• Title/Summary/Keyword: 최적입도

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Preparation of Seaweed Calcium Microparticles by Wet-grinding Process and their Particle Size Distribution Analysis (초미세습식분쇄공정의 공정변수에 따른 해조칼슘의 입자크기 분석)

  • Han, Min-Woo;Youn, Kwang-Sup
    • Food Engineering Progress
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    • v.13 no.4
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    • pp.269-274
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    • 2009
  • The main objective of this study was to establish optimum condition of wet grinding process for manufacturing microparticulated seaweed calcium. Process parameters such as concentration of forming agent, rotor speed, bead size, feed rate, and grinding time were adapted during wet-grinding of seaweed calcium. The particle size range of the raw seaweed calcium was 10-20 $\mu$m. The calcium particles were reduced to under 1 $\mu$m as nano scale after grinding. Gum arabic was suitable for forming agent and 5%(w/v) concentration was the most effective in grinding efficiency. A wet-grinding process operated at 4,000 rpm rotor speed, 0,4 mm bead size, and 0.4 L/hr feeding rate, respectively, produced less than 600 mm(>>90%)-sized particles. In batch systems, 8 cycles of grinding showed higher efficiency, but 20 min of grinding time in continuous processing was more efficient to reduce particle size than the batch processing. Based on the result, the optimum conditions of the wet grinding process were established: operation time of 20 minutes, rotor speed of 4,000 rpm, bead size of 0.4 mm, feed rate of 40 mL/min and 30% mixing ration with water. The size of the resulting ultra fine calcium particles ranged between 40 and 660 mm.

Effect of the Degree of Weathering on the Distribution of Aggregate Particle Size and the Generation of Fine Rock Particles during Crushing of Granite (화강암 파쇄시 풍화정도가 골재 입도분포 및 미석분 발생에 미치는 영향)

  • You, Byoung-Woon;Lee, Jin-Young;Lee, Dong-kil;Cheong, Young-Wook
    • Economic and Environmental Geology
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    • v.55 no.5
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    • pp.429-438
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    • 2022
  • This study evaluated the effect of the degree of weathering on the particle size distribution and the amount of fine particles generated in the aggregate production process during the crushing of igneous rock. Rock samples were collected from three areas with differences in strength from the Schmith hammer measurement at the aggregate quarry in Geochang, Gyeongsangbuk-do. After crushing with a jaw crusher under the same conditions in laboratory, particle size analysis, mineral analysis, chemical analysis, and weathering index were calculated. The Schmidt hammer measurements were 56, 28, and <10, and the CIA and CIW values of weathering index were also different, so the rock samples were classified into hard rock, soft rock, and weathered rock according to the weathering degree. It shows a smaller particle size distribution toward weathered rocks under the microscope, and the proportion of altered clay minerals such as sericite increased. The composition of feldspar and quartz was high for hard rock, and the ratio of muscovite and kaolinite was low. As a result of the crushing of the jaw crusher, hard rock produced a lot of coarse crushed material (13.2mm), while soft rock and weathered rock produced fine crushed material (4.75mm). The former showed the characteristics of the beta distribution curve, and the latter showed the bimodal distribution curve. The production of fine rock particles (based on 0.71mm of sieve, wt. %) increased to 13%<21%<22% in hard rock, soft rock, and weathered rock, and the greater the degree of weathering, the more fine rock particles were generated. The fine particles are recovered by the operation of the sand unit in the wet aggregate production process. Therefore, in order to minimize the amount of sludge generated in the aggregate production process, it was judged that a study on the optimal operation of cyclones could be necessary.

Effect of Fouling Reducing Additives on Membrane Filtration Resistance of Activated Sludge (막오염 감소제가 활성슬러지의 여과저항에 미치는 영향)

  • Chung, Tai Hak;Lee, Jong Hoon;Kim, Hyoung Gun;Bae, Young Kyoung
    • Journal of Korean Society of Environmental Engineers
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    • v.34 no.6
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    • pp.406-413
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    • 2012
  • Effect of three additives, chitosan, ferric chloride, and MPE50 on membrane fouling reduction was studied. They were introduced with various dosing rate into activated sludge, and changes in filtration resistance measured by the batch cell filtration test were evaluated. Both the filtration resistance and the specific cake resistance were minimized at 20 mg/g-MLSS with chitosan, 70 mg/g-MLSS with ferric chloride, and 20 mg/g-MLSS with MPE50 addition, respectively. Introduction of the additives into the activated sludge resulted in reduction of not only cake resistance, but also fouling resistance. However, the chitosan addition to three different activated sludge resulted in three different optimal dose of 10, 20, 30 mg/g-MLSS, respectively. This implies that the optimal dose is dependent on sludge characteristics rather than a constant value. Overdose above the optimal dosage always aggravated filterability in all cases. Zeta potential of sludge flocs, relative hydrophobicity, floc size distribution, soluble EPS concentration and supernatant turbidity were measured in order to analyze fouling reduction mechanism. Nearly neutral surface charge along with the largest particle size was observed at the optimal dose. This could be explained by particle destabilization and restabilization mechanism as positively charged additives were injected into sludge flocs of negative surface charge. Both soluble EPS concentration and supernatant turbidity also showed the lowest value at the optimal dose. These foulants are believed to be coagulated and entrapped in sludge flocs during flocculation. Chitosan and MPE50 which are cationic polymeric substances showed higher reduction in both soluble EPS and fine particles comparing with ferric chloride.

Fabrication of Low Temperature Cofiring Substrate Containing Fluorine by Water Swelling (Water Swelling을 이용한 Fluorine함유 저온소결 기판의 제조)

  • 윤영진;최정헌;이용수;강원호
    • Journal of the Microelectronics and Packaging Society
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    • v.9 no.2
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    • pp.19-25
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    • 2002
  • Glass composed of $Li_2$O.MgO. $MgF_2$.$SiO_2$.$B_2O_3$ for the fabrication of green sheet was prepared by melting process, and glass ceramics was prepared by the process of nucleation and grystal growth for the glass of $Li_2$O.MgO. $MgF_2$.$SiO_2$.$B_2O_3$ system with Lithium fluorhectorite and Lithium boron fluorphlogopite crystal phase. Powderization of the glass ceramics was carried out by water swelling. The average particle size at this point was 2.574 $\mu\textrm{m}$. Slurry was prepared for green sheet using high viscous sol fabricated by water swelling, which shows cleavage phenomenon in prepared glass ceramics. The optimum ratio of powder to water for the tape casting was 18:100, and its viscosity was 11,000~14,000 cps.

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Evaluation of Rutting Behavior of Hot Mix Asphalt using Slag and Waste Foundry Sand as Asphalt Paving Materials (슬래그와 폐주물사를 이용한 아스팔트 혼합물의 소성변형특성에 관한 연구)

  • Lee, Kwan-Ho;Cho, Jae-Yoon;Jeon, Joo-Yong
    • 한국도로학회:학술대회논문집
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    • 2002.10a
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    • pp.89-92
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    • 2002
  • The objective of this research is to evaluate engineering properties of recycled aggregates, slag as coarse & fine aggregate and waste foundry sand(WFS) as fine aggregate, in hot mix asphalt(HMA). In this research, soundness, gradation and particle analysis, abrasion, specific gravity and absorption test were carried out. The optimum asphalt binder content(OAC) for various HMA combinations of recycled aggregate was determined by Marshall Mix Design. The ranges determined is between 7.2% and 7.5%. Indirect tensile test, resilient modulus test, creep test were carried out for characterization of rutting behavior of various combination of HMA. Judging from the limited tests, the HMA with recycled aggregates is not as good rutting resistance as the HMA with common aggregates. After finishing the Wheel tracking test, the application or feasibility for the use of recycled aggregate as asphalt paving material will be determined.

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Effect of Oyster Shell Addition on the Dissolved Air Flotation and Sedimentation of Bulking Sludge (팽화슬러지의 용존공기부상과 침전에 미치는 굴패각 첨가의 영향)

  • Kim, Dong-Seog;Park, Young-Seek
    • Journal of Korean Society of Environmental Engineers
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    • v.29 no.1
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    • pp.82-88
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    • 2007
  • The objective of this study is to examine the effect of the waste oyster shell powder as the addition agent in bulking sludge thickening of paper manufacturing plant using DAF(Dissolved Air Flotation) and gravitational sedimentation. The effect of parameters such as dosage and size distribution of oyster shell were examined. The results showed that the optimum dosage of mixed oyster shell(size range : $\sim250{\mu}m$) was 0.8 g/L. The oyster shell addition of 5.0 g/L in sedimentation process was increased thickening concentration of 3.25 times. When 5.0 g/L of oyster shell was added in DAF process, water content of sludge was decreased from 95.5% to 82.7% in dewatering process using Buchner funnel test device. When size of oyster shell was divided four ranges($\sim53{\mu}m$, $53\sim106{\mu}m$, $106\sim150{\mu}m$, $150\sim250{\mu}m$), optimum size range for the flotation and dewatering was $53\sim106{\mu}m$.

FEA and Model test of Backfill Materials for Underground Facility with Recycling Materials (재활용 재료를 이용한 지하 매설물용 뒤채움재의 모형시험 및 유한요소해석)

  • Lee, Kwan Ho;Kim, Sung Kyum
    • 한국방재학회:학술대회논문집
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    • 2011.02a
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    • pp.177-177
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    • 2011
  • 현재 대부분 사용되는 지하매설물용 뒤채움재는 다짐공법을 많이 사용하고 있으며, 실제로 이러한 방법은 부적절한 다짐으로 인해 침하 및 내구성 저하로 인해 파손을 초래하는 경우가 많다. 이러한 문제를 해결 할 수 있는 하나의 대안으로 유동성 뒤채움재를 이용할 수 있다. 유동성 뒤채움재는 초기 유동성, 시간에 따른 자기 강도 발현 무다짐공법 적용 등 많은 장점을 가지고 있다. 본 연구에서는 현장발생토사, 정수장슬러지 및 폐타이어분말 등 재활용 재료를 이용한 유동성 뒤채움재의 기본물성을 평가하였다. 각각의 재활용재료에 대한 입도 및 비중을 평가하였고, 최적배합설계를 결정하였으며, 모형 시험과 유한요소 해석을 위한 기본 물성값을 위해 일축압축시험, 삼축압축시험, 공진주시험 등을 수행하였다. 최적배합설계를 산정하는 과정에서 수행한 실험중 대표적인 시험으로 자가수평능력 및 자기다짐등에 필요한 유동성을 판단하는 Flow시험(ASTM D 6133) 결과 기준으로 정한 20cm이상의 값을 얻을 수 있었으며 일축압축강도의 경우 시공 후 유지 보수가 용이한 강도인 $3.0kg/cm^2{\sim}5.6kg/cm^2$이하로 설계하였으며 28일재령 일축압축강도 결과 $3.15{\sim}3.74kg/cm^2$라는 유지보수에 적당한 결과값을 나타내었다. 이 배합이 현장에서 사용이 가능하다는 것으로 판단하고 현장모형시험과 유한요소해석를 통하여 현장에서 사용하였을 때 관의 변형과 관에 작용하는 하중변화를 확인하고 현장모형시험과 유한요소해석 간의 상관관계를 규명하였다. 현장 모형 시험은 현장과 비슷하게 제작된 모형을 이용하였으며 최대한 현장과 비슷한 조건에서 뒤채움재를 타설과정 중과 타설이 완료된 상태에서 7일 양생 후 하중재하와 같이 두가지 경우에서 수직 수평토압, 관의 수직 수평변위, 관의 종단변형을 측정하였다. 유한요소해석 프로그램은 Midas GTS를 이용하여 실시하였으며 관의 변형률, 유효응력을 측정하여 규명하였다.

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The Estimation of the Loss Possibility of Zeolite in Sandy Soil (사질토양(砂質土壤)에서의 Zeolite 유실(流失) 가능성(可能性)의 추정(推定))

  • Kang, Shin-Jyung;Choi, Jyung
    • Applied Biological Chemistry
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    • v.29 no.3
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    • pp.311-317
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    • 1986
  • This experiment was conducted to find out the minimum size of pores through that Zeolite particles moved vertically out with percolated solution in the sand column and to estimate whether they were lost through the pores in the field sandy soil. The results were as follows. 1. The amount of Zeolite loss through sand columns was increased in the order of the columns filled with $2{\sim}1>1{\sim}0.5>0.5>0.25mm$ sand particles. 2. The Zeolite particles lost through columns filled with $1{\sim}0.5$ and $0.5{\sim}0.25mm$ sand were clay fraction. 3. The pore sire that clay fraction of Zeolite mineral could migrate through was determined to be above $150{\mu}m$ and Jangchon subsoil was presumed to have possibility of Zeolite loss in consideration of its pore size distribution. 4. The suitable particle size of Zeolite for application in sandy soil was presumed to be above $2{\mu}m$.

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Glass-Ceramics of $Li_2O-Al_2O_3-SiO_2$ System Produced by Sintering (소결법에 의한 $Li_2O-Al_2O_3-SiO_2$계 결정화 유리의 제조)

  • 연석주
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.3 no.2
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    • pp.176-184
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    • 1993
  • The glasses, which the $\beta$-spodumene as the principal crystalline phase could be precipitated, were melted by adding >, $P_2O_5, TiO_2, ZrO_2 in the Li_2O-Al_2O_3-SiO_2$ system. In order to achieve the glass-ceramic body of near-theoritical density by sintering method, the optimum condition of heat treatment, the effect of glass powder size and the properties were investigated by DTA, XRD, bulk density, thermal expansion and SEM. Addition of $P_20_5$ imProved the tendency of sintering and the sample with 9wt% $P_20_5$ content was the most dense OOdy by sintering method. The optimum condition of heat treatmemt was sintered for densitification at $740^{\circ}C$ and crystallized at $950^{\circ}C$. In the optimum condition, the relative density was above 90% and the thermal expansion was negative about $-1{\times}10^{-7}/^{\circ}C$.

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A Study for Preparation of Nano Ethosome Loaded with Resveratrol (레스베라트롤을 함유한 나노 에토좀 제조에 관한 연구)

  • Seo, Dong Hoan;Yoon, Jong Hyuk;Kim, Youn Joon;Byun, Sang Yo
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.41 no.2
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    • pp.105-112
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    • 2015
  • Resveratrol is a natural polyphenol. It protects skin from skin injury, ultraviolet radiation and pathogenic attack. This study is to find the optimum condition for the preparation of ethosome loading amount of resveratrol in ethosome. Ethosomes were prepared by modified hydrated liquid crystal method. Investigation of factors affecting the entrapment efficiency and particle size of ethosomes was carried out. The particle size of ethosome were measured by particle analyzer. The loading efficiency of resveratrol in ethosome was measured by HPLC. The particle sizes were 111.2 ~ 112.8 nm and the loading efficiency of resveratrol was 81.25 ~ 88.75%. The optimum conditions for the preparation of ethosome was obtained from of lecithin : resveratrol : cholesterol : ethanol at a weight ratio of 2.0 : 0.08 : 0.05 : 20.0.