure traceability, a phantom device was created. Correction values were calculated by measuring the length and angle of the phantom device using the software. Type A uncertainty was calculated by obtaining the standard deviation of cephalometric measurements of 100 persons and the standard error of repeated measurements. Determination of the type B uncertainty was induced by minimum resolution and the position of the head. Using these, the combined standard uncertainty was obtained and the expanded uncertainty was calculated. The results of this study confirm that the currently used software has high accuracy and reliability. Furthermore, the uncertainty of orthodontic measurements in Korean children aged 6 to 13 years was calculated, and distribution range for class I malocclusion with 95% confidence interval was suggested.

A Study on the Effects of Cross-sectional Dimension Change of Brake Pad Specimen on the Uncertainty of the Compressive Strength (제동 패드의 압축강도시편의 단면치수변화가 압축강도 불확도에 미치는 영향 분석)

  • Park, Soo Hong;Park, Jin Kyu;Kim, Si Wan;Park, Chan Kyoung
    • Journal of the Korean Society for Railway
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    • v.17 no.4
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    • pp.223-227
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    • 2014
  • The brake pad is one of the basic brake elements of a railway vehicle. It accomplishes braking action by friction between a pad and a brake disc. Because the brake pad must endure specified high pressure, the compressive strength is managed as the main performance factor. The standards for measuring the compressive strength of brake pads are KRS, KRCS, and KRT. These standards specify the size of the test piece for measuring compressive strength as $20mm{\times}10mm{\times}15mm$ ($W{\times}D{\times}H$). To reduce the uncertainty of the compressive strength, factors of uncertainty were analyzed. The results show that changing the dimensions of the cross section was useful to reduce the uncertainty. The uncertainty due to the new cross-sectional dimension shows the effectiveness of reducing uncertainty.

Measurement uncertainty for QC/QA applied to the chemical analysis (화학 분석 결과의 QA/QC를 위한 측정 불확도)

  • Woo, Jin-Chun;Oh, Sang-Hyub;Kim, Byoung-Moon;Bae, Hyun-Kil;Kim, Kwang-Sub;Kim, Young-Doo
    • Analytical Science and Technology
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    • v.18 no.6
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    • pp.475-482
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    • 2005
  • The expression of uncertainty applied to the chemical analysis is highly recommended with increasing demands upon the systematic quality assurance and control(QA/QC) with ISO 17025. For the quantification of quality source, 7 major common sources of uncertainty, normally contributing to the quality of the chemical analysis, were selected from QA/QC literatures of chemical analysis. They were classified into repeatability, drift, uncertainty in standards, linearity of calibration, homogeneity, stability of sample, and matrix effect. And, the quantification of the sources by means of measurement uncertainty was proposed as a prerequisite steps for QA/QC. Examples applied to the quantification procedures of modelling, combination and expression of standard uncertainty for the 7 major common sources were presented as a reference guide for QA/QC in chemical analysis.

Estimation of Uncertainty in Critical Flow Function for Natural Gas (천연가스의 임계유동함수 불확도 평가)

  • Ha, Young-Cheol
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.38 no.7
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    • pp.625-638
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    • 2014
  • In this study, the uncertainties in the critical flow functions (CFFs) calculated by the AGA8-dc equation of state were estimated. To this end, the formulas for enthalpy, entropy, and speed of sound, which are used in calculating the CFF, were expressed in the form of dimensionless Helmholtz free energy and its derivatives, and the uncertainty in Helmholtz free energy was inferred. To consider the variations in the compressibility-dependent variables induced by the variation (i.e., uncertainty) in compressibility, the form of the AGA8-dc equation was modified to have a deviation equal to the uncertainty under each flow condition. For each independent uncertainty component of the CFF, a model for uncertainty contribution was developed. All these changes were applied to GASSOLVER, which is KOGAS's thermodynamic database. As a result, the uncertainties in the CFF were estimated to be 0.025, 0.055, and 0.112 % at 10, 50, and 100 bar, respectively, and are seen to increase with the increase in pressure. Furthermore, these results could explain the deviations in the CFFs across the different labs in which the CFF international comparison test was conducted under the ISO management in 1999.